CN107982570A - One kind eliminates the unusual smell conditioning liquid, its preparation method and the sanitary napkin that eliminates the unusual smell - Google Patents

One kind eliminates the unusual smell conditioning liquid, its preparation method and the sanitary napkin that eliminates the unusual smell Download PDF

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CN107982570A
CN107982570A CN201711267355.7A CN201711267355A CN107982570A CN 107982570 A CN107982570 A CN 107982570A CN 201711267355 A CN201711267355 A CN 201711267355A CN 107982570 A CN107982570 A CN 107982570A
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eliminates
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张志全
李鹏先
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YUNNAN BAIYAO QINGYITANG INDUSTRY Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/42Use of materials characterised by their function or physical properties
    • A61L15/46Deodorants or malodour counteractants, e.g. to inhibit the formation of ammonia or bacteria
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/20Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing organic materials
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/40Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing ingredients of undetermined constitution or reaction products thereof, e.g. plant or animal extracts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2300/00Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
    • A61L2300/20Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing organic materials
    • A61L2300/216Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing organic materials with other specific functional groups, e.g. aldehydes, ketones, phenols, quaternary phosphonium groups
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2300/00Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
    • A61L2300/20Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing organic materials
    • A61L2300/30Compounds of undetermined constitution extracted from natural sources, e.g. Aloe Vera
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2300/00Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
    • A61L2300/40Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
    • A61L2300/404Biocides, antimicrobial agents, antiseptic agents

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Abstract

本发明提供了一种除异味护理液、其制备方法以及除异味卫生巾,涉及卫生用品领域。该除异味护理液的组成成分按质量份数计包括:四氢甲基嘧啶羧酸0.2‑2份、4‑乙基‑4‑大豆基硫酸乙酯吗啉0.5‑5份、甘草酸二钾0.1‑2份、苯甲酸钠0.1‑2份、苯氧乙醇1‑5份、葡萄柚果提取物0.1‑1份、葡萄糖氯己定1‑4份、乙醇20‑50份以及水20‑50份。其能有效去除异味,有效防止卫生巾表面繁殖细菌。该除异味护理液的制备方法通过将上述组成成分混合均匀,操作简单,容易实现,制得的除异味护理液能有效去除异味,防止异味散发。该除异味卫生巾,将上述除异味护理液喷涂至卫生巾表面,能有效去除异味,防止异味散发。This invention provides an odor-removing care solution, its preparation method, and an odor-removing sanitary napkin, relating to the field of hygiene products. The odor-removing care solution comprises, by weight parts: 0.2-2 parts tetrahydromethylpyrimidine carboxylic acid, 0.5-5 parts 4-ethyl-4-daidzein morpholine sulfate, 0.1-2 parts dipotassium glycyrrhizate, 0.1-2 parts sodium benzoate, 1-5 parts phenoxyethanol, 0.1-1 parts grapefruit fruit extract, 1-4 parts chlorhexidine gluconate, 20-50 parts ethanol, and 20-50 parts water. It effectively removes odors and prevents bacterial growth on the surface of the sanitary napkin. The preparation method of the odor-removing care solution involves uniformly mixing the above components; the operation is simple and easy to implement, and the resulting odor-removing care solution effectively removes odors and prevents odor emission. The odor-removing sanitary napkin, when sprayed with the above odor-removing care solution, effectively removes odors and prevents odor emission.

Description

一种除异味护理液、其制备方法以及除异味卫生巾A deodorizing nursing solution, its preparation method and deodorizing sanitary napkin

技术领域technical field

本发明涉及卫生用品领域,具体而言,涉及一种除异味护理液、其制备方法以及除异味卫生巾。The invention relates to the field of sanitary products, in particular to a deodorizing nursing solution, a preparation method thereof and a deodorizing sanitary napkin.

背景技术Background technique

卫生巾在使用了一定时间后,由于经血本身的气味、经血离体后氧化分解产生气体、微生物滋生代谢物产生气味、使用者本身的体味等影响,会产生混合的。令人不悦的气味,造成经期女性尴尬,甚至不好意思在人群中多逗留,严重影响女性经期的生活便捷度,且产生心理困扰。有些女性通过经期使用其他气味的香薰来试图掩盖经期产生的气味,有些卫生巾产品通过添加某些香味物质来掩盖经期的味道,但是两者均是治标不治本,有时候甚至会发生反应产生更为复杂、难闻的气味,额外添加的气味本身也令部分消费者产生畏惧感。After the sanitary napkin is used for a certain period of time, it will be mixed due to the smell of menstrual blood itself, the gas produced by oxidation and decomposition of menstrual blood after it is separated from the body, the odor produced by microbial growth metabolites, and the user's own body odor. The unpleasant smell makes menstruating women feel embarrassed, and even embarrassed to stay in the crowd, which seriously affects the convenience of women's menstruating life and causes psychological distress. Some women try to cover up the smell during menstruation by using aromatherapy with other scents during menstruation, and some sanitary napkin products cover up the smell of menstrual period by adding certain fragrance substances, but both of them treat the symptoms but not the root cause, and sometimes even react to produce more As a complex and unpleasant smell, the added smell itself also makes some consumers feel intimidated.

