CN106947599A - A kind of cigarette quick-fried pearl HERBA DENDROBII essence and its application in cigarette - Google Patents

Abstract

The invention belongs to cigarette filter rod production technical field, and in particular to a kind of cigarette quick-fried pearl HERBA DENDROBII essence and its patent application of the application in cigarette.The HERBA DENDROBII essence is made up of golden hairpin dendrobium extract, beta pinene, linalool, gaultherolin, laurene, myrrh oil, Glycerin, mixed triester with caprylic acid capric acid.The quick-fried pearl of HERBA DENDROBII cigarette can be prepared using the essence, the quick-fried pearl can be added in filter stick and the quick-fried pearl cigarette application of cigarette is prepared.The application is by providing a kind of HERBA DENDROBII essence for being specifically used for the quick-fried pearl of cigarette and combining more perfect quick-fried pearl production technology, Forming Quality stabilization, the uniform quick-fried pearl product of cigarette can be prepared, the quick-fried pearl is inserted after cigarette filter, the excitant of cigarette can preferably be weakened, improve and abundant cigarette flavor, the fragrance that is obviously improved cigarette is rich, the interest of aesthetic quality and suction, thus has preferable application value and popularization and application meaning for design, exploitation and the production and sales of quick-fried pearl cigarette.

Description

Dendrobium nobile essence for popping pearls in cigarettes and its application in cigarettes

technical field

The invention belongs to the technical field of cigarette filter rod production, and in particular relates to a patent application for a dendrobium nobile essence for popping pearls in cigarettes and its application in cigarettes.

Background technique

In the traditional cigarette flavoring technology, it is mainly to add the flavoring liquid to the shredded tobacco. The liquid added in this way is often partially lost during the burning process of the cigarette. At the same time, due to the unpredictable reaction of the complex material system at high temperature, some Feed liquid can also produce some bad sensory effects. As a new flavoring method of cigarettes, popping pearl flavoring can overcome the defects of existing flavoring methods to a certain extent. The popping beads in the filter stick are re-ignited to smoke cigarettes. At this time, when the smoke passes through the filter tip and the popping beads liquid acts on the consumer, the process of adding flavor and flavoring is completed; On the other hand, since the spices are placed in the sealed pop-up beads, there will be no loss during the storage of the cigarettes, thereby ensuring the stability of the quality of the cigarettes.

As an emerging material in cigarettes, "Puffing Beads" has more and more prominent functions in supplementing, improving, and coordinating cigarette smoking quality and improving, changing, and cigarette product style due to the special release method of its contents. To improve the interest and sensory quality of cigarette smoking, in recent years, "popping pearl" cigarettes are being used more and more in the production of Chinese-style cigarettes, and are also loved by consumers.

In the prior art, although there are a certain number of puffed bead cigarettes on the market, the fragrance in this kind of puffed bead is relatively poor in coordination with the smoke due to the lack of targeted design, and it has an impact on the aroma characteristics of the cigarette itself. Larger, thus affecting the smoking experience of popcorn cigarettes.

Although "Pearl" cigarettes have sprung up like bamboo shoots after rain, due to their relatively new products, the current production standards and specifications are relatively lacking, so many new issues have emerged in the addition and use of "Pearl". Especially in view of the particularity of cigarette products, in terms of the design of the formulation of the "Pearl" content, the stable release of the content, and the impact of the "Pearl" filter stick on the physical indicators, chemical indicators, and hazard index of cigarettes, etc. Rarely reported. Therefore, the contents of "Pearls" with different components are designed, and the release law of the special contents of "Pearls" is systematically studied, and the influence of the contents of "Pearls" on the physical indicators, smoke indicators, and hazard indexes of cigarettes, etc. It has important theoretical and practical significance.

Contents of the invention

The purpose of the present invention is to provide a pertinent Dendrobium nobile essence used in cigarette filter rods, thereby enriching the types of cigarette products and providing cigarette products with different style characteristics.

The technical solution adopted by this application is described in detail as follows.

