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All Journal Jambi Medical Journal : Jurnal Kedokteran dan Kesehatan The Journal of Pure and Applied Chemistry Research Jurnal Agroekoteknologi CHEMPUBLISH JOURNAL JOURNAL ONLINE OF PHYSICS Jurnal Teknologi Laboratorium Chimica et Natura Acta Indonesian Food Science and TechnologyJournal Pharmacology and Clinical Pharmacy Research PengabdianMu: Jurnal Ilmiah Pengabdian kepada Masyarakat Jurnal Ilmiah Ibnu Sina (JIIS): Ilmu Farmasi dan Kesehatan International Journal of Hydrological and Environmental for Sustainability Makara Journal of Science Jurnal Pengabdian Pada Masyarakat Molekul: Jurnal Ilmiah Kimia Journal of The Indonesian Society of Integrated Chemistry
Madyawati Latief
Prodi Kimia Fakultas Sains dan Teknologi Universitas Jambi
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KARAKTERISASI SENYAWA DARI FRAKSI AKTIF ANTIBAKTERI DAUN Garcinia celebica linn (Kandis) Latief, Madyawati
CHEMPUBLISH JOURNAL Vol 1, No 1 (2015)
Publisher : Program Studi Kimia FST Universitas Jambi

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Abstract

Telah diisolasi 3-oxofridelin dari fraksi etil asetat yang merupakan fraksi aktif antibakteri dari daun Garcinia celebica (Guttiferae).  Struktur molekul senyawa ditetapkan berdasarkan data spektroskopi IR, 1H dan 13C NMR serta perbandingan data tersebut dengan data sejenis yang telah dilaporkan.  Aktivitas antibakteri dari senyawa isolasi juga diuji dengan menggunakan bakteri  Escherichia coli, Shigella dysentriae, Bacillus subtilis dan Staphylococcus aureus. Kata Kunci : Garcinia celebica, Guttiferae, fridelin, antibakteri
ADSORPSI MERKURI (II) MENGGUNAKAN ZEOLIT DARI FLY ASH BATUBARA Mandalahi, Helmina; Muis, Lince; Latief, Madyawati
CHEMPUBLISH JOURNAL Vol 1, No 1 (2015)
Publisher : Program Studi Kimia FST Universitas Jambi

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Abstract

Pembuatan zeolit dari abu terbang batubara dan diaplikasikan sebagai adsorben untuk penyerapan merkuri (II) telah dilakukan. Zeolit dibuat dari abu terbang batubara dengan menggunakan metode solid state dan dikarakterisasi dengan menggunakan XRD dan FTIR. Adsorpsi merkuri (II) menggunakan zeolit dilakukan dengan variasi suhu furnace dan waktu kontak. Hasil karakterisasi dengan XRD memperlihatkan bahwa tipe zeolit adalah Faujasit dengan puncak pada 6,0688°; 15,3959°; dan 23,2781°. Karakterisasi dengan FTIR menunjukkan bahwa abu terbang dapat digunakan untuk pembuatan zeolit pada 462,92 cm-1. Adsorpsi merkuri (II) menggunakan zeolit menunjukkan bahwa suhu optimum furnace adalah 7500C dan waktu kontak optimum pada 150 menit. Data isoterm digambarkan dengan Persamaan Langmuir dan kinetika adsorpsi mengikuti model kinetika orde dua pseudo dengan konstanta laju adsorpsi adalah 0,818 (g/mg min). Kata kunci: abu terbang, batubara, zeolit, adsorpsi, merkuri (II)  
Aktivitas Anti-Inflamasi Senyawa Squale dari Ekstrak Metanol Abroma augusta L pada Mus musculus Latief, Madyawati; Muhaimin, Muhaimin; Amanda, Hilda; Prahandika, Graha; Tarigan, Indra Lasmana
Jurnal Teknologi Laboratorium Vol 9 No 2 (2020): 2020 (2)
Publisher : POLTEKKES KEMENKES YOGYAKARTA

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.29238/teknolabjournal.v9i2.228