发明内容Contents of the invention

本发明的第一目的在于提供一种除异味护理液,其能有效去除异味,防止异味散发。The first object of the present invention is to provide a deodorizing care solution, which can effectively remove the peculiar smell and prevent the emission of the peculiar smell.

本发明的第二目的在于提供一种除异味护理液的制备方法,该制备方法简单,操作条件容易实现,制得的除异味护理液能有效去除异味,防止异味散发。The second object of the present invention is to provide a method for preparing a deodorizing care solution. The preparation method is simple and the operating conditions are easy to realize. The prepared deodorizing care solution can effectively remove peculiar smell and prevent the emission of peculiar smell.

本发明的第三目的在于提供一种除异味卫生巾,将除异味护理液应用于卫生巾上,能有效去除异味,防止异味散发。The third object of the present invention is to provide a deodorizing sanitary napkin. The deodorizing care solution is applied to the sanitary napkin, which can effectively remove the peculiar smell and prevent the emission of the peculiar smell.

本发明的实施例是这样实现的:Embodiments of the present invention are achieved like this:

一种除异味护理液,其组成成分按质量份数计包括:四氢甲基嘧啶羧酸0.2-2份、4-乙基-4-大豆基硫酸乙酯吗啉0.5-5份、甘草酸二钾0.1-2份、苯甲酸钠0.1-2份、苯氧乙醇1-5份、葡萄柚果提取物0.1-1份、葡萄糖氯己定1-4份、乙醇20-50份以及水20-50份。A deodorizing care solution, the composition of which includes, in parts by mass: 0.2-2 parts of tetrahydromethylpyrimidine carboxylic acid, 0.5-5 parts of 4-ethyl-4-soydine ethylsulfate morpholine, glycyrrhizic acid Dipotassium 0.1-2 parts, sodium benzoate 0.1-2 parts, phenoxyethanol 1-5 parts, grapefruit fruit extract 0.1-1 parts, glucose chlorhexidine 1-4 parts, ethanol 20-50 parts and water 20- 50 servings.

一种除异味护理液的制备方法,其包括:将部分水、四氢甲基嘧啶羧酸、4-乙基-4-大豆基硫酸乙酯吗啉、甘草酸二钾、苯甲酸钠、苯氧乙醇以及葡萄柚果提取物混合均匀,搅拌直至无沉淀或结晶,形成第一混合液,调节pH至5-6;再向第一混合液中加入葡萄糖氯己定搅拌直至无沉淀析出,再加入乙醇搅拌直至无沉淀析出,补足剩余的水。A preparation method for deodorizing nursing solution, comprising: mixing part of water, tetrahydromethylpyrimidine carboxylic acid, 4-ethyl-4-soydyl ethylsulfate morpholine, dipotassium glycyrrhizinate, sodium benzoate, phenoxy Mix ethanol and grapefruit fruit extract evenly, stir until there is no precipitation or crystallization, form the first mixed solution, adjust the pH to 5-6; then add glucose chlorhexidine to the first mixed solution and stir until no precipitation occurs, then add Stir with ethanol until no precipitate separates out, and make up the remaining water.

一种除异味卫生巾,将上述除异味护理液喷涂至卫生巾表面经挥发后制成。A sanitary napkin for deodorizing, which is made by spraying the deodorizing care solution on the surface of the sanitary napkin and volatilizing it.

本发明实施例的有益效果例如包括:The beneficial effects of the embodiments of the present invention include, for example:

本发明实施例提供的除异味护理液利用其组成成分中的四氢甲基嘧啶羧酸与4-乙基-4-大豆基硫酸乙酯吗啉进行复配,有效去除异味,4-乙基-4-大豆基硫酸乙酯吗啉能够有效配位或中和有异味的有机分子,且减少它们在蒸气相中的浓度,从而达到驱除异味的效果。甘草酸二钾的复配,能够进一步减缓4-乙基-4-大豆基硫酸乙酯吗啉的刺激性,且有利于保护皮肤,苯氧乙醇、葡萄糖酸氯己定以及葡萄柚提取物具有抑菌抗菌功效,其通过对微生物和细菌的抑制作用,能够有效防止卫生巾表面繁殖细菌,进而减少了细菌滋生产生的异味。此外,利用易挥发的乙醇作为组分中的一种,能够将防异味护理液喷涂在卫生巾上后,保持卫生巾的干燥,舒适度更佳。The odor-removing care solution provided by the embodiment of the present invention utilizes tetrahydromethylpyrimidine carboxylic acid and 4-ethyl-4-soydyl ethylsulfate morpholine in its components to compound, effectively removes odor, and 4-ethyl -4-Soydyl ethyl sulfate morpholine can effectively coordinate or neutralize odorous organic molecules, and reduce their concentration in the vapor phase, thereby achieving the effect of repelling odors. The compound of dipotassium glycyrrhizinate can further slow down the irritation of 4-ethyl-4-soydyl ethyl sulfate morpholine, and is beneficial to protect the skin. Phenoxyethanol, chlorhexidine gluconate and grapefruit extract have Antibacterial and antibacterial effect, through the inhibition of microorganisms and bacteria, it can effectively prevent the breeding of bacteria on the surface of the sanitary napkin, thereby reducing the odor produced by bacterial breeding. In addition, by using volatile ethanol as one of the components, the anti-odor care solution can be sprayed on the sanitary napkin to keep the sanitary napkin dry and more comfortable.