A Dendrobium nobile essence for popping pearls in cigarettes, in terms of mass percentage, consists of the following components:

10.0~15.0% Dendrobium nobile extract,

1.0~2.0% β-pinene,

0.3~0.6% of linalool,

0.5~1.0% methyl salicylate,

0.2~0.5% myrcene,

1.0~2.0% myrrh oil,

78.9~87.0% caprylic capric acid glyceride.

The Dendrobium nobile extract is the ethanol extract of Dendrobium nobile;

The caprylic capric acid glyceride is medium-chain triglyceride (MCT), which is a product of esterification of fatty acid with 8-12 carbon chains and glycerol.

The Dendrobium nobile extract can be prepared by referring to the following steps:

(1) After the dried Dendrobium nobile is crushed, pass through a 40-60 mesh sieve to prepare Dendrobium nobile powder;

(2) Add an ethanol solution with a volume fraction of 60-90% to the Dendrobium nobile powder in step (1), and reflux in a water bath at 60-80°C for 3-5 hours; the solid-liquid ratio of the Dendrobium nobile powder to the ethanol solution is, Dendrobium nobile powder: ethanol=1g: 4~6mL;

(3) The heat reflux liquid in step (2) is concentrated under reduced pressure at 55-65°C and 60-80Kpa until the volume does not change, and the obtained extract is the Dendrobium nobile extract.

The Dendrobium nobile essence is used for the cigarette popping pearls, and the specific formula is, for example: 12% Dendrobium nobile extract, 1.5% β-pinene, 0.4% linalool, 0.7% methyl salicylate, 0.35 % myrcene, 1.5% myrrh oil and 83.55% caprylic capric glycerides.

What needs to be explained is that different flavors have different formulas according to their uses, and their formulas are generally specially designed. The Dendrobium nobile flavor described in this application is combined with the production process characteristics of cigarette popping beads, and at the same time, it is specially designed according to the use in the final cigarette. On the basis of ensuring the quality of popping beads, the results of adjusting the quality of smoke and improving the quality of cigarette smoking can be better achieved.

The Dendrobium nobile cigarette popping beads prepared by using the Dendrobium nobile essence for the cigarette popping beads, the cigarette popping beads refer to using natural polymer materials or synthetic polymer materials to wrap flavors and fragrances in an airtight popping beads Among them, a kind of sealed popping beads with different colors, which are mostly round, is formed. The diameter of the popping beads is 2.0~4.0mm, and the flavor content in the popping beads is 20~25μL/capsule; for example: the diameter of the popping beads is 3.65mm, the weight It is 23mg/capsule; the essence content in the popping beads is 23μL/capsule. In a word, its specific specification can be adjusted according to the different machine equipment and the different specifications of the filter rod used.

For the application of the Dendrobium nobile cigarette popping beads in cigarettes, the cigarette popping beads are added to ordinary (circumference 24.3 mm) cigarette filter rods, and the position of the popping beads is 12.5 mm from the lip end, and one popping bead is added to each cigarette.

The Dendrobium nobile essence for cigarette popping pearls provided in this application has obvious sweet and herbal aroma, and these aromas are the most important aroma characteristics in cigarette smoke; it is prepared into the product form of "popping pearls" and applied After smoking the cigarettes, the results of smoking showed that compared with the control sample, the Dendrobium nobile cigarettes can not only change the aroma style of the cigarette smoke, but also significantly improve the richness of the smoke aroma. , enhance the fullness and richness of the smoke, thereby improving the coordination between the aroma and the sensory quality of the product, and increasing the fun of smoking cigarettes; It has the effects of moistening lung and relieving cough, nourishing yin and clearing away heat, promoting body fluid and quenching thirst, etc., thus making this application have the effect of reducing the harm of cigarette smoking to a certain extent.

Generally speaking, the Dendrobium nobile essence used in this application is extracted from natural Dendrobium nobile, so these aroma substances can reduce the irritation of the smoke after entering the cigarette smoke and improve the quality of the cigarette smoke. The soft roundness, richness and plumpness of aroma can improve its smoking quality and sensory comfort.

