CN107668771A - Fragrant line fennel essence and its application in a kind of ramuscule filter stick - Google Patents

Abstract

The invention belongs to the technical field of slim cigarette filter rod production, and in particular relates to a patent application for fennel flavoring essence for incense thread in slim filter rods and its application. In terms of mass percentage, it consists of the following components: 10.0~15.0% star anise oil, 3.0~5.0% sweet cumin oil, 2.0~5.0% anethole, 0.2~0.5% methyl black pepper phenol, 0.2~0.5% eugenol, 0.1~0.2% linalool, 1.0~2.0% lemon oil, 71.8~83.5% caprylic acid glyceride. This application not only provides an anise flavor essence for slim cigarettes with a special fragrance, but also improves the smoking effect of slim cigarettes with the improvement of the filter rod structure of slim cigarettes, and the improvement effect is obvious. At the same time, it has good demonstration, promotion and application significance for the design, development, production and sales of new slim cigarettes.

Description

A kind of fennel essence for fine-branched filter stick and its application

technical field

The invention belongs to the technical field of slim cigarette filter rod production, and in particular relates to a patent application for fennel flavoring essence for incense thread in slim filter rods and its application.

Background technique

With the continuous improvement of people's living standards, there are more and more varieties of cigarettes on the cigarette market, which also provides consumers with more choices, and slim cigarettes are a typical example. Judging from the actual sales effect, slim cigarettes have conquered more and more consumers with their unique charm.

Judging from the quality of cigarettes, the tar content of slim cigarettes is generally lower than that of ordinary cigarettes, and the taste is also lighter, so it is more in line with the needs of specific consumers, especially urban women who pursue fashion, elegance and avant-garde life. special favor. With the rapid development of low-tar cigarettes, the advantages of slim cigarettes in "reducing tar and maintaining flavor" have attracted special attention.

Due to the inherent advantages of small cigarette volume and relatively low tar release, slim cigarettes also have problems such as light smoke and insufficient aroma, which also limits their popularization and application. For this reason, existing cigarette manufacturers are also solving this technical problem by reducing the pressure drop of filter rods and optimizing the structure of shredded tobacco.

Focusing on the flavor enhancement of slim cigarettes, in the existing technical ideas, flavor granules and flavor capsules are mainly used to supplement or increase the flavor of cigarettes. Short, poor coordination with smoke and other defects, so that the effect of improving the fragrance is not obvious enough. Therefore, it is extremely necessary to further improve the uniformity, stability and coordination of aroma enhancement through comprehensive means such as flavor formula and improvement of aroma enhancement methods on the basis of existing aroma enhancement methods.

Contents of the invention

The purpose of the present invention is to provide an anise essence for the fragrance thread in slim filter sticks, and at the same time cooperate with the improvement of the structure of the slim filter sticks to further improve the flavoring effect of slim cigarettes while enriching the types of slim cigarettes.

The technical solution adopted by this application is described in detail as follows.

A kind of fennel essence for incense sticks in fine filter sticks, which consists of the following components in terms of mass percentage:

10.0~15.0% star anise oil, 3.0~5.0% sweet cumin oil, 2.0~5.0% anethole,

0.2~0.5% methyl black pepper phenol, 0.2~0.5% eugenol, 0.1~0.2% linalool, 1.0~2.0% lemon oil,

71.8~83.5% caprylic capric acid glyceride.

The star anise oil can be prepared by using the finished product, or by referring to the following preparation method:

(1) After the dried star anise is crushed, pass through a 50-60 mesh sieve to obtain star anise powder;

(2) Take a certain amount of star anise powder and put it into a distillation flask, add a certain amount of distilled water, and steam distill for 4~5 hours to obtain a distillate with oil and water layers;

(3) Extract the oil phase in the distillate with dichloromethane, and dry it with anhydrous sodium sulfate;

(4) After filtering the oil obtained in step (3), the solvent was evaporated in a water bath at 55° C. to obtain star anise oil.

The sweet fennel oil can be prepared as a finished product, or with reference to the following preparation method:

(1) After the dried sweet cumin is crushed, pass through a 50-60 mesh sieve to obtain sweet cumin powder;

(2) Put a certain amount of sweet cumin powder into a distillation flask, add a certain amount of distilled water, and steam distill for 4 to 5 hours to obtain a distillate with oil and water layers;

(3) Extract the oil phase in the distillate with dichloromethane, and dry it with anhydrous sodium sulfate;

(4) After filtering the oil obtained in step (3), the solvent was evaporated in a water bath at 55° C. to obtain sweet cumin oil.

