CN110918041B - A kind of micro-nano sol quick-mixing reaction bottle device and using method thereof - Google Patents
A kind of micro-nano sol quick-mixing reaction bottle device and using method thereof Download PDFInfo
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- CN110918041B CN110918041B CN201911221242.2A CN201911221242A CN110918041B CN 110918041 B CN110918041 B CN 110918041B CN 201911221242 A CN201911221242 A CN 201911221242A CN 110918041 B CN110918041 B CN 110918041B
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 37
- 238000000034 method Methods 0.000 title claims abstract description 11
- 239000007788 liquid Substances 0.000 claims abstract description 51
- 239000002243 precursor Substances 0.000 claims abstract description 17
- 238000005192 partition Methods 0.000 claims abstract description 15
- 238000007789 sealing Methods 0.000 claims description 10
- 239000003086 colorant Substances 0.000 claims description 2
- 230000001105 regulatory effect Effects 0.000 claims 1
- 238000002360 preparation method Methods 0.000 abstract description 19
- 239000002086 nanomaterial Substances 0.000 abstract description 9
- 239000000463 material Substances 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 3
- 238000005054 agglomeration Methods 0.000 abstract 1
- 230000002776 aggregation Effects 0.000 abstract 1
- 239000000047 product Substances 0.000 description 11
- 230000000844 anti-bacterial effect Effects 0.000 description 6
- 239000002994 raw material Substances 0.000 description 5
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 230000033228 biological regulation Effects 0.000 description 3
- 239000012295 chemical reaction liquid Substances 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 2
- 235000013547 stew Nutrition 0.000 description 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010364 biochemical engineering Methods 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000009713 electroplating Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 230000002147 killing effect Effects 0.000 description 1
- 244000000010 microbial pathogen Species 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 229910001961 silver nitrate Inorganic materials 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Details Of Rigid Or Semi-Rigid Containers (AREA)
Abstract
一种微纳米溶胶速配反应瓶体装置及其使用方法，其中微纳米溶胶速配反应瓶体装置包括瓶体，瓶体的内部设有两个隔板，每个隔板的上表面和每个隔板的底面分别与瓶体的内顶壁和瓶体的内底壁固定连接，瓶体通过两个隔板分为第一空腔、第二空腔和混合腔，两个隔板相互远离的一侧面均开设有通孔，瓶体的内部设有两个堵塞，每个堵塞的外表面均与每个通孔的内壁相接触，两个堵塞相互远离的一侧面均固定连接有调节杆，瓶体的外表面开设有相对的调节孔。使用时，通过拉动调节杆能够使前驱液和还原液流向混合腔，即时反应制备高活性、不团聚的微纳米材料，突破了微纳米溶胶材料制备中由设备、材料等带来的局限，实现了微纳米材料制备的终端化和快捷化。
A micro-nano sol fast-matching reaction bottle device and a method of using the same, wherein the micro-nano sol fast-matching reaction bottle device includes a bottle body, and two partitions are arranged inside the bottle body, the upper surface of each partition and each partition The bottom surface of the plate is respectively fixedly connected with the inner top wall of the bottle body and the inner bottom wall of the bottle body. One side is provided with through holes, and the inside of the bottle body is provided with two blockages, the outer surface of each blockage is in contact with the inner wall of each through hole, and one side of the two blockages away from each other is fixedly connected with an adjustment rod, The outer surface of the bottle body is provided with relative adjustment holes. When in use, by pulling the adjusting rod, the precursor liquid and reducing liquid can flow to the mixing chamber, and the micro-nano material with high activity and non-agglomeration can be prepared in an instant reaction, which breaks through the limitations brought by equipment and materials in the preparation of micro-nano sol materials. The terminalization and expedited preparation of micro-nano materials.
Description
Technical Field
The invention belongs to the technical field of biochemical engineering, relates to a chemical or biological reduction method preparation technology of metal micro-nano sol, and particularly relates to a micro-nano sol rapid-preparation reaction bottle device and a using method thereof.
Background
With the development of micro-nano technology, metal micro-nano materials play an increasingly greater role in human life, for example, a metal silver simple substance with a nano-scale particle size can have strong inhibition and killing effects on dozens of pathogenic microorganisms, and becomes a first material in the antibacterial field, and in addition, micro-nano silver has wide application in various fields such as electronics, catalysis, superconduction, electroplating, optical materials and the like.