In a word, this application provides a Dendrobium nobile essence specially used for cigarette popping beads and a relatively perfect popping pearl production process, which can prepare and obtain cigarette popping pearl products with stable and uniform molding quality, and put the popping pearls into cigarettes After the filter tip, it can better reduce the irritation of cigarettes, improve and enrich the aroma of cigarettes, and significantly improve the aroma richness, sensory quality and fun of smoking of cigarettes. It has the effects of nourishing the stomach, nourishing the lungs and relieving cough, nourishing yin and clearing heat, promoting body fluid and quenching thirst, and reducing the harm of cigarettes. Therefore, it has good application value and promotion significance for the design, development, production and sales of popcorn cigarettes.

detailed description

The present invention is further explained below in conjunction with embodiment. Before introducing the specific examples, firstly, the preparation process of the cigarette popping beads described in the following examples is briefly introduced as follows.

The main preparation process of the cigarette quick-fried beads of the prior art is as follows:

The mainstream technology of popping beads production mainly adopts the split flow method-in-liquid dripping method for production, that is, the shear force of cooling oil is used to cut off the glue column to complete the popping beads dripping system; specifically: first, use two different incident angles The cooling oil forms a shear force in the solenoid, cuts off the wall material and core liquid during the dripping process, and finally condenses into balls in the cooling oil by virtue of the surface tension, and then goes through degreasing, drying, screening, etc. After the procedure, the final finished product popping beads are made; the popping beads prepared in the following examples are entrusted to Shanghai Huabao Biotechnology Co., Ltd. for processing by this method;

It should also be noted that the materials used in the following examples: β-pinene, linalool, methyl salicylate, myrcene, myrrh oil and glyceryl capricate, etc. are all from Shanghai Huabao Biological Co., Ltd. Technology Co., Ltd. company products;

The Dendrobium nobile extract used in the following examples is prepared according to the following steps:

(1) After the dried Dendrobium nobile is crushed, pass through a 50-mesh sieve to prepare Dendrobium nobile powder;

(2) Add an ethanol solution with a volume fraction of 75% to the Dendrobium nobile powder in step (1), and reflux in a water bath at 70°C for 4 hours; the solid-liquid ratio of the Dendrobium nobile powder to the ethanol solution is: =1g:5mL;

(3) The heat reflux liquid in step (2) is concentrated under reduced pressure at 60°C and 70Kpa until the volume does not change, and the obtained extract is the Dendrobium nobile extract.

Example 1

The Dendrobium nobile essence for popping cigarettes in the present embodiment is composed of the following components in terms of mass percentage:

10% Dendrobium nobile extract, 1.0% β-pinene, 0.3% linalool, 0.5% methyl salicylate, 0.2% myrcene, 1.0% myrrh oil and 87.0% octyl Glyceryl caprate.

The Dendrobium nobile essence was prepared into cigarette popping beads with a diameter of 3.65 mm and a weight of 23 mg/capsule. The flavor content in the popping beads was 23 μL/capsule, which was Dendrobium nobile cigarette popping beads.

According to the existing filter rod production process, the blasting beads are put into the center of the filter rod through the filter rod forming machine, and added to the ordinary (circumference 24.3mm) cigarette filter rod. The position of the blasting beads is 12.5mm from the lip end, and one Popping beads, that is, the popping beads filter rod, and after the cigarette sample is rolled, it is the Dendrobium nobile popping beads cigarette.

For the prepared Dendrobium nobile puffed pearl cigarettes, 7 professional sensory evaluators conducted detection and comparative smoking evaluation on the sample and the blank cigarette sample of the control example (blank puffed puffed pearls were added at the same position).

For smoke detection and specific smoking evaluation scores, see the following table.

