CN107802030A - Fragrant line lilac compound and its application in a kind of ramuscule filter stick - Google Patents

Abstract

The invention belongs to the technical field of slim cigarette filter rod production, and in particular relates to a patent application for a clove flavor used in a slim filter rod for incense thread and its application. In terms of mass percentage, it consists of the following components: 10.0~15.0% clove oil, 2.0~5.0% syringaldehyde, 0.05~0.1% octanal, 0.05~0.1% nonanal, 0.05~0.1% decanal , 0.2~0.5% linalool, 0.1~0.2% terpineol, 79.0~87.55% caprylic acid glyceride. This application not only provides a clove essence with a special flavor for the middle incense thread of slim cigarettes, but also cooperates with the improvement of the filter rod structure of slim cigarettes, which can improve the smoking effect of slim cigarettes, and the improvement effect is obvious, and has a good Practical value, while enriching the types of cigarette products, it has good demonstration, promotion and application significance for the design, development, production and sales of new slim cigarettes.

Description

A kind of clove essence and application thereof for incense thread in fine filter stick

technical field

The invention belongs to the technical field of slim cigarette filter rod production, and in particular relates to a patent application for a clove flavor used in a slim filter rod for incense thread and its application.

Background technique

With the continuous improvement of people's living standards, there are more and more varieties of cigarettes on the cigarette market, which also provides consumers with more choices, and slim cigarettes are a typical example. Judging from the actual sales effect, slim cigarettes have conquered more and more consumers with their unique charm.

Judging from the quality of cigarettes, the tar content of slim cigarettes is generally lower than that of ordinary cigarettes, and the taste is also lighter, so it is more in line with the needs of specific consumers, especially urban women who pursue fashion, elegance and avant-garde life. special favor. With the rapid development of low-tar cigarettes, the advantages of slim cigarettes in "reducing tar and maintaining flavor" have attracted special attention.

Due to the inherent advantages of small cigarette volume and relatively low tar release, slim cigarettes also have problems such as light smoke and insufficient aroma, which also limits their popularization and application. For this reason, existing cigarette manufacturers are also solving this technical problem by reducing the pressure drop of filter rods and optimizing the structure of shredded tobacco.

Focusing on the flavor enhancement of slim cigarettes, in the existing technical ideas, flavor granules and flavor capsules are mainly used to supplement or increase the flavor of cigarettes. Short, poor coordination with smoke and other defects, so that the effect of improving the fragrance is not obvious enough. Therefore, it is extremely necessary to further improve the uniformity, stability and coordination of aroma enhancement through comprehensive means such as flavor formula and improvement of aroma enhancement methods on the basis of existing aroma enhancement methods.

Contents of the invention

The purpose of the present invention is to provide a clove essence for slim filter rods, and at the same time cooperate with the improvement of the structure of the slim filter rods to further improve the flavoring effect of the slim cigarettes while enriching the types of the slim cigarettes.

The technical scheme adopted by this application is described in detail as follows.

A kind of clove essence for fine filter stick medium incense thread, by mass percentage, consists of the following components:

10.0~15.0% clove oil, 2.0~5.0% syringaldehyde,

0.05~0.1% octanal, 0.05~0.1% nonanal, 0.05~0.1% decanal, 0.2~0.5% linalool,

0.1~0.2% terpineol, 79.0~87.55% caprylic capric acid glyceride.

Described clove oil can be finished product, or prepare with reference to following preparation method:

(1) Grind the dried cloves and pass through a 50-60 mesh sieve to obtain clove powder;

(2) Take a certain amount of clove powder and put it into a distillation flask, add a certain amount of distilled water, and steam distill for 4-5 hours to obtain a distillate with oil-water layering;

(3) Extract the oil phase in the distillate with dichloromethane, and dry it with anhydrous sodium sulfate;

(4) After filtering the oil obtained in step (3), the solvent was evaporated in a water bath at 55° C. to obtain clove essential oil.

The clove essence used for the incense thread in the thin filter stick, the specific formula is, for example: 12.0% clove oil, 3.0% syringaldehyde, 0.08% octanal, 0.08% nonanal, 0.08% decanal, 0.35% linalool, 0.16% terpineol, 84.25% caprylic capric glyceride.

The application of the clove essence for thin filter rods in cigarettes is used for fine cigarette filter rods.

