CN107034021A - A kind of cigarette quick-fried pearl savory essence of lily and its application in cigarette - Google Patents

Abstract

The invention belongs to cigarette filter rod production technical field, and in particular to a kind of cigarette quick-fried pearl savory essence of lily and its patent application of the application in cigarette.The savory essence of lily is made up of Bulbus Lilii extract, rhodinol, linalool, benzyl carbinol, geranium oil, Glycerin, mixed triester with caprylic acid capric acid.The quick-fried pearl of lily taste cigarette can be prepared using the essence, the quick-fried pearl can be added in filter stick and the quick-fried pearl cigarette application of cigarette is prepared.The application is by providing a kind of savory essence of lily for being specifically used for the quick-fried pearl of cigarette and combining more perfect quick-fried pearl production technology, Forming Quality stabilization, the uniform quick-fried pearl product of cigarette can be prepared, the quick-fried pearl is inserted after cigarette filter, the excitant of cigarette can preferably be weakened, improve and abundant cigarette flavor, the fragrance that is obviously improved cigarette is rich, the interest of aesthetic quality and suction, thus has preferable application value and popularization and application meaning for design, exploitation and the production and sales of quick-fried pearl cigarette.

Description

A kind of lily-flavored essence for popping pearls of cigarettes and its application in cigarettes

technical field

The invention belongs to the technical field of cigarette filter rod production, and in particular relates to a patent application for a lily-flavored essence for popping pearls in cigarettes and its application in cigarettes.

Background technique

In the traditional cigarette flavoring technology, it is mainly to add the flavoring liquid to the shredded tobacco. The liquid added in this way is often partially lost during the burning process of the cigarette. At the same time, due to the unpredictable reaction of the complex material system at high temperature, some Feed liquid can also produce some bad sensory effects. As a new flavoring method of cigarettes, popping pearl flavoring can overcome the defects of existing flavoring methods to a certain extent. The popping beads in the filter stick are re-ignited to smoke cigarettes. At this time, when the smoke passes through the filter tip and the popping beads liquid acts on the consumer, the process of adding flavor and flavoring is completed; On the other hand, because the spices are placed in the sealed pop-up beads, there will be no loss during the storage of the cigarettes, thereby ensuring the stability of the quality of the cigarettes.

As an emerging material in cigarettes, "Puffing Beads" has more and more prominent functions in supplementing, improving, and coordinating cigarette smoking quality and improving, changing, and cigarette product style due to the special release method of its contents. To improve the interest and sensory quality of cigarette smoking, in recent years, "popping pearl" cigarettes are being used more and more in the production of Chinese-style cigarettes, and are also loved by consumers.

In the prior art, although there are a certain number of puffed bead cigarettes on the market, the fragrance in this kind of puffed bead is relatively poor in coordination with the smoke due to the lack of targeted design, and it has an impact on the aroma characteristics of the cigarette itself. Larger, thus affecting the smoking experience of popcorn cigarettes.

Although "Pearl" cigarettes have sprung up like bamboo shoots after rain, due to their relatively new products, the current production standards and specifications are relatively lacking, so many new issues have emerged in the addition and use of "Pearl". Especially in view of the particularity of cigarette products, in terms of the design of the formulation of the "Pearl" content, the stable release of the content, and the impact of the "Pearl" filter stick on the physical indicators, chemical indicators, and hazard index of cigarettes, etc. Rarely reported. Therefore, the contents of "Pearls" with different components are designed, and the release law of the special contents of "Pearls" is systematically studied, and the impact of the contents of "Pearls" on the physical indicators, smoke indicators, and hazard indexes of cigarettes, etc. It has important theoretical and practical significance.

Contents of the invention

The purpose of the present invention is to provide a pertinent lily-flavored essence used in cigarette filter sticks, thereby enriching types of cigarette products and providing cigarette products with different styles and characteristics.

The technical solution adopted by this application is described in detail as follows.

A lily-flavored essence for popping cigarettes, in mass percentage, consists of the following components:

5.0~10.0% lily extract,

1.0~3.0% rose alcohol,

2.0~5.0% linalool,

8.0~12.0% phenylethyl alcohol,

4.0~8.0% geranium oil,

62.0~80.0% caprylic capric acid glyceride.

The lily extract is the ethanol extract of lily;

The caprylic capric acid glyceride is medium-chain triglyceride (MCT), which is a product of esterification of fatty acid with 8-12 carbon chains and glycerol.