The results of the smoking evaluation show that the 7 cigarette reviewers agreed that after the addition of Dendrobium nobile cigarettes, the cigarette samples had a clear aroma of "Dendrobium nobile", and the aroma of the smoke was improved to a certain extent. The fragrance and burnt sweetness are enhanced, there is a sense of sweetness, the irritation is reduced, the miscellaneous gas is reduced, the fineness of the smoke is improved, and the aftertaste is improved.

Example 2

The Dendrobium nobile essence for popping cigarettes in the present embodiment is composed of the following components in terms of mass percentage:

12% Dendrobium nobile extract, 1.5% beta-pinene, 0.4% linalool, 0.7% methyl salicylate, 0.35% myrcene, 1.5% myrrh oil and 83.55% octyl Glyceryl caprate.

The Dendrobium nobile essence was prepared into cigarette popping beads with a diameter of 3.65 mm and a weight of 23 mg/capsule. The flavor content in the popping beads was 23 μL/capsule, which was Dendrobium nobile cigarette popping beads.

According to the existing filter rod production process, the popping beads are put into the center of the filter rod through the filter rod forming machine, and added to the ordinary circumference (24.3mm) cigarette filter rod. Popping beads, that is, the popping beads filter rod, and after the cigarette sample is rolled, it is the Dendrobium nobile popping beads cigarette.

For the prepared Dendrobium nobile puffed pearl cigarettes, 7 professional sensory evaluators conducted detection and comparative smoking evaluation on the sample and the blank cigarette sample of the control example (blank puffed puffed pearls were added at the same position).

For smoke detection and specific smoking evaluation scores, see the following table.

The results of the smoking evaluation showed that the 7 cigarette smokers agreed that after the addition of Dendrobium nobile cigarettes, the "Dendrobium nobile fragrance" of the cigarette samples was more obvious, and the richness of the smoke aroma increased significantly, and the sweetness and The burnt sweet aroma is obviously enhanced, there is a clear sense of sweetness, the irritation is significantly reduced, the miscellaneous gas is reduced, the fineness of the smoke is significantly improved, and the aftertaste is significantly improved.

Example 3

The Dendrobium nobile essence for popping cigarettes in the present embodiment is composed of the following components in terms of mass percentage:

15% Dendrobium nobile extract, 2.0% beta-pinene, 0.6% linalool, 1.0% methyl salicylate, 0.5% myrcene, 2.0% myrrh oil and 78.9% octyl Glyceryl caprate.

The Dendrobium nobile essence was prepared into cigarette popping beads with a diameter of 3.65 mm and a weight of 23 mg/capsule. The flavor content in the popping beads was 23 μL/capsule, which was Dendrobium nobile cigarette popping beads.

According to the existing filter rod production process, the popping beads are put into the center of the filter rod through the filter rod forming machine, and added to the ordinary circumference (24.3mm) cigarette filter rod. Popping beads, that is, the popping beads filter rod, and after the cigarette sample is rolled, it is the Dendrobium nobile popping beads cigarette.

For the prepared Dendrobium nobile puffed pearl cigarettes, 7 professional sensory evaluators conducted detection and comparative smoking evaluation on the sample and the blank cigarette sample of the control example (blank puffed puffed pearls were added at the same position).

For smoke detection and specific smoking evaluation scores, see the following table.

The results of the smoking evaluation showed that the 7 cigarette smokers agreed that after the addition of Dendrobium nobile cigarettes, the "Dendrobium nobile fragrance" of the cigarette samples was very obvious, the aroma of the smoke decreased, and the irritation increased. The miscellaneous gas is reduced, the smoke coordination is poor and there is an uncomfortable sweet and greasy feeling, and the aftertaste is not as good as that of normal cigarettes (control cigarettes).

The quick-fried pearl products prepared in different embodiments were detected, and the cigarettes prepared in the above-mentioned embodiments were tested routinely, so as to analyze the physical and chemical indicators of the cellulose acetate tow samples in the cigarette samples, the physical indicators of the filter stick samples, and the cigarette samples. In addition, according to the method of "GB/T 19609-2004 Determination of total particulate matter and tar by smoking machine for routine analysis of cigarettes", the indicators of total particulate matter, tar, nicotine and moisture in mainstream smoke of cigarettes were measured The tests were carried out and the specific results are shown in the table below.