A thin composite filter rod with built-in clove essence fragrance thread, the composite filter rod is wrapped with molding paper outside, and the inside is composed of ordinary acetate fiber filter rod section and built-in clove essence fragrance thread acetate fiber filter rod section, and the built-in The clove essence fragrance line acetate fiber filter rod section is close to the cut tobacco section;

Ordinary acetate filter rod section and acetate fiber filter rod section with built-in clove essence fragrance thread, the section shape of the acetate fiber tow used is Y-shaped, and the tow specification requirements are: single denier is 6.0den~11.0den, and total denier is 15000den~ 17000den;

The length ratio of the ordinary acetate filter rod section to the built-in clove essence fragrance thread acetate fiber filter rod section can be adjusted according to the suction resistance or the demand for flavor enhancement. The specific length ratio is, for example, 1:1;

The built-in clove essence fragrance thread acetate fiber filter rod section has a built-in fragrance thread in the middle, and the fragrance thread is adsorbed with clove essence; its preparation process can be prepared according to the existing technology, specifically: the fragrance thread enters the filter rod after coming out of the thread roller. Before the rod forming machine, the fragrance is applied through the fragrance system equipped with a certain concentration of clove essence;

The specific specifications of the composite filter rod are, for example: the length is 120mm, the circumference is 16.90mm, and the pressure drop is 2600Pa~4200Pa.

The amount of essence applied to a single filter stick of the fine-branched incense thread filter stick is 10 mg to 30 mg.

Slim cigarettes are prepared by using the slim composite filter stick with built-in clove essence and fragrance thread.

In the present invention, a clove-flavored essence with a special fragrance is firstly prepared by independently designing the essence formula, which is used as an aroma-increasing additive in the fine-branched incense thread filter rod, and a fine-branched composite filter rod with the clove fragrance is prepared. Clove is pungent and warm in nature and flavor, has the effects of warming the middle and lowering the adverse, warming the kidney and supporting the yang, harmonizing the stomach and relieving vomiting, dispelling wind and cold, and analgesic and antispasmodic effects. Therefore, the fragrance product provided by the application can partially reduce the harmfulness of tobacco while enriching the type of fragrance.

Preliminary application shows that when the composite filter rod of slim incense thread is used in slim cigarettes, it not only improves the uniformity of flavor application and the stability of release, but also improves the coordination between aroma and product sensory quality. Since the clove essence applied is obtained from natural substances, after these aroma substances enter the cigarette smoke, they can highlight the "roasted sweet" aroma of cigarettes, improve the aroma fullness and fullness of slim cigarettes, and then improve their flavor. Smoking quality and sensory comfort.

Compared with the existing perfuming technology, the main advantages of the present invention are:

(1) The process is simple: the preparation process of the present invention is simple, no need to make significant adjustments to the current production process and equipment, no need for large-scale equipment and expensive reagents, simple operation and easy control;

(2) Safe and hygienic: the raw and auxiliary materials adopted in the present invention are widely used in the field of food processing, and there is no problem of toxic reagent residue, so they are safe and reliable;

(3) Stable release: The compound filter stick with built-in incense thread used in the present invention helps to slow down the loss of aroma while avoiding direct contact with the incense thread in the mouth.

In general, while providing a clove essence with a special flavor for the incense thread of slim cigarettes, this application can better improve the smoking effect of slim cigarettes, and improve the effect Obviously, it has good practical value. While enriching the types of cigarette products, it has good demonstration, promotion and application significance for the design, development, production and sales of new slim cigarettes.

Description of drawings

Fig. 1 is the fine branch composite filter stick structural representation of the built-in clove essence fragrance thread provided by the present invention;

Fig. 2 is a schematic diagram of the structure of a slim cigarette prepared by using a slim composite filter stick with a built-in clove flavor thread.

Detailed ways

The present application will be further explained below in conjunction with the embodiments. Before introducing the specific embodiments, it should be noted that the materials such as clove oil, syringaldehyde, octanal, nonanal, decanal, linalool, terpineol, caprylic acid glyceride used in the following examples are all It is the product of Shanghai Huabao Biological Technology Co., Ltd.; incense sticks, fine filter sticks, etc. are also produced according to the existing technology.

Example 1

The clove essence for fine filter stick medium incense thread provided by this embodiment is composed of the following components in terms of mass percentage:

10.0% clove oil, 2.0% syringaldehyde, 0.05% octanal, 0.05% nonanal, 0.05% decanal, 0.2% linalool, 0.1% terpineol 87. 55% octadecyl Glycerides.