The lily extract can be prepared with reference to the following steps:

(1) After the dried lily is crushed, pass through a 45-55 mesh sieve to prepare lily powder;

(2) Add ethanol solution with a volume fraction of 65-85% to the lily powder in step (1), and reflux in a water bath at 60-80°C for 4-6 hours; the solid-liquid ratio of lily powder to ethanol solution is, lily powder: ethanol =1g: 4~6mL;

(3) Concentrate the heated reflux liquid in step (2) under reduced pressure at 55-65°C and 65-75Kpa until the volume does not change, and the obtained extract is the lily extract.

The lily-flavored essence for cigarette popping pearls, the specific formula is, for example: 7.0% lily extract, 2.0% rose alcohol, 3.5% linalool, 10.50% phenylethyl alcohol, 6.0% geranium oil and 71.0% of caprylic capric acid glyceride.

It needs to be explained that different flavors are generally specially designed according to their uses. The lily-flavored flavor described in this application combines the characteristics of the production process of cigarette popping beads and is specially designed according to the use of the final cigarette, so as to ensure On the basis of the quality of the popping beads, the results of adjusting the quality of smoke and improving the quality of cigarette smoking can be better achieved.

The lily-flavored cigarette popping beads prepared by using the lily-flavored flavor of the cigarette popping beads, the cigarette popping beads refer to using natural polymer materials or synthetic polymer materials to wrap flavors and fragrances in a closed popping beads, Form a kind of sealed popping beads with different colors, mostly round. The diameter of the popping beads is 2.0~4.0mm. / grain; the essence content in the popping beads is 23μL / grain, in a word, its specific specification can be adjusted according to the different machine equipment and the different filter rod specifications used;

For the application of the lily-flavored cigarette popping beads in cigarettes, the cigarette popping beads are added to the filter rod, added to the ordinary (circumference 24.3mm) cigarette filter rod, preferably set in the middle of the cigarette filter rod, that is, the popping beads are located at At a distance of about 12.5mm from the lip end, each cigarette can add one popping bead.

The lily-flavored essence for cigarette popping beads provided in this application has obvious herbal aroma, and these aromas are the most important aroma characteristics in cigarette smoke; after it is prepared into the product form of "popping beads" and applied to cigarettes, the product The smoking results show that: compared with the control sample, the use of Lily-flavored cigarettes can not only improve the richness of smoke aroma, but also enhance the fullness of smoke without changing the smoke aroma style of the cigarettes. Feeling and richness, thereby improving the coordination between aroma and product sensory quality, and increasing the fun of smoking cigarettes; at the same time, because lily has the functions of nourishing yin and moistening lungs, clearing heart and calming nerves, etc., this application has the effect of reducing cigarette smoking to a certain extent. Harmful effect.

Generally speaking, the lily-flavored essence used in this application is extracted from natural lily, so these aroma substances can reduce the irritation of the smoke after entering the cigarette smoke, and improve the softness and roundness of the cigarette smoke. Degree, aroma fullness and plumpness, thereby improving its smoking quality and sensory comfort.

In a word, by providing a lily-flavored essence specifically used for cigarette popping beads and a relatively perfect combination of popping beads production process, the present application can prepare and obtain cigarette popping beads products with stable and uniform molding quality, and put the popping beads into cigarette filters After the mouth, it can better reduce the irritation of cigarettes, improve and enrich the aroma of cigarettes, significantly enhance the richness of aroma, sensory quality and fun of smoking, and because it has certain functions of nourishing yin and moistening lungs, clearing heart and tranquilizing mind, and reducing the harm of cigarettes and other effects, so it has good application value and promotion and application significance for the design, development, production and sales of popcorn cigarettes.

detailed description

The present invention is further explained below in conjunction with embodiment. Before introducing the specific examples, firstly, the preparation process of the cigarette popping beads described in the following examples is briefly introduced as follows.

The main preparation process of the cigarette quick-fried beads of the prior art is as follows:

The mainstream technology of popping beads production mainly adopts the split flow method-in-liquid dripping method for production, that is, the shear force of cooling oil is used to cut off the glue column to complete the popping beads dripping system; specifically: first, use two different incident angles The cooling oil forms a shear force in the solenoid, cuts off the wall material and core liquid during the dripping process, and finally condenses into balls in the cooling oil by virtue of the surface tension, and then goes through degreasing, drying, screening, etc. After the procedure, the final finished product popping beads are made; the popping beads prepared in the following examples are entrusted to Shanghai Huabao Biotechnology Co., Ltd. for processing by this method;

It should also be noted that the materials used in the following examples: rhodamine, linalool, phenylethyl alcohol, geranium oil, caprylic capric acid glyceride, etc. are also products of Shanghai Huabao Biotechnology Co., Ltd.;

The lily extract used in the following examples is prepared according to the following steps:

(1) After the dried lily is crushed, pass through a 50-mesh sieve to prepare lily powder;

(2) Add ethanol solution with a volume fraction of 75% to the lily powder in step (1), and reflux in a water bath at 70°C for 5 hours; the solid-liquid ratio of lily powder to ethanol solution is, lily powder:ethanol=1g:5mL;

(3) The heat reflux liquid in step (2) is concentrated under reduced pressure at 60°C and 70Kpa until the volume does not change, and the obtained extract is the lily extract.