Abstract

Abroma augusta L plant traditionally was used to treat swellings, cuts, sores, and bruises. In the province of Jambi, A. augusta is used in folk medicine to treat wounds. This study aims to isolate the steroid compound from the root of A. augusta L and determine its anti-inflammatory activities. Extraction and fractionation have been done with graded maceration using solvents with different polarities, which are n-hexane, ethyl acetate, and methanol. The separation was performed by column chromatography, followed by preparative thin-layer chromatography. The characterization of the isolate was carried out using UV-Vis spectrophotometry and infrared spectrophotometry, GC-MS. The anti-inflammatory activities of methanol extract and isolate of A. augusta was performed in this study was designed to evaluate the dose-response relationship of the anti-inflammatory activity in rat models of chronic inflammation chromatography to obtain isolate 2.1.1 that characterize and showed maximum absorbance at 265. The result of IR showed the presence of functional groups, -C=C-H, -C=H, -CH, CH3, CH2, and –CO belongs to the steroid compound. The results of the GC-MS show that isolates contain squalene compounds with a value of m/z 410, Isolate and crude extract showed an anti-inflammatory activity that almost approached the positive control of sodium 4-chlorophenolate. It could be concluded that isolate and extract provide good anti-inflammatory activity, that promise for new drug candidate squalene-based A. augusta.
Isolation and Characterization of Ethyl Acetate Fraction from Abroma augusta L as an Anti-Inflammatory Agent Latief, Madyawati; Tarigan, Indra Lasmana; Muhaimin, Muhaimin; Amanda, Hilda; Yulianti, Nike Desvi
Makara Journal of Science Vol. 25, No. 2
Publisher : UI Scholars Hub

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Abstract

Abroma augusta is a bush plant that lives on the edge of the river. This plant is commonly used as an anti-inflammatory drug for joints and broken bones. It contains several secondary metabolites, such as alkaloids, triterpenoids, steroids, and flavonoids, which exhibit anti-inflammatory activity. UV-visible (UV-Vis) spectrophotometry of isolate 1.3 indicated absorption at a maximum wavelength of 282 nm. The wavelength suggested that the electron transition π–π* is the absorption of UV spectra typical for triterpenoid compounds that have chromophores in the form of non-conjugated double bonds. FT-IR spectrophotometer characterization data from isolate 1.3 revealed the presence of triterpenoid compounds having carboxyl groups C-O (ester), C-(CH3)2 (gem-dimethyl), carbonyl C = O esters, and C-H (alkyl). Analyses of UV-Vis, FT-IR, GC-MS, 1H-NMR, and 13C-NMR spectra showed that the compound obtained was the triterpenoid β-amyrin. Activity test demonstrated that isolate 1.3 with a 10 mg dose showed stronger anti-inflammatory activity than the positive control of sodium diclofenac.
UJI IRITASI DAN EFEKTIFITAS SPRAY HANDSINITIZER EKSTRAK ETANOL DAUN JERUJU (Achantus Ilicifolious) SEBAGAI ANTIBAKTERI Lestari, Uce; Suci, Ulan; Latief, Madyawati
JAMBI MEDICAL JOURNAL "Jurnal Kedokteran dan Kesehatan" Vol. 9 No. 1 (2021): Special Issues: JAMHESIC 2020
Publisher : FAKULTAS KEDOKTERAN DAN ILMU KESEHATAN UNIVERSITAS JAMBI

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (197.387 KB) | DOI: 10.22437/jmj.v9i0001.12891