According to the prior art, prepare the fine-branched composite filter stick with built-in clove essence fragrance thread, as shown in Figure 1, 2, the prepared composite filter stick 3, the outside is wrapped with molding paper, the inside is made of ordinary acetate fiber filter stick section 2 and built-in filter stick. The clove essence fragrance thread vinegar fiber filter rod section 1 is compounded, and the clove essence fragrance thread acetate fiber filter rod section 1 is built in close to the shredded tobacco section 4;

Ordinary acetate fiber filter rod section 2, the cross-sectional shape of the acetate fiber tow used is Y-shaped, and the specification of the tow is: 6.0Y/17000 (den/den);

Built-in clove essence fragrance thread acetate filter rod section 2, the cross-sectional shape of the acetate tow used is Y-shaped, and the specification of the tow is: 8.0Y/15000 (den/den);

The length ratio of the common acetate filter stick section to the built-in clove essence fragrance thread acetate filter stick section is 1:1; the specific specifications of the composite filter stick are: the length is 120mm, and the circumference is 16.90mm (in Fig. 2, In actual use, the length of the filter tip is 30mm (that is, the structural length of part 1+2 in Figure 2)).

When preparing the fine-branch composite filter stick with built-in clove essence fragrance thread, it is carried out according to the existing filter rod production process, firstly, the fragrance thread applied with clove essence is inserted into the center of the filter rod through a filter rod forming machine to make a fragrance thread filter rod , and then formed into a fine-branched incense thread binary composite filter rod (the fine-branched composite filter rod with built-in clove flavor fragrance thread) through the filter rod compound machine and the ordinary acetate filter rod. After molding, the measurement results show that the amount of clove essence for incense thread in each composite filter stick is about 20mg (that is, the amount of 120mm long filter stick is 20mg).

According to the existing technology, the thin composite filter stick with the built-in clove essence fragrance thread and the tobacco sample are wound into a thin cigarette sample as a test sample, and a blank control sample (blank fragrance thread is added at the same position of the filter rod) is used as a test sample. For the control sample, 7 professional sensory evaluators conducted detection and suction evaluation on the test sample and the control sample respectively. For specific smoke test results and specific smoking evaluation scores, see the table below.

The results of the smoking evaluation show that after the clove flavor is added, the "clove" aroma of the cigarette sample is obvious, the aroma richness of the smoke is improved to a certain extent, the irritation is reduced, the miscellaneous gas is reduced, the fineness of the smoke is improved, and the aftertaste is improved .

Example 2

The clove essence for fine filter stick medium incense thread provided by this embodiment is composed of the following components in terms of mass percentage:

12.0% clove oil, 3.0% syringaldehyde, 0.08% octanal, 0.08% nonanal, 0.08% decanal, 0.35% linalool, 0.16% terpineol, 84.25% caprylic acid Glycerides.

With the filter stick specifications of Example 1, a thin composite filter stick with built-in clove essence fragrance thread was prepared. After molding, the measurement results show that the application amount of clove essence for incense thread in each composite filter stick is about 20 mg.

The slim composite filter rod with the built-in clove essence fragrance line and the tobacco sample were rolled into a slim cigarette sample as a test sample, and the smoking evaluation was carried out.

The results of smoking evaluation show that after adding clove essence, the "clove fragrance" of cigarette samples is more obvious, the richness of smoke aroma is significantly increased, the irritation is significantly reduced, the miscellaneous gas is reduced, the fineness of smoke is significantly improved, and the aftertaste is significantly improved .

Example 3

The clove essence for fine filter stick medium incense thread provided by this embodiment is composed of the following components in terms of mass percentage:

15.0% clove oil, 5.0% syringaldehyde, 0.1% octanal, 0.1% nonanal, 0.1% decanal, 0.5% linalool, 0.2% terpineol, 79.0% caprylic acid Glycerides.

With the filter stick specifications of Example 1, prepare a thin composite filter stick with built-in clove essence fragrance thread. After molding, the measurement results show that the amount of clove essence applied to the incense thread in each composite filter stick is about 20 mg.

The slim composite filter rod with the built-in clove essence fragrance line and the tobacco sample were rolled into a slim cigarette sample as a test sample, and the smoking evaluation was carried out.

The results of smoking evaluation show that after adding clove essence, the "clove fragrance" of the cigarette sample is very obvious, the smoke aroma coordination is reduced, the irritation is increased, the miscellaneous gas is reduced, the smoke coordination is poor and there is an uncomfortable smell. Sweet and greasy, the aftertaste is not as good as normal cigarettes (compared with control cigarettes).

The composite filter sticks prepared in different examples were tested. In addition, the total particulate matter and tar in the mainstream smoke of cigarettes were determined according to the method of "GB/T 19609-2004 Determination of total particulate matter and tar by smoking machine for routine analysis of cigarettes". Indicators such as tar, nicotine and moisture were tested, and the specific results are shown in the table below.