Example 1

The lily-flavored essence for popping cigarettes in the present embodiment is composed of the following components in terms of mass percentage:

5.0% lily extract, 1.0% rose alcohol, 2.0% linalool, 8.0% phenylethyl alcohol, 4.0% geranium oil, 80.0% caprylic acid glyceride.

The lily-flavored flavor was prepared into cigarette popping beads with a diameter of 3.65 mm and a weight of 23 mg/cap. The flavor content in the popping beads was 23 μL/cap, which was the lily-flavored cigarette popping beads.

According to the existing filter rod production process, after the popping beads are inserted into the center of the filter rod through the filter rod forming machine, the popping ball filter rod is formed, and after being rolled into a cigarette sample, the lily-flavored popping pearl cigarette is obtained.

For the prepared Lily-flavored puffed pearl cigarettes, 7 professional sensory evaluators conducted detection and comparative smoking evaluation on the sample and the blank cigarette sample of the control example (blank puffed pearls were added at the same position).

For smoke detection and specific smoking evaluation scores, see the following table.

The results of the smoking evaluation show that the 7 cigarette reviewers agreed that after the addition of lily-flavored cigarettes, the "lily-flavored" aroma of the cigarette samples was obvious, and the richness of the aroma of the smoke was improved to a certain extent. The aroma is enhanced, there is a sense of sweetness, the irritation is reduced, the miscellaneous gas is reduced, the fineness of the smoke is improved, and the aftertaste is improved.

Example 2

The lily-flavored essence for popping cigarettes in the present embodiment is composed of the following components in terms of mass percentage:

7.0% lily extract, 2.0% rose alcohol, 3.5% linalool, 10.50% phenylethyl alcohol, 6.0% geranium oil and 71.0% caprylic acid glyceride.

The lily-flavored flavor was prepared into cigarette popping beads with a diameter of 3.65 mm and a weight of 23 mg/cap. The flavor content in the popping beads was 23 μL/cap, which was the lily-flavored cigarette popping beads.

According to the existing filter rod production process, the blasting beads are put into the center of the filter rod through the filter rod forming machine, and added to the ordinary (circumference 24.3mm) cigarette filter rod. The position of the blasting beads is 12.5mm from the lip end, and one One grain of popping pearls is the popping pearl filter rod, and after being rolled and connected into a cigarette sample, it is a lily-flavored popping pearl cigarette.

For the prepared Lily-flavored puffed pearl cigarettes, 7 professional sensory evaluators conducted detection and comparative smoking evaluation on the sample and the blank cigarette sample of the control example (blank puffed pearls were added at the same position).

For smoke detection and specific smoking evaluation scores, see the following table.

The results of the smoking evaluation show that the 7 cigarette reviewers agreed that after the addition of lily-flavored cigarettes, the "lily fragrance" of the cigarette samples is more obvious, the richness of the smoke aroma is significantly increased, and the sweetness and burnt sweetness are felt. Significantly enhanced, there is a clear sense of sweetness, the irritation is significantly reduced, the miscellaneous gas is reduced, the fineness of the smoke is significantly improved, and the aftertaste is significantly improved.

Example 3

The lily-flavored essence for popping cigarettes in the present embodiment is composed of the following components in terms of mass percentage:

10.0% lily extract, 3.0% rose alcohol, 5.0% linalool, 12.0% phenylethyl alcohol, 8.0% geranium oil and 62.0% caprylic acid glycerides.

The lily-flavored flavor was prepared into cigarette popping beads with a diameter of 3.65 mm and a weight of 23 mg/cap. The flavor content in the popping beads was 23 μL/cap, which was the lily-flavored cigarette popping beads.

According to the existing filter rod production process, the blasting beads are put into the center of the filter rod through the filter rod forming machine, and added to the ordinary (circumference 24.3mm) cigarette filter rod. The position of the blasting beads is 12.5mm from the lip end, and one One grain of popping pearls is the popping pearl filter rod, and after being rolled and connected into a cigarette sample, it is a lily-flavored popping pearl cigarette.