Anise essence for incense thread in the thin filter stick, the specific formula is, for example: 12.0% star anise oil, 4.0% sweet cumin oil, 3.0% anethole, 0.35% methyl black pepper phenol, 0.3 % Eugenol, 0.15% Linalool, 1.5% Lemon Oil, 78.7% Caprylic Capric Glycerides.

The application of the fennel essence for thin filter rods in cigarettes is used for fine cigarette filter rods.

A thin composite filter rod with built-in fennel essence fragrance thread, the composite filter rod is wrapped with molding paper outside, and the inside is composed of ordinary acetate fiber filter rod section and built-in fennel essence fragrance thread acetate fiber filter rod section, and the built-in The section of fennel flavored fiber acetate filter rod is close to the cut tobacco section;

Ordinary acetate filter rod section and acetate fiber filter rod section with built-in fennel essence thread, the section shape of the acetate fiber tow used is Y-shaped, and the tow specification requirements are: single denier is 6.0den~11.0den, and total denier is 15000den~ 17000den;

The length ratio of the ordinary acetate filter rod section and the built-in fennel essence fragrance thread acetate fiber filter rod section can be adjusted according to the suction resistance or the demand for flavor enhancement, and the specific length ratio is, for example, 1:1;

The built-in fennel essence fragrance thread acetate fiber filter rod section has a built-in fragrance thread in the middle, and the fragrance thread is adsorbed with fennel essence; its preparation process can be prepared according to the existing technology, specifically: the fragrance thread enters the filter rod after coming out of the thread roller. Before the rod forming machine, the flavor is applied through the flavoring system equipped with a certain concentration of anise flavor;

The specific specifications of the composite filter rod are, for example: the length is 120mm, the circumference is 16.90mm, and the pressure drop is 2600Pa~4200Pa.

The amount of essence applied to a single filter stick of the fine-branched incense thread filter stick is 10 mg to 30 mg.

Slim cigarettes are prepared by using the slim composite filter stick with built-in fennel flavor thread.

In the present invention, firstly, an anise-flavored essence with a special fragrance is prepared by independently designing the essence formula, which is used as an aroma-enhancing additive in a fine-branched incense thread filter rod, and a fine-branched composite filter rod with anise-flavored is prepared. Because fennel has the effects of warming the liver and kidneys, warming stomach qi, dispelling congestion, dispelling cold and relieving pain, regulating qi and harmonizing the stomach, the present application can reduce the harmfulness of tobacco to human health to a certain extent while enriching the types of flavors.

Preliminary application shows that when the composite filter rod of slim incense thread is used in slim cigarettes, it not only improves the uniformity of flavor application and the stability of release, but also improves the coordination between aroma and product sensory quality. Since the applied fennel essence is obtained from natural substances, these aroma substances can further highlight the "roasted sweet" aroma of cigarettes after entering the cigarette smoke, improve the aroma fullness and fullness of slim cigarettes, and then improve their quality. Smoking quality and sensory comfort.

Compared with the existing perfuming technology, the main advantages of the present invention are:

(1) The process is simple: the preparation process of the present invention is simple, no need to make significant adjustments to the current production process and equipment, no need for large-scale equipment and expensive reagents, simple operation and easy control;

(2) Safe and hygienic: the raw and auxiliary materials adopted in the present invention are widely used in the field of food processing, and there is no problem of toxic reagent residue, so they are safe and reliable;

(3) Stable release: The compound filter stick with built-in incense thread used in the present invention helps to slow down the loss of aroma while avoiding direct contact with the incense thread in the mouth.

In general, the present application provides an anise essence for slim cigarettes with a special flavor, and at the same time cooperates with the improvement of the filter rod structure of slim cigarettes, which can better improve the smoking effect of slim cigarettes, and improve the effect Obviously, it has good practical value. While enriching the types of cigarette products, it has good demonstration, promotion and application significance for the design, development, production and sales of new slim cigarettes.

Description of drawings

Fig. 1 is the structural representation of the thin composite filter stick with built-in fennel essence provided by the present invention;

Fig. 2 is a schematic diagram of the structure of slim cigarettes prepared by using the slim composite filter stick with built-in fennel flavor thread.

detailed description

The present application will be further explained below in conjunction with the embodiments. Before introducing specific examples, it should be noted that the materials used in the following examples are star anise oil, sweet cumin oil, anethole, methyl black pepper phenol, eugenol, linalool, etc. The products of Treasure Biotechnology Co., Ltd.; incense sticks, fine filter sticks, etc. are also produced according to the existing technology.