The preparation of micro-nano sol generally belongs to the industrial link, people generally use finished products in daily use, still take antibacterial materials as examples, antibacterial medicines and medical instruments, antibacterial plastics and rubber products, antibacterial textiles and clothes, shoes and socks, antibacterial coatings, ceramics and glass, do not need users to carry out the preparation operation of micro-nano sol, but metal micro-nano materials are easy to oxidize and inactivate for a long time, and are easy to agglomerate and grow in the sol, and can also carry out continuous reaction or unpredictable chemical reaction due to the influence of external environment, so that no matter laboratories carry out research, or some special industrial application occasions, in order to obtain high-activity and controllable micro-nano materials, professional personnel are often required to prepare on site, and higher requirements are provided for personnel quality, equipment and materials.
Disclosure of Invention
In order to solve the problems in the prior art, the inventor researches and provides a micro-nano sol rapid-preparation reaction bottle device and a using method thereof, so that the limitation caused by equipment, materials and the like in the preparation of micro-nano sol materials is broken through, the terminating and rapid preparation of the micro-nano material preparation is realized, and the activity and controllability of the product in the instant use are improved.
The technical scheme adopted by the invention is as follows:
a micro-nano sol fast-matching reaction bottle body device comprises a bottle body, wherein two clapboards are arranged inside the bottle body, the upper surface of each clapboard and the bottom surface of each clapboard are fixedly connected with the inner top wall of the bottle body and the inner bottom wall of the bottle body respectively, the bottle body is divided into a first cavity, a second cavity and a mixing cavity through the two clapboards, one side surface of each clapboard, which is far away from the other, is provided with a through hole, the inside of the bottle body is provided with two plugs, the outer surface of each plug is contacted with the inner wall of each through hole, one side surface of each plug, which is far away from the other, is fixedly connected with an adjusting rod, the outer surface of the bottle body is provided with opposite adjusting holes, one end, which is far away from the other, of each adjusting rod penetrates through each adjusting hole and extends to one side, which is, every the inner circle of sealing washer all contacts with the surface of every regulation pole, the liquid outlet has been seted up to the upper surface of bottle, the fixed surface intercommunication of upper surface of bottle has the bottle neck, and the bottle neck is linked together with the liquid outlet.
Preferably, symmetrical liquid inlets are formed in the upper surface of the bottle body, and a sealing plug is clamped in each liquid inlet.
Preferably, the two ends of the adjusting rods, which are far away from each other, are fixedly connected with pull plates, and the pull plates are in a T shape.
Preferably, the outer surface of each adjusting rod is fixedly connected with symmetrical limiting plates, and the limiting plates are located between the two adjusting holes.
Preferably, the outer surface of the bottle mouth is provided with threads, a bottle cap is arranged above the bottle body, the inner wall of the bottle cap is provided with threads, and the inner wall of the bottle cap is in threaded connection with the outer surface of the bottle mouth.
Preferably, the symmetrical label is fixedly connected to the outer surface of the bottle body, and the label is positioned at the upper part of the bottle body.
Preferably, the front surface of the bottle body is provided with a mark, and the back surface of the mark is fixedly connected with the front surface of the bottle body.
Preferably, the whole body of the bottle body is a brown bottle, or one side of the bottle body is brown and the other side of the bottle body is other colors.
The using method of the micro-nano sol rapid-preparation reaction bottle body device is characterized by comprising the following steps of:
s1, pre-injecting a precursor solution into the first cavity and a reducing solution into the second cavity before use or before delivery;
s2, when the device is used, the adjusting rod is pulled to separate the plug from the through hole, so that the precursor liquid and the reducing liquid flow to the mixing cavity, and when the driving liquid and the reducing liquid flow to a certain amount, the adjusting rod is pushed to enable the plug to be in contact with the through hole, so that the precursor liquid and the reducing liquid are isolated;
s3, standing for 5-120min (can be matched with light and micro vibration to shake uniformly), and turning over the bottle body to enable the micro-nano sol to flow out through the liquid outlet and the bottle mouth for use.