For the prepared Lily-flavored puffed pearl cigarettes, 7 professional sensory evaluators conducted detection and comparative smoking evaluation on the sample and the blank cigarette sample of the control example (blank puffed pearls were added at the same position).

For smoke detection and specific smoking evaluation scores, see the following table.

The results of the smoking evaluation show that the 7 cigarette reviewers agreed that after the addition of lily-flavored cigarettes, the "lily fragrance" of the cigarette samples is very obvious, the coordination of the smoke aroma is reduced, the irritation is increased, and the miscellaneous gas is reduced. The smoke coordination is poor and has an uncomfortable sweet and greasy feeling, and the aftertaste is not as good as that of normal cigarettes (control cigarettes).

The quick-fried pearl products prepared in different embodiments were detected, and the cigarettes prepared in the above-mentioned embodiments were tested routinely, so as to analyze the physical and chemical indicators of the cellulose acetate tow samples in the cigarette samples, the physical indicators of the filter stick samples, and the cigarette samples. In addition, according to the method of "GB/T 19609-2004 Determination of total particulate matter and tar by smoking machine for routine analysis of cigarettes", the indicators of total particulate matter, tar, nicotine and moisture in mainstream smoke of cigarettes were measured The tests were carried out and the specific results are shown in the table below.

Table 1, the detection results of the quick-fried beads prepared in different examples:

.

Table 2, the test results of the filter sticks containing explosive beads prepared by different embodiments:

.

Table 3. Physical indicators and mainstream smoke test results of different cigarette samples:

.

From the above data in Table 2, it can be seen that compared with the normal cellulose acetate tow filter rod, there is no significant difference in the physical indicators of the filter rod with lily popping beads, mainly due to the significant change in the pressure drop of the filter rod. From the data in Table 3, it can be seen that compared with the normal cigarettes of the control example, the mainstream smoke of the Lily-flavored pop-pear cigarettes has changed, but after the puff-puff beads are pinched, the key indicators that affect the cigarette’s senses, such as tar and nicotine, have not changed significantly .

Table 4, the sensory quality evaluation results of different cigarette samples:

.

From the results in Table 4, it can be seen that the sensory quality of cigarettes can be significantly improved by using Lily Balls. The sensory score can be increased by up to 1.23 points.

To sum up, through the targeted design of a specific scented bead formula, after applying it to cigarettes, it can significantly improve the aroma characteristics of cigarettes when smoking, enrich and enhance the smoking experience, and at the same time, due to the special efficacy of lily, it can also reduce the harm of cigarettes . Therefore, this application, as a new type of lily popping beads that highlights the "lily" fragrance of cigarettes, improves the quality of smoking, and reduces the harm of cigarettes, has certain promotion and application value in the industry.

It should be emphasized that the above-mentioned popping bead formula is designed for the improvement of formula cigarettes, and it also has good application effect when applied to slim cigarettes, but the specifications of the popping bead and the addition of The amount is adjusted appropriately and will not be described in detail here.

Claims (6)

1. a lily-flavored essence for quick-fried pearls of cigarettes, characterized in that, by mass percentage, it is composed of the following components: 5.0~10.0% lily extract, 1.0~3.0% rose alcohol, 2.0~5.0% linalool, 8.0~12.0% phenylethyl alcohol, 4.0~8.0% geranium oil, 62.0~80.0% caprylic acid glyceride; The lily extract is the ethanol extract of lily. 2. as claimed in claim 1, the lily-flavored essence for popping pearls for cigarettes is characterized in that, 7.0% lily extract, 2.0% rose alcohol, 3.5% linalool, 10.50% phenylethyl alcohol, 6.0% incense Leaf oil and 71.0% caprylic glyceride. 3. The lily-flavored cigarette popping beads prepared by using the lily-flavored essence for cigarette popping beads according to claim 1, characterized in that, the diameter of the popping beads is 2.0-4.0 mm; 4. The Lily-flavored cigarette popping beads according to claim 3, characterized in that, the popping beads have a diameter of 3.65 mm, a weight of 23 mg per capsule, and the flavor content in the popping beads is 23 μL per capsule. 5. The application of the lily-flavored cigarette quick-fried pearls in claim 3, characterized in that the cigarette quick-fried pearls are added to the filter rod. 6. The application of lily-flavored cigarette popping beads in cigarettes as claimed in claim 5, wherein the cigarette popping beads are located in the middle of the filter rod, and one popping pearl is added to each cigarette filter rod.