CN110433521A - A kind of KL540 crystallization apparatus - Google Patents
A kind of KL540 crystallization apparatus Download PDFInfo
- Publication number
- CN110433521A CN110433521A CN201910783363.XA CN201910783363A CN110433521A CN 110433521 A CN110433521 A CN 110433521A CN 201910783363 A CN201910783363 A CN 201910783363A CN 110433521 A CN110433521 A CN 110433521A
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- CN
- China
- Prior art keywords
- autoclave body
- stirring rod
- periphery
- stirring
- motor
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/85—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with two or more stirrers on separate shafts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/92—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with helices or screws
- B01F27/922—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with helices or screws with two or more helices, e.g. with intermeshing helices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D2009/0086—Processes or apparatus therefor
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The invention discloses a kind of KL540 crystallization apparatus, including rack and autoclave body, the autoclave body is fixed on the rack, the autoclave body top is provided with feed pipe, the autoclave body bottom end is provided with discharge nozzle, valve is mounted on the feed pipe and discharge nozzle, the interior of the autoclave body offers cooling chamber, input pipe and efferent duct are connected on the cooling chamber, the input pipe and efferent duct all extend to outside autoclave body, the autoclave body inner tip is rotatably equipped with the first stirring rod, the periphery of first stirring rod is equipped with several equally distributed first stirring sheets, the autoclave body top is equipped with first motor, the present invention passes through the first auxiliary rabbling mechanism of setting and the second auxiliary rabbling mechanism, material can adequately be stirred, greatly reduce stirring dead angle, material in crystallization kettle is heated evenly, crystallization effect is good, it mentions High crystalline rate.
Description
Technical field
The present invention relates to technical field of pesticide, specially a kind of KL540 crystallization apparatus.
Background technique
Pesticide refers to agriculturally for preventing and treating the chemical agent of pest and disease damage and coordinate plant growth.It is widely used in Agriculture, forestry And Animal Husbandry
Industry production, environment and domestic hygiene remove the evil epidemic prevention, industrial goods it is mould proof with it is mothproof etc..There are many pesticide species, can mainly divide by purposes
For insecticide, acaricide, rat poison, nematicide, invertebrate poison, fungicide, herbicide, plant growth regulator etc..
KL540 is that one of pesticide producing process intermediate is crystallized in the production process of KL540, but current
The problems such as KL540 crystallization kettle is low there are production efficiency.
Summary of the invention
The purpose of the present invention is to provide a kind of KL540 crystallization apparatus, to solve the problems mentioned in the above background technology.
To achieve the above object, the invention provides the following technical scheme:
A kind of KL540 crystallization apparatus, including rack and autoclave body, the autoclave body are fixed on the rack, and the autoclave body top is set
It is equipped with feed pipe, the autoclave body bottom end is provided with discharge nozzle, and valve, the autoclave body are mounted on the feed pipe and discharge nozzle
Interior offer cooling chamber, input pipe and efferent duct are connected on the cooling chamber, the input pipe and efferent duct are equal
It extends to outside autoclave body, the autoclave body inner tip is rotatably equipped with the first stirring rod, the periphery installation of first stirring rod
There are several equally distributed first stirring sheets, the autoclave body top is equipped with first motor, and the top of first stirring rod is passed through
It wears autoclave body roof to be connected with the output end of first motor, the periphery of first stirring rod is surrounded with several first auxiliary stirrings
Mechanism, the autoclave body inner bottom are provided with several second auxiliary rabbling mechanisms.
Preferably, the first auxiliary rabbling mechanism includes the second stirring rod, is provided on the inner sidewall of the autoclave body solid
Determine block, second stirring rod is rotatably installed in fixed block top, and the top of second stirring rod is rotatably connected in autoclave body
Portion top, second stirring rod periphery are equipped with several equally distributed second stirring sheets, the periphery of second stirring rod
Fixing sleeve is equipped with driven gear, and first stirring rod periphery fixing sleeve is equipped with driving gear, the driven gear and driving tooth
Wheel engagement connection.
Preferably, first stirring sheet and the arrangement alternating with each other of the second stirring sheet.
Preferably, the second auxiliary rabbling mechanism includes third stirring rod, is provided with mounting plate below the autoclave body, institute
It states mounting plate top and the second motor is installed, the output end of autoclave body bottom wall and the second motor is run through in the bottom end of the third stirring rod
It is connected, the periphery that the third stirring rod is located at autoclave body interior section is equipped with spiral helicine blade.