Example 1

The fennel flavor used in the fine filter stick provided in this example is composed of the following components in terms of mass percentage:

10.0% Star Anise Oil, 3.0% Sweet Cumin Oil, 2.0% Anethole, 0.2% Methylpironol, 0.2% Eugenol, 0.1% Linalool, 1.0% Lemon Oil, 83.5% caprylic capric acid glycerides.

According to the prior art, a thin composite filter rod with built-in fennel essence fragrance thread is prepared, as shown in Fig. The fennel essence fragrance thread acetate fiber filter rod section 1 is compounded, and the fennel essence fragrance thread acetate fiber filter rod section 1 is built close to the shredded tobacco section 4;

Ordinary acetate fiber filter rod section 2, the cross-sectional shape of the acetate fiber tow used is Y-shaped, and the specification of the tow is: 6.0Y/17000 (den/den);

Built-in fennel essence fragrance thread acetate filter rod section 2, the cross-sectional shape of the acetate tow used is Y-shaped, and the specification of the tow is: 8.0Y/15000 (den/den);

The length ratio of the ordinary acetate filter stick section to the built-in fennel essence fragrance thread acetate filter stick section is 1:1; the specific specifications of the composite filter stick are: the length is 120mm, and the circumference is 16.90mm (in Fig. 2, In actual use, the length of the filter tip is 30mm (that is, the structural length of part 1+2 in Figure 2)).

When preparing the thin composite filter stick with built-in fennel essence fragrance thread, it is carried out according to the existing filter rod production process, firstly, the fragrance thread applied with fennel essence is inserted into the center of the filter rod through a filter rod forming machine to make a fragrance thread filter rod , and then through the filter stick compound machine and the ordinary acetate filter stick to form a fine-branched incense thread binary composite filter rod (the fine-branched composite filter rod with built-in fennel essence fragrance thread). After molding, the measurement results show that the amount of fennel essence for incense thread in each composite filter stick is about 20mg (that is, the amount of 120mm long filter stick is 20mg).

According to the existing technology, the thin composite filter stick with the built-in fennel essence flavor thread and the tobacco sample are rolled into a thin cigarette sample as a test sample, and a blank control sample (blank incense thread is added at the same position of the filter stick) is used as a test sample. For the control sample, 7 professional sensory evaluators conducted detection and suction evaluation on the test sample and the control sample respectively. For specific smoke test results and specific smoking evaluation scores, see the table below.

The results of the smoking evaluation show that after the addition of fennel essence, the "fennel" aroma of the cigarette sample is obvious, the aroma richness of the smoke is improved to a certain extent, the irritation is reduced, the miscellaneous gas is reduced, the fineness of the smoke is improved, and the aftertaste is improved .

Example 2

The fennel flavor used in the fine filter stick provided in this example is composed of the following components in terms of mass percentage:

12.0% Star Anise Oil, 4.0% Sweet Cumin Oil, 3.0% Anethole, 0.35% Methylpironol, 0.3% Eugenol, 0.15% Linalool, 1.5% Lemon Oil, 78.7% caprylic capric acid glycerides.

With the filter stick specifications of Example 1, a thin composite filter stick with built-in fennel essence fragrance thread was prepared. After molding, the measurement results show that the amount of fennel essence applied to the incense thread in each composite filter stick is about 20 mg.

The slim composite filter stick with the built-in fennel essence flavor thread and the tobacco sample were rolled and connected into a slim cigarette sample as a test sample, and the smoking evaluation was carried out.

The results of smoking evaluation show that after the addition of fennel essence, the "fennel" of the cigarette sample is more obvious, the richness of smoke aroma is significantly increased, the irritation is significantly reduced, the miscellaneous gas is reduced, the fineness of smoke is significantly improved, and the aftertaste is significantly improved .

Example 3

The fennel flavor used in the fine filter stick provided in this example is composed of the following components in terms of mass percentage:

15.0% Star Anise Oil, 5.0% Sweet Cumin Oil, 5.0% Anethole, 0.5% Methylpironol, 0.5% Eugenol, 0.2% Linalool, 2.0% Lemon Oil, 71.8% caprylic capric acid glycerides.

With the filter stick specifications of Example 1, a thin composite filter stick with built-in fennel essence fragrance thread was prepared. After molding, the measurement results show that the amount of fennel essence applied to the incense thread in each composite filter stick is about 20 mg.

The slim composite filter stick with the built-in fennel essence flavor thread and the tobacco sample were rolled and connected into a slim cigarette sample as a test sample, and the smoking evaluation was carried out.