Table 1, the detection results of the quick-fried beads prepared in different examples:

.

Table 2, the test results of the filter sticks containing explosive beads prepared by different embodiments:

Table 3. Physical indicators and mainstream smoke test results of different cigarette samples:

.

As can be seen from the data in Table 2 above, compared with normal cellulose acetate tow filter rods, the physical indicators of the filter rods placed with Dendrobium nobile beads have no significant difference, mainly due to the significant change in the pressure drop of the filter rods. It can be seen from the data in Table 3 that, compared with the normal cigarettes of the control example, the mainstream smoke of the Dendrobium nobile pop-pear cigarettes has changed, but after the puff-puff beads are pinched, the key indicators that affect the senses of the cigarettes are not significantly tar and nicotine. Variety.

Table 4, the sensory quality evaluation results of different cigarette samples:

.

It can be seen from the results in Table 4 that the sensory quality of cigarettes can be significantly improved by using Dendrobium nobile pearls. The sensory score can be increased by up to 1.15 points, the aroma is significantly improved, the aftertaste is improved, and the irritation and miscellaneous gas are also greatly reduced.

To sum up, through the targeted design of a specific scented bead formula and applying it to cigarettes, it can significantly improve the aroma characteristics of cigarettes when smoking, enrich and enhance the smoking experience, and at the same time, due to the special effect of Dendrobium nobile, it can also reduce the Cigarette hazards. Therefore, this application has a certain application value in the industry as a new type of Dendrobium nobile explosive beads that highlights the fragrance of cigarettes "Dendrobium nobile", improves the quality of smoking, and reduces the harm of cigarettes.

It should be emphasized that the above-mentioned puffing bead formula is designed for the improvement of conventional formula cigarettes, and it also has good application effect when applied to slim cigarettes. The amount of addition is properly adjusted, and will not be described in detail here.

Claims (6)

1. a kind of cigarette quick-fried pearl HERBA DENDROBII essence, it is characterised in that be calculated in mass percent, composed of the following components：

10.0 ~ 15.0% golden hairpin dendrobium extract,

1.0 ~ 2.0% nopinene,

0.3 ~ 0.6% linalool,

0.5 ~ 1.0% gaultherolin,

0.2 ~ 0.5% laurene,

1.0 ~ 2.0% myrrh oils,

78.9 ~ 87.0% Glycerin, mixed triester with caprylic acid capric acid；

The golden hairpin dendrobium extract is the ethanol extract of HERBA DENDROBII.

2. cigarette quick-fried pearl HERBA DENDROBII essence as claimed in claim 1, it is characterised in that 12% golden hairpin dendrobium extract, 1.5% nopinene, 0.4% linalool, 0.7% gaultherolin, 0.35% laurene, 1.5% myrrh oil and 83.55% Glycerin, mixed triester with caprylic acid capric acid.

3. the quick-fried pearl of cigarette described in claim 1 is utilized with the quick-fried pearl of HERBA DENDROBII cigarette prepared by HERBA DENDROBII essence, its feature It is, a diameter of 2.0 ~ 4.0mm of quick-fried pearl that essence content is 20 ~ 25 μ L/ in quick-fried pearl.

4. the quick-fried pearl of HERBA DENDROBII cigarette as claimed in claim 3, it is characterised in that the quick-fried a diameter of 3.65mm of pearl, weight are 23mg/ Essence content is 23 μ L/ in grain, quick-fried pearl.

5. application of the quick-fried pearl of HERBA DENDROBII cigarette in cigarette described in claim 3, it is characterised in that make an addition to the quick-fried pearl of cigarette In filter stick.

6. application of the quick-fried pearl of HERBA DENDROBII cigarette as claimed in claim 5 in cigarette, it is characterised in that the quick-fried pearl of cigarette is located at filter In the middle part of rod, a quick-fried pearl is added in every cigarette filter rod.