Preferably, third stirring rod periphery is disposed with the first stop collar and the second stop collar, institute from top to bottom
It states the first stop collar to be located inside autoclave body, second stop collar is located at below autoclave body.
Preferably, the mounting plate bottom end contact is provided with cam, and the cam is fixedly mounted on the output of third motor
End, the third motor are fixedly mounted on the rack.
Preferably, the periphery of the third motor is provided with the guide rod of several bilateral symmetry distributions, and the guide rod is solid
It is fixed that the top of the guide rod extends to above mounting plate through mounting plate on the rack, the installation plate surface offer and
The corresponding through-hole of guide rod, is connected with buffer spring between the mounting plate bottom end and rack, the buffer spring is sleeved on
Guide rod periphery.
Preferably, the outer side wall surface of the autoclave body is covered with thermal insulation layer.
Compared with prior art, the beneficial effects of the present invention are: driving gear can turn while the rotation of the first stirring rod
It is dynamic, and driving gear engages connection with driven gear, therefore will drive driven gear, i.e. the second stirring rod rotation, to drive
Second stirring sheet is stirred the unlapped region of the first stirring sheet；In crystallization process, pass through third motor driven cam
Rotation, driving third stirring rod does periodic elevating movement, while the second motor driven third stirring rod rotates, spiral helicine
Blade can play the effect for promoting material to convey upwards, to constantly dig the material of bottom in autoclave body upwards, make bottom
The material of layer can be also cooled, and avoid the problem that the material for being deposited in bottom is difficult to crystallize；In mounting plate lifting, guiding
Bar can play the role of limition orientation, guarantee that mounting plate moves in the vertical direction, buffer spring promotes movement more steady；Every
Thermosphere plays the role of obstructing inside and outside heat, and ambient temperature is avoided to have an impact crystallization process.The present invention passes through setting first
Rabbling mechanism and the second auxiliary rabbling mechanism are assisted, material can adequately be stirred, stirring dead angle, crystallization are greatly reduced
Material in kettle is heated evenly, and crystallization effect is good, improves crystalline rate.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of KL540 crystallization apparatus；
Fig. 2 is a kind of structural schematic diagram of autoclave body in KL540 crystallization apparatus；
Fig. 3 is a kind of structural schematic diagram of the second auxiliary rabbling mechanism in KL540 crystallization apparatus.
In figure: 1- rack, 2- autoclave body, 3- feed pipe, 4- discharge nozzle, 5- valve, 6- cooling chamber, 7- input pipe, 8- output
Pipe, the first stirring rod of 9-, 10- first motor, the first stirring sheet of 11-, 12- first assist rabbling mechanism, the auxiliary stirring of 13- second
Mechanism, 14- fixed block, the second stirring rod of 15-, the second stirring sheet of 16-, 17- driven gear, 18- driving gear, 19- third are stirred
Mix bar, 20- blade, the second motor of 21-, the first stop collar of 22-, the second stop collar of 23-, 24- mounting plate, 25- third motor,
26- cam, 27- guide rod, 28- buffer spring, 29- thermal insulation layer.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Fig. 1~3 are please referred to, the present invention provides a kind of technical solution: a kind of KL540 crystallization apparatus, including rack 1 and autoclave body
2, the autoclave body 2 is fixed in rack 1, and 2 top of autoclave body is provided with feed pipe 3, and 2 bottom end of autoclave body is provided with discharge nozzle
4, valve 5 is mounted on the feed pipe 3 and discharge nozzle 4, and the interior of the autoclave body 2 offers cooling chamber 6, described cold
But input pipe 7 and efferent duct 8 are connected on chamber 6, the input pipe 7 and efferent duct 8 all extend to outside autoclave body 2, the autoclave body 2
Inner tip is rotatably equipped with the first stirring rod 9, and the periphery of first stirring rod 9 is equipped with several equally distributed first and stirs
Piece 11 is mixed, 2 top of autoclave body is equipped with first motor 10, and 2 roof of autoclave body and first are run through in the top of first stirring rod 9
The output end of motor 10 is connected, and the periphery of first stirring rod 9 is surrounded with several first auxiliary rabbling mechanisms 12, the kettle
2 inner bottom of body is provided with several second auxiliary rabbling mechanisms 13 and leads in use, material is put into autoclave body 2 from feed pipe 3
It crosses input pipe 7 and efferent duct 8 and is recycled into cooling chamber 6 and be passed through coolant, while first motor 10 drives the rotation of the first stirring rod 9
Turn, the first auxiliary rabbling mechanism 12 of cooperation and the second auxiliary rabbling mechanism 13 are stirred material, promote material heated equal
It is even, to accelerate the crystallization process of material.