Abstract

ABSTRAKPendahuluan: Acanthus ilicifolius.L merupakan tanaman mangrove yang banyak dimanfaatkan sebagaitanaman obat. Kandungan flavonoid dan fenolik yang terkandung didalamnya dapat digunakan sebagaiantibakteri. Setiap hari tangan kita menyentuh barang yang penuh dengan bakteri, salah satunya Staphylococcusaureus yang dapat mengakibatkan terjadinya infeksi kulit. Untuk mencegah penyebaran bakteri tersebut makadibuatlah spray hand sanitizer ekstrak etanol daun jeruju dengan konsentrasi 6%.Metode: Penelitian ini bertujuan untuk memformulasi sediaan farmasi yang memiliki aktivitas daya hambatterhadap bakteri penyebab infeksi kulit. Spray Hand sanitizer ini dipilih karena lebih praktis, tidak lengket dancepat menyebar pada kulit. Tahapan penelitian terdiri dari uji iritasi, hedonik dan aktivitas antibakteri terhadapStaphylococcus aureus sebelum dan sesudah penggunaan spray hand sanitizer. Menggunakan 10 orangpanellist rentang usia 25 s/d 30 tahun kategori kulit tangan normal.Hasil: Hasil menyatakan bahwa tidak ada satupun panellist yang mengalami iritasi, gatal, bengkak ataupunkemerahan pada kulit, 80% menyukai warna, aroma dan bau dari spray hand sanitizer, nilai daya hambatminimum terhadap bakteri Staphylococcus aureus sebesar 5,66 mm dan jumlah koloni sebelum penggunakansebanyak 88 koloni sedangkan setelah penggunaan sebanyak 10 koloni.Kesimpulan: Dapat disimpulkan bahwa spray hand sanitizer ekstrak etanol daun jeruju 6% aman padapenggunaannya serta memiliki kemampuan untuk menghambat bakteri Staphylococcus aureus penyebab infeksikulit.Kata kunci: Jeruju, spray handsinitizer, Staphylococcus Aureus
X-Ray Fluorescence Monitoring Metal Content and Nutrient Elements for Predicting Soil Fertility Parameters Based on pH in Ultisol Soil Samsidar, Samsidar; Maison, Maison; Ermadani, Ermadani; Latief, Madyawati; Pebralia, Jesi; Riany, Hesti; Amanda, Dwi Rahma; Maulana, Lucky Zaehir
International Journal of Hydrological and Environmental for Sustainability Vol 2, No 3 (2023): International Journal of Hydrological and Environmental for Sustainability
Publisher : CV FOUNDAE

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.58524/ijhes.v2i3.290

Abstract

Soil fertility parameters, including macronutrients, micronutrients, and metal content, are very important for optimizing agricultural and plantation land management. Ultisol is a type of soil that is commonly used as a planting medium for oil palm plantations, rubber, and various types of vegetables. Continuous land use causes variations in nutrient and metal content. This change is also caused by the fertilization process and the characteristics of the plants grown in the area. In this study, an analysis of soil fertility parameters (macronutrients, micronutrients, and metal content) was analyzed using X-Ray Fluorescence (XRF) on Ultisol soil taken from Muara Jambi Regency, Indonesia. This analysis was conducted across land-use areas (Palm, Rubber, Vegetables, and Forest). Subsequently, the obtained measurements were used to model correlations with soil pH values to predict soil fertility parameters. The quantitative results showed that the metal content values were reasonably consistent across all locations regarding metal types and their percentage concentrations. However, locations 1 (T1) and 2 (T2) have higher aluminum (Al) content than locations 3 and 4 and lower magnesium (Mg) content. The modeling, when correlated with pH values, indicated that metal elements correlated 0.938, macronutrients 0.934, and micronutrients 0.767. From these correlations, it can be qualitatively inferred that there is a strong relationship between pH and the presence of metal content, macronutrients, and micronutrients. In the future, this can serve as a model for estimating the presence of soil fertility parameters.
Encapsulation of Jeruju Leaves Ethanol Extract (Acanthus ilicifolius L.) and It's Antiinflammatory Activities Against Carrageenan-Induced Mice Tarigan, Indra Lasmana; Kharisma, Tiara; Bemis, Restina; Sutrisno, Sutrisno; Latief, Madyawati
Molekul Vol 18 No 3 (2023)
Publisher : Universitas Jenderal Soedirman