Table 1, the test results of the thin composite filter stick with built-in clove essence fragrance thread prepared by different embodiments:

;

Table 2. Physical indicators and mainstream smoke test results of different cigarette samples:

;

It can be seen from the data in Table 1 above that, compared with the normal cellulose acetate tow filter stick, there is no significant difference in the physical indicators of the filter stick with the clove string placed there. It can be seen from the data in Table 2 that compared with the normal cigarettes of the control example, the mainstream smoke of clove cigarettes has no significant change, and the key indicators affecting the sense of cigarette tar and nicotine have no significant changes.

Table 3, the sensory quality evaluation results of different cigarette samples:

.

From the results in Table 3, it can be seen that the sensory quality of cigarettes can be significantly improved by using the composite filter stick of clove essence and flavor thread, and the sensory score can be increased by up to 1.03 points, the aroma is significantly improved, the aftertaste is improved, and the irritation and miscellaneous gas are also greatly improved. reduce.

To sum up, through the targeted design of flavor formulas for incense filter sticks with specific flavors and applying them to cigarettes, the aroma characteristics of cigarettes can be significantly improved when smoking, and the smoking experience can be enriched and enhanced. The thread filter stick can avoid the rapid loss of conventional incense thread filter sticks, and is safe and hygienic at the same time. Therefore, this application, as a novel clove-flavored thin-branched incense thread composite filter stick that highlights the "clove" aroma of cigarettes and improves smoking quality, has certain promotion and application value in the industry.

Claims (5)

1. A kind of 1. fragrant line lilac compound in ramuscule filter stick, it is characterised in that it is calculated in mass percent, it is composed of the following components：

   10.0 ~ 15.0% caryophyllus oil, 2.0 ~ 5.0% syringaldehyde,

   0.05 ~ 0.1% octanal, 0.05 ~ 0.1% aldehyde C-9,0.05 ~ 0.1% capraldehyde, 0.2 ~ 0.5% linalool,

   0.1 ~ 0.2% terpinol, 79.0 ~ 87. 55% Glycerin, mixed triester with caprylic acid capric acid.
2. 2. fragrant line lilac compound in ramuscule filter stick as claimed in claim 1, it is characterised in that specific formula is：

   12.0% caryophyllus oil, 3.0% syringaldehyde, 0.08% octanal, 0.08% aldehyde C-9,0.08% capraldehyde, 0.35% virtue Camphor tree alcohol, 0.16% terpinol, 84.25% Glycerin, mixed triester with caprylic acid capric acid；

   Or it is：10.0% caryophyllus oil, 2.0% syringaldehyde, 0.05% octanal, 0.05% aldehyde C-9,0.05% capraldehyde, The Glycerin, mixed triester with caprylic acid capric acid of 0.2% linalool, 0.1% terpinol 87. 55%；

   Or it is：15.0% caryophyllus oil, 5.0% syringaldehyde, 0.1% octanal, 0.1% aldehyde C-9,0.1% capraldehyde, 0.5% Linalool, 0.2% terpinol, 79.0% Glycerin, mixed triester with caprylic acid capric acid.
3. 3. application of the fragrant line lilac compound in cigarette in the ramuscule filter stick of claim 1 or 2, it is characterised in that be used for Fragrant line in ramuscule cigarette filter rod.
4. 4. a kind of ramuscule composite filter of built-in lilac compound perfume (or spice) line, it is characterised in that the composite filter outer wrap has into Type paper, inside is combined by common vinegar fibre filter rod segments and built-in lilac compound perfume (or spice) line vinegar fibre filter rod segments, wherein built-in cloves is fragrant The fragrant line vinegar fibre filter rod segments of essence are close to pipe tobacco section；

   Common vinegar fibre filter rod segments and built-in lilac compound perfume (or spice) line vinegar fibre filter rod segments, the cross sectional shape of diacetate fiber used are Y types, silk Beam specification requires：Single-strand is 6.0den ~ 11.0den, and total denier is 15000den ~ 17000den；

   The length ratio of common vinegar fibre filter rod segments and built-in lilac compound perfume (or spice) line vinegar fibre filter rod segments is 1:1；

   The built-in lilac compound perfume (or spice) line vinegar fibre filter rod segments, its middle part are built-in with fragrant line, and fragrant line is adsorbed with lilac compound.
5. 5. existed using ramuscule cigarette, its feature prepared by the ramuscule composite filter of built-in lilac compound perfume (or spice) line described in claim 4 In the essence applied amount of single branch filter stick is 10mg ~ 30mg.