The first auxiliary rabbling mechanism 12 includes the second stirring rod 15, is provided with fixation on the inner sidewall of the autoclave body 2
Block 14, second stirring rod 15 are rotatably installed in 14 top of fixed block, and the top of second stirring rod 15 is rotatably connected on
2 inner tip of autoclave body, 15 periphery of the second stirring rod are equipped with several equally distributed second stirring sheets 16, and described second stirs
The periphery fixing sleeve of bar 15 is mixed equipped with driven gear 17, the 9 periphery fixing sleeve of the first stirring rod is equipped with driving gear 18, described
Driven gear 17 engages connection with driving gear 18, and while the rotation of the first stirring rod 9, driving gear 18 be can rotate, and lead
Moving gear 18 engages connection with driven gear 17, therefore will drive driven gear 17, i.e. the second stirring rod 15 rotation, to drive
Second stirring sheet 16 is stirred the unlapped region of the first stirring sheet 9.
First stirring sheet 9 and the arrangement alternating with each other of the second stirring sheet 16.
The second auxiliary rabbling mechanism 13 includes third stirring rod 19, is provided with mounting plate 24, institute below the autoclave body 2
It states 24 top of mounting plate and the second motor 21 is installed, 2 bottom wall of autoclave body and the second motor are run through in the bottom end of the third stirring rod 19
21 output end is connected, and the periphery that the third stirring rod 19 is located at 2 interior section of autoclave body is equipped with spiral helicine blade 20.
19 periphery of third stirring rod is disposed with the first stop collar 22 and the second stop collar 23 from top to bottom, described
First stop collar 22 is located inside autoclave body 2, and second stop collar 23 is located at 2 lower section of autoclave body, the first stop collar 22 and the second limit
Position ring 23 plays position-limiting action to the lifting of third stirring rod 19.
24 bottom end of the mounting plate contact is provided with cam 26, and the cam 26 is fixedly mounted on the output of third motor 25
End, the third motor 25 is fixedly mounted in rack 1, in crystallization process, drives cam 26 to rotate by third motor 25,
Driving third stirring rod 19 does periodic elevating movement, while the second motor 21 driving third stirring rod 19 rotates, helical form
Blade 20 can play the effect for promoting material to convey upwards, so that constantly the material of bottom in autoclave body 2 be dug upwards,
Making the material of bottom can also be cooled, and avoid the problem that the material for being deposited in bottom is difficult to crystallize.
The periphery of the third motor 25 is provided with the guide rod 27 of several bilateral symmetry distributions, and the guide rod 27 is fixed
In rack 1, the top of the guide rod 27 extends to 24 top of mounting plate through mounting plate 24, and 24 surface of mounting plate is opened
Equipped with through-hole corresponding with guide rod 27, buffer spring 28 is connected between 24 bottom end of mounting plate and rack 1, it is described slow
It rushes spring 28 and is sleeved on 27 periphery of guide rod, when mounting plate 24 is gone up and down, guide rod 27 can play the role of limition orientation, guarantee
Mounting plate 24 moves in the vertical direction, and buffer spring 28 promotes movement more steady.
The outer side wall surface of the autoclave body 2 is covered with thermal insulation layer 29, and thermal insulation layer 29 plays the role of obstructing inside and outside heat, keep away
Exempt from ambient temperature to have an impact crystallization process.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (8)
1. a kind of KL540 crystallization apparatus, including rack (1) and autoclave body (2), it is characterised in that: the autoclave body (2) is fixed on rack
(1) on, autoclave body (2) top is provided with feed pipe (3), and autoclave body (2) bottom end is provided with discharge nozzle (4), the charging
It is mounted on valve (5) on pipe (3) and discharge nozzle (4), the interior of the autoclave body (2) offers cooling chamber (6), described cold
But input pipe (7) and efferent duct (8) are connected on chamber (6), the input pipe (7) and efferent duct (8) all extend to autoclave body (2) outside
Portion, autoclave body (2) inner tip are rotatably equipped with the first stirring rod (9), first stirring rod (9) if periphery be equipped with
Equally distributed first stirring sheet (11) is done, autoclave body (2) top is equipped with first motor (10), first stirring rod
(9) top is connected through autoclave body (2) roof with the output end of first motor (10), the periphery of first stirring rod (9)
Several first auxiliary rabbling mechanism (12) are surrounded with, autoclave body (2) inner bottom is provided with several second auxiliary rabbling mechanisms
(13)。
2. a kind of KL540 crystallization apparatus according to claim 1, it is characterised in that: the first auxiliary rabbling mechanism
It (12) include the second stirring rod (15) being provided with fixed block (14) on the inner sidewall of the autoclave body (2), second stirring rod
(15) it is rotatably installed in fixed block (14) top, the top of second stirring rod (15) is rotatably connected on top inside autoclave body (2)
End, the second stirring rod (15) periphery is equipped with several equally distributed second stirring sheets (16), second stirring rod
(15) periphery fixing sleeve is equipped with driven gear (17), and the first stirring rod (9) periphery fixing sleeve is equipped with driving gear (18),
The driven gear (17) engages connection with driving gear (18).