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.20884/1.jm.2023.18.3.8820

Abstract

Jeruju (Acanthus ilicifolius) leaves ethanol extract contains flavonoids that function as an antiinflammatory source. So it is necessary to research to increase the utilization of ethanol extract of Acanthus ilicifolius leaves (A. ilicifolius L.) in encapsulations to increase the stability of antiinflammatory chemical compounds. Concentrated dyestuff extracts are often unstable, so they need to be converted into solid form, and one technique that can be done is encapsulation. Encapsulation aims to protect sensitive components of the material and reduce the degradation of active compounds in the material. The research method begins with preparing samples to be extracted with ethanol solvent, extract phytochemical screening tests, validation determination tests for the analysis method of ethanol extract levels of jeruju leaves, encapsulated formulations, encapsulated physics and chemical properties test and anti-inflammatory tests. In this research, the secondary metabolite compounds contained in the ethanol extract of Jeruju Leaves were flavonoids, phenolics, steroids, and saponins. The determination of the validation of the analysis method of ethanol extract levels of jeruju leaves was obtained by measurement using a UV-vis spectrophotometer and obtained extract levels of 1367,831 mg/g. This research used maltodextrin coating material for encapsulation formulation because it has low viscosity in many ratios, high solubility, has no taste. The freeze-dryer method was used in this study because it produces better drying quality than other drying methods. The physical property test was carried out by analysis using FTIR and SEM while the chemical properties of encapsulation obtained the highest yield proportion of 58.81%, and the highest solubility proportion of 98.76%. Anti-inflammatory testing is carried out using male mice as test animals. Anti-inflammatory testing in mice based on the Rat hind paw oedema method. The average percent inhibition of each dose administered is calculated based on the data results. The high average percent inhibition obtained for Diclofenac Na is 80%. In the research Encapsule 1:12, the 120 mg/KgBW dose had a significant percentage of inhibition of 75.55%, with Na Diclofenac dose of 10 mg/KgBW being 80%.
Nanoemulsion Formulation as a Drug Delivery System for Coleus atropurpureus Bioactive Compounds Oktavioni, Marsella; Natasya, Dian; Yusnaidar, Yusnaidar; Latief, Madyawati; Tarigan, Indra L.
Pharmacology and Clinical Pharmacy Research Vol 9, No 1 (2024)
Publisher : Universitas Padjadjaran, Indonesia

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15416/pcpr.v9i1.50371

Abstract

Miana plant (Coleus) is a plant with compound flowers. Miana leaves have various bioactive compounds widely used to treat diseases such as fever, cold, cough, headaches, asthma, constipation, and skin diseases. Based on phytochemical screening of Coleus atropurpureus Benth. Several bioactive compounds are produced, such as sterols, terpenoids, alkaloids, phenols, flavonoids, glycosides, lactones, catechols, and tannins. Miana leaf extract has been tested for antioxidants using the DPPH method, and the IC50 value obtained from the antioxidant test results is 3.80 ppm and is categorized as a powerful antioxidant. There were four formulations of miana leaf extract nanoemulsion. Based on the characterization on the Miana leaf extract nanoemulsion preparation, formulations with good results were obtained in F1 and F3 with precise results and high transmittance values. In testing the miana leaf extract nanoemulsion, an organoleptic test was carried out on each formulation. It was found that all formulations had a distinctive smell of miana leaves, and no phase separation occurred, with the clarity of F1 and F3 classified as straightforward but F2 and F4 not clear, and the resulting color increased from F1 -F4. Meanwhile, for the physicochemical test, an O/W type nanoemulsion was produced, physically stable, with a particle size of F1 153.9 nm and F3 795.6 nm, with a zeta potential of F1 of 16.4 and F3 of -28.266.
Pertumbuhan Bibit Kopi Liberika Tungkal Komposit pada Aplikasi Pupuk Kandang Ayam Lizawati, Lizawati; Kartika, Elis; Latief, Madyawati; Tarigan, Indra Lasmana; Sutrisno, Sutrisno; Puspitasari, Ratih Dyah
Jurnal Agroekoteknologi Vol 16, No 1 (2024)
Publisher : Jurusan Agroekoteknologi Fakultas Pertanian Untirta

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.33512/jur.agroekotetek.v16i1.22467