The results of smoking evaluation show that after adding fennel essence, the "fennel" of the cigarette samples is very obvious, the smoke aroma coordination is reduced, the irritation is increased, the miscellaneous gas is reduced, the smoke coordination is poor and there is an uncomfortable smell. Sweet and greasy, the aftertaste is not as good as normal cigarettes (compared with control cigarettes).

The composite filter sticks prepared in different examples were tested. In addition, the total particulate matter and tar in the mainstream smoke of cigarettes were determined according to the method of "GB/T 19609-2004 Determination of total particulate matter and tar by smoking machine for routine analysis of cigarettes". Indicators such as tar, nicotine and moisture were tested, and the specific results are shown in the table below.

Table 1, the detection results of the fine-branched composite filter sticks with built-in fennel essence and fragrance threads prepared in different examples:

;

Table 2. Physical indicators and mainstream smoke test results of different cigarette samples:

.

It can be seen from the data in Table 1 above that, compared with the normal cellulose acetate tow filter stick, there is no significant difference in the physical index of the filter stick with anise thread. It can be seen from the data in Table 2 that, compared with the normal cigarettes of the control example, the mainstream smoke of the anise line cigarettes has no significant change, and the key indicators affecting the sense of cigarette tar and nicotine have no significant changes.

Table 3, the sensory quality evaluation results of different cigarette samples:

.

From the results in Table 3, it can be seen that the sensory quality of cigarettes can be significantly improved by using the composite filter stick of fennel essence flavor thread, and the sensory score can be increased by up to 1.37 points, the aroma is significantly improved, the aftertaste is improved, and the irritation and miscellaneous gas are also greatly improved. reduce.

To sum up, through the targeted design of flavor formulas for incense filter sticks with specific flavors and applying them to cigarettes, the aroma characteristics of cigarettes can be significantly improved when smoking, and the smoking experience can be enriched and enhanced. The thread filter stick can avoid the rapid loss of conventional incense thread filter sticks, and is safe and hygienic at the same time. Therefore, this application, as a novel anise-flavored thin-branch composite filter stick that highlights the "fennel" flavor of cigarettes and improves smoking quality, has certain promotion and application value in the industry.

Claims (5)

1. an anise flavor essence for fragrant thread in a thin filter stick, characterized in that, in terms of mass percentage, it is composed of the following components: 10.0~15.0% star anise oil, 3.0~5.0% sweet cumin oil, 2.0~5.0% anethole, 0.2~0.5% methyl black pepper phenol, 0.2~0.5% eugenol, 0.1~0.2% linalool, 1.0~2.0% lemon oil, 71.8~83.5% caprylic capric acid glyceride. 2. as claimed in claim 1, the fennel essence for fine-branched filter stick middle incense thread is characterized in that, the specific formula is: 12.0% star anise oil, 4.0% sweet fennel oil, 3.0% anethole, 0.35 % methyl black pepper phenol, 0.3% eugenol, 0.15% linalool, 1.5% lemon oil, 78.7% caprylic acid glyceride; Or as: 15.0% Star Anise Oil, 5.0% Sweet Cumin Oil, 5.0% Anethole, 0.5% Methylpironol, 0.5% Eugenol, 0.2% Linalool, 2.0% Lemon oil, 71.8% caprylic acid glyceride; Or as: 10.0% Star Anise Oil, 3.0% Sweet Cumin Oil, 2.0% Anethole, 0.2% Methylpironol, 0.2% Eugenol, 0.1% Linalool, 1.0% Lemon Oil, 83.5% Caprylic Glycerides. 3. The application of the fennel essence for thin filter rods in cigarettes according to claim 1 or 2, characterized in that it is used for fine cigarette filter rods. 4. A thin composite filter rod with built-in fennel essence fragrance thread, characterized in that the composite filter rod is wrapped with molding paper outside, and the interior is composed of ordinary acetate filter rod section and built-in fennel essence fragrance thread acetate fiber filter rod section Composite, in which the built-in fennel essence flavor thread acetate fiber filter rod section is close to the tobacco section; Ordinary acetate filter rod section and acetate fiber filter rod section with built-in fennel essence thread, the section shape of the acetate fiber tow used is Y-shaped, and the tow specification requirements are: single denier is 6.0den~11.0den, and total denier is 15000den~ 17000den; The length ratio of the ordinary acetate filter rod section to the built-in fennel essence fragrance thread acetate filter rod section is 1:1; The built-in fennel essence fragrance thread acetate fiber filter rod segment has a built-in fragrance thread in the middle, and the fragrance thread is adsorbed with fennel essence. 5. The slim cigarettes prepared by using the slim composite filter stick with built-in fennel essence and flavor thread according to claim 4, characterized in that the amount of essence applied to a single filter stick is 10 mg to 30 mg.