3. a kind of KL540 crystallization apparatus according to claim 2, it is characterised in that: first stirring sheet (9) and second
Stirring sheet (16) arrangement alternating with each other.
4. a kind of KL540 crystallization apparatus according to claim 1, it is characterised in that: the second auxiliary rabbling mechanism
(13) include third stirring rod (19), be provided with mounting plate (24) below the autoclave body (2), mounting plate (24) the top installation
Have the second motor (21), the output end of autoclave body (2) bottom wall and the second motor (21) is run through in the bottom end of the third stirring rod (19)
It is connected, the periphery that the third stirring rod (19) is located at autoclave body (2) interior section is equipped with spiral helicine blade (20).
5. a kind of KL540 crystallization apparatus according to claim 4, it is characterised in that: third stirring rod (19) periphery
It is disposed with the first stop collar (22) and the second stop collar (23) from top to bottom, first stop collar (22) is located at autoclave body
(2) internal, second stop collar (23) is located at below autoclave body (2).
6. a kind of KL540 crystallization apparatus according to claim 5, it is characterised in that: mounting plate (24) the bottom end contact
It is provided with cam (26), the cam (26) is fixedly mounted on the output end of third motor (25), and the third motor (25) is solid
Dingan County is on rack (1).
7. a kind of KL540 crystallization apparatus according to claim 6, it is characterised in that: the periphery of the third motor (25)
It is provided with the guide rod (27) of several bilateral symmetry distributions, the guide rod (27) is fixed on rack (1), the guide rod
(27) top extends to above mounting plate (24) through mounting plate (24), and mounting plate (24) surface offers and guide rod
(27) corresponding through-hole is connected with buffer spring (28), the buffering elastic between mounting plate (24) bottom end and rack (1)
Spring (28) is sleeved on guide rod (27) periphery.
8. a kind of KL540 crystallization apparatus according to claim 1, it is characterised in that: the outer side wall surface of the autoclave body (2)
It is covered with thermal insulation layer (29).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910783363.XA CN110433521A (en) | 2019-08-23 | 2019-08-23 | A kind of KL540 crystallization apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910783363.XA CN110433521A (en) | 2019-08-23 | 2019-08-23 | A kind of KL540 crystallization apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110433521A true CN110433521A (en) | 2019-11-12 |
Family
ID=68437336
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910783363.XA Pending CN110433521A (en) | 2019-08-23 | 2019-08-23 | A kind of KL540 crystallization apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110433521A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DK165279B (en) * | 1983-09-30 | 1992-11-02 | Eridania | CRYSTAL CULTIVATION PLANT |
| CN206276059U (en) * | 2016-12-21 | 2017-06-27 | 宜昌凯翔化工有限公司 | For the crystallization kettle in phosphorous acid production system |
| CN107584663A (en) * | 2017-09-25 | 2018-01-16 | 郑州天舜电子技术有限公司 | It is a kind of with the mixed mud agitating device moved up and down |
-
2019
- 2019-08-23 CN CN201910783363.XA patent/CN110433521A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DK165279B (en) * | 1983-09-30 | 1992-11-02 | Eridania | CRYSTAL CULTIVATION PLANT |
| CN206276059U (en) * | 2016-12-21 | 2017-06-27 | 宜昌凯翔化工有限公司 | For the crystallization kettle in phosphorous acid production system |
| CN107584663A (en) * | 2017-09-25 | 2018-01-16 | 郑州天舜电子技术有限公司 | It is a kind of with the mixed mud agitating device moved up and down |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20191112 |
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| RJ01 | Rejection of invention patent application after publication |