In summary, due to the adoption of the technical scheme, the invention has the beneficial effects that:
according to the invention, the bottle body can be divided into the first cavity, the second cavity and the mixing cavity through the partition plate, so that the precursor solution and the reducing solution can be stored in different cavities of the bottle body, the aim of separately storing two reaction solutions is achieved, the micro-nano sol is prepared by rapid preparation before use, and the problem that the micro-nano material finished product is volatile and fails to activate or agglomerate and grow up after being stored for a long time is effectively solved.
According to the bottle body device, the plug can be separated from the through hole by pulling the adjusting rod, so that the precursor liquid and the reducing liquid flow to the mixing cavity, the precursor liquid and the reducing liquid can perform mixing reaction by taking the mixing cavity as a main space, mutual permeation of the two reaction liquids to respective containing spaces is reduced, possibility is provided for multiple use, the whole bottle body device is reasonable in structure, raw material information and use information can be checked through a striking label and a striking mark, and people can learn and use the bottle body device conveniently.
According to the industrial and market requirements, the micro-nano sol fast-matching reaction bottle device can be injected with raw materials by a manufacturer, so that the micro-nano sol fast-matching reaction bottle device can be used as a fast consumer product in a specific field, and the raw materials can also be injected by a user, so that the micro-nano sol fast-matching reaction bottle device can be simultaneously used as an intermediate container tool, meets the requirements of scientific research and the like, and has a great industrial application prospect.
Drawings
FIG. 1 is a sectional view showing a front view of a bottle apparatus according to the present invention;
FIG. 2 is a front view of the bottle apparatus of the present invention;
FIG. 3 is an enlarged view of the structure at A in FIG. 1 according to the present invention;
FIG. 4 is an enlarged view of the structure at B in FIG. 1 according to the present invention.
The labels in the figure are: 1. a bottle body; 2. a partition plate; 3. a first cavity; 4. a second cavity; 5. a mixing chamber; 6. a through hole; 7. blocking; 8. adjusting a rod; 9. an adjustment hole; 10. a seal ring; 11. a liquid outlet; 12. a bottle mouth; 13. a bottle cap; 14. a liquid inlet; 15. a sealing plug; 16. marking; 17. a label; 18. a bottle bottom; 19. pulling a plate; 20. and a limiting plate.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is described in further detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Referring to fig. 1-4, a micro-nano sol fast-matching reaction bottle device comprises a bottle body 1, two partition plates 2 are arranged inside the bottle body 1, the upper surface of each partition plate 2 and the bottom surface of each partition plate 2 are fixedly connected with the inner top wall of the bottle body 1 and the inner bottom wall of the bottle body 1 respectively, the bottle body 1 is divided into a first cavity 3, a second cavity 4 and a mixing cavity 5 by the two partition plates 2, through holes 6 are arranged on the side surfaces of the two partition plates 2 away from each other, two plugs 7 are arranged inside the bottle body 1, the outer surface of each plug 7 is contacted with the inner wall of each through hole 6, adjusting rods 8 are fixedly connected to the side surfaces of the two plugs 7 away from each other, opposite adjusting holes 9 are arranged on the outer surface of the bottle body 1, the ends of the two adjusting rods 8 away from each other penetrate through each adjusting hole 9 and extend to the side of the two adjusting holes 9 away from each, the inner circle of every sealing washer 10 all contacts with every surface of adjusting pole 8, symmetrical inlet 14 has been seted up to the upper surface of bottle 1, the equal joint in inside of every inlet 14 has sealing plug 15, liquid outlet 11 has been seted up to the upper surface of bottle 1, the last fixed surface intercommunication of bottle 1 has bottle neck 12, and bottle neck 12 is linked together with liquid outlet 11, the screw thread has been seted up to the surface of bottle neck 12, the top of bottle 1 is equipped with bottle lid 13, the screw thread has been seted up to the inner wall of bottle lid 13, the inner wall of bottle lid 13 and the surface threaded connection of bottle neck 12.
This embodiment is divided into first cavity 3, second cavity 4 and hybrid chamber 5 with bottle 1 through baffle 2 to can make forerunner's liquid and reduction liquid deposit in the different cavities of bottle 1, reached and separately deposited the purpose to two kinds of reaction liquid, just carry out the rapid-match before the use and prepare micro-nano sol, the effectual micro-nano material finished product of having solved is deposited the problem that the life became invalid or reunion grow up of losing a specified time.