Abstract

One of the efforts to increase the growth of Liberica coffee of Tungkal composite seedlings is through organic fertilization as considered inorganic fertilizers replacement. The purpose of this study was to look for the best dose of chicken manure for the growth of Liberica coffee of Tungkal composite seedlings. This study used a randomized block design with 4 replications with one factor, namely chicken manure consisting of 7 treatment levels, namely 0, 50, 100, 150, 200, 250 and 300 g of chicken manure/polybag. The variables observed were increase in seedling height, increase in stem diameter, increase in number of leaves, leaf area, crown dry weight, and root dry weight. The results showed that the application of chicken manure was able to increase the increase in seedling height, increase in stem diameter, increase in the number of leaves, and crown dry weight of liberica coffee seedlings, but was not able to increase leaf area and root dry weight. The recommended dose of chicken manure to increase the growth of liberica coffee seedlings was 211 g of chicken manure/polybag.
Production Process Technology of Lecithin from Crude Palm Oil on The Physico Chemical Properties of Halal Dark Chocolate produced Latief, Madyawati; Nizori, Addion; Rahmi, Silvi Leila; Nabila, Annisa Candra; Tarigan, Indra Lasmana; Huda, Nurul; Yusof, Yus Aniza
Indonesian Food Science and Technology Journal Vol. 6 No. 2 (2023): Volume 6. Number 2, July 2023 |IFSTJ|
Publisher : Department of Technology of Agricultural product (THP) Jambi University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.22437/ifstj.v6i2.29184

Abstract

This research was conducted to determine the effect of the addition of CPO (Crude Palm Oil) lecithin as an Emulsifier on the physicochemical and sensory characteristics of dark chocolate, and to determine the amount of lecithin addition as an appropriate Emulsifier to produce chocolate with the best physico-chemical and sensory characteristics. This study used a completely randomized design (CRD) method with a treatment level of 0%. 0.1%, 0.2%, 0.3%, 0.4% with 4 repetitions to obtain 20 experimental units. Parameters observed included color degee, antioxidant activity, fat blooming, stability level, color sensory test, taste, aroma, texture and overall acceptability. The data obtained were analyzed using ANOVA levels of 1% and 5%. If there is a significant effect on the treatment, it will be continued with the Duncan's Multiple Range Test (DNMRT) at the 5% level. The best concentration of adding lecithin to dark chocolate is 0.3% which contains 66.76% antioxidant activity, color degee L*28.58, a* 13.67, b* 22.67, hue 58.75, good stability (melting properties), able to prevent fat blooming, has good color very chocolatey (4.20), very distinctive aroma of chocolate (4.44), bitter taste (2.68), smooth texture (3.36) and the overall acceptance of the panelists really liked it (8.16).
Co-Authors -, Maison Addion Nizori Alfi Khatib, Alfi Alrizal, Alrizal Amanda, Dwi Rahma Amanda, Hilda Ardhica, Jammes Arum, Dewi Azizah, Regina Wan Bela, Anisa Budiyati Ichwan Bulan, Catherine Putri Delviani, Delviani Dewi, Tribuana Tungga Elis Kartika Ermadani Ermadani Faizar Farid Farah, Farah Fisesa, Anggun Tri Helmina Mandalahi, Helmina Hengky Irawan, Hengky Heriyanti Heriyanti, Heriyanti Husna, Naimul Indra Lasmana Tarigan Jamaludin Al-Anshori Kharisma, Tiara Lince Muis Lizawati Lizawati Lucky Zaehir Maulana Maharani, Viola Giary Rizkillah Masruri Masruri Melani, Fitria Muhaimin Muhaimin Nabila, Annisa Candra Natasya, Dian Nelson Nurjannah, Sofia Nurul Huda Oktavioni, Marsella Pebralia, Jesi Prabawa, Satria Prahandika, Graha Puspitasari, Ratih Dyah Putri Maya Sari Putri, Silvi Ayudiah Putri, Yunika Eka qurrota aini Ramadhan, Ilham Ifandi Raza'i, Tengku Said Resta, Ichy Lucya Restina Bemis, Restina Riany, Hesti Saharin, Siti Munirah Samsidar Samsidar Sari, Tika Shadrina, Putri Nur Silvi Leila Rahmi Sinurat, Julius Alvin Novensius Suci, Ulan Susanto, Nindita Clourisa Amaris Sutrisno, Sustrisno Sutrisno, Sutrisno Tarigan, Indra L. Uce Lestari Warni, Tri Yoza Fendriani Yulianti, Nike Desvi Yusnaidar, Yusnaidar Yusof, Yus Aniza