Combine fig. 1 and fig. 4, two equal fixedly connected with arm-tie 19 of one end of adjusting pole 8 and keeping away from each other, and arm-tie 19 is the T shape, conveniently stimulates and adjusts pole 8, is convenient for adjust, and is further, the symmetrical limiting plate 20 of the equal fixedly connected with of surface of every regulation pole 8, and limiting plate 20 is located between two regulation holes 9, can restrict the position of adjusting pole 8, and it is troublesome to reduce unnecessary. The plug 7 can be separated from the through hole 6 by pulling the adjusting rod 8, so that the precursor liquid and the reducing liquid flow to the mixing chamber 5, the precursor liquid and the reducing liquid can perform mixing reaction by taking the mixing chamber 5 as a main space, and mutual permeation of the two reaction liquids to respective accommodating spaces is reduced.
Furthermore, the outer fixed surface of the bottle body 1 is connected with symmetrical labels 17, and the labels 17 are positioned on the upper portion of the bottle body 1, so that the liquid information in each cavity in the bottle body 1 can be conveniently known, the front of the bottle body 1 is provided with the mark 16, the back of the mark 16 is fixedly connected with the front of the bottle body 1, so that the information such as the use instruction can be checked, and the understanding is convenient.
As a brand-new micro-nano material preparation product, a user can conveniently know a new product through the eye-catching label 17 and the mark 16, the raw material information and the use information are checked, the learning and the use are fast, and the method is more effective than the method of printing important information on a specification.
Before the micro-nano sol fast-preparation reaction bottle device is used or before the micro-nano sol fast-preparation reaction bottle device leaves a factory, the sealing plug 15 is taken out from the liquid inlet 14, the precursor solution is pre-injected into the first cavity 3, the reducing solution is pre-injected into the second cavity 4, if the two solutions are injected from a manufacturer, the micro-nano sol fast-preparation reaction bottle device can be defined as a fast consumer product, and if the two solutions are injected from a user, the micro-nano sol fast-preparation reaction bottle device is actually used as an intermediate container tool at the same time, and the micro-nano sol fast-preparation reaction bottle device is set according to actual needs of industry and markets and is not particularly limited.
During the use, pulling adjust pole 8 makes jam 7 with through-hole 6 separation makes precursor liquid and reduction liquid flow to mixing chamber 5, when the driving liquid reaches a certain amount with reduction liquid, promote adjust pole 8 make jam 7 with through-hole 6 contacts, keeps apart precursor liquid and reduction liquid, according to the raw materials type, concentration, the nature of two kinds of reaction solution that inject different, stew 5-120min, just mix the back or stew in-process can cooperate light and slight vibration shake even, after the time, upset bottle 1 makes micro-nano sol flow out through liquid outlet 11 and bottleneck 12, uses.
As mentioned above, the precursor solution and the reducing solution can be mixed and reacted by taking the mixing chamber 5 as a main space, so that mutual permeation of the two reaction solutions into respective accommodating spaces is reduced, therefore, the reaction solution of the present invention can be used for multiple times, but the time interval is not easy to be too long, on one hand, the package seal is opened, air is easy to permeate, on the other hand, although the slight mutual permeation between the two reaction solutions can be ignored due to the concentration difference after permeation, the slight reaction product has a certain influence on the new product, of course, in the production, the whole volume of the bottle body 1 can be properly controlled not to be too large, and the product cost is lower.
In this embodiment, specific precursor solution and reducing solution contained in the first cavity 3 and the second cavity 4 are not particularly limited, for example, silver nitrate may be filled in the first cavity 3, and a chemical or biological reducing agent may be filled in the second cavity 4 to prepare micro-nano silver sol, in this case, the whole bottle body 1 is suitably designed as a brown bottle, or at least one side of the first cavity 3 is a brown bottle, and the other side is actually required to be selected, but the cost of the whole manufacturing is lower.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents and improvements made within the spirit and principle of the present invention are intended to be included within the scope of the present invention.
Claims (10)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911221242.2A CN110918041B (en) | 2019-12-03 | 2019-12-03 | A kind of micro-nano sol quick-mixing reaction bottle device and using method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201911221242.2A CN110918041B (en) | 2019-12-03 | 2019-12-03 | A kind of micro-nano sol quick-mixing reaction bottle device and using method thereof |
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| CN110918041A CN110918041A (en) | 2020-03-27 |
| CN110918041B true CN110918041B (en) | 2021-06-18 |
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