本发明实施例提供的除异味护理液的制备方法,该制备方法简单,操作条件容易实现,制得的除异味护理液能有效去除异味,防止异味散发。The preparation method of the odor-removing care solution provided by the embodiment of the present invention is simple, and the operating conditions are easy to realize. The prepared deodorization care solution can effectively remove the odor and prevent the emission of the odor.

本发明实施例提供的除异味卫生巾,将除异味护理液应用于卫生巾上,能有效去除异味,防止异味散发。The odor-removing sanitary napkin provided by the embodiment of the present invention applies the deodorizing care solution to the sanitary napkin, which can effectively remove the odor and prevent the emission of the odor.

具体实施方式Detailed ways

下面将结合实施例对本发明的实施方案进行详细描述,但是本领域技术人员将会理解,下列实施例仅用于说明本发明,而不应视为限制本发明的范围。实施例中未注明具体条件者,按照常规条件或制造商建议的条件进行。所用试剂或仪器未注明生产厂商者,均为可以通过市售购买获得的常规产品。Embodiments of the present invention will be described in detail below in conjunction with examples, but those skilled in the art will understand that the following examples are only for illustrating the present invention, and should not be considered as limiting the scope of the present invention. Those who do not indicate the specific conditions in the examples are carried out according to the conventional conditions or the conditions suggested by the manufacturer. The reagents or instruments used were not indicated by the manufacturer, and they were all conventional products that could be purchased from the market.

下面对本发明实施例的除异味护理液、其制备方法以及除异味卫生巾进行具体说明。The deodorizing care solution of the embodiment of the present invention, its preparation method and the deodorizing sanitary napkin are described in detail below.

一种除异味护理液,其组成成分按质量份数计包括:四氢甲基嘧啶羧酸0.2-2份、4-乙基-4-大豆基硫酸乙酯吗啉0.5-5份、甘草酸二钾0.1-2份、苯甲酸钠0.1-2份、苯氧乙醇1-5份、葡萄柚果提取物0.1-1份、葡萄糖氯己定1-4份、乙醇20-50份以及水20-50份。A deodorizing care solution, the composition of which includes, in parts by mass: 0.2-2 parts of tetrahydromethylpyrimidine carboxylic acid, 0.5-5 parts of 4-ethyl-4-soydine ethylsulfate morpholine, glycyrrhizic acid Dipotassium 0.1-2 parts, sodium benzoate 0.1-2 parts, phenoxyethanol 1-5 parts, grapefruit fruit extract 0.1-1 parts, glucose chlorhexidine 1-4 parts, ethanol 20-50 parts and water 20- 50 servings.

其中,四氢甲基嘧啶羧酸又称之为依克多因,其能有效提升皮肤细胞的免疫防护能力,增加细胞修复能力,使皮肤能有效对抗微生物及过敏原的入侵。Among them, tetrahydromethyl pyrimidine carboxylic acid, also known as ectoine, can effectively enhance the immune protection ability of skin cells, increase cell repair ability, and enable the skin to effectively resist the invasion of microorganisms and allergens.

4-乙基-4-大豆基硫酸乙酯吗啉,其型号为FORESTALL,FORESTALL是一个非常独特的阳离子表面活性剂,可用于驱除多种多样的异味。它通过配位或中和有异味的有机分子,且减少它们在蒸气相中的浓度,从而达到驱除异味的效果。由于它的效果好,无须额外添加香精,在产品中很容易加入。它的活性物用量,以及在水中的完全的相溶性,使得它成为在家居和工业领域中大多数除味产品的理想选择。4-Ethyl-4-soydyl ethyl sulfate morpholine, its model is FORESTALL, FORESTALL is a very unique cationic surfactant, which can be used to repel a variety of odors. It achieves the effect of repelling odors by coordinating or neutralizing odorous organic molecules and reducing their concentration in the vapor phase. Because of its good effect, it is easy to add in products without adding additional fragrance. Its active content, combined with its complete miscibility in water, make it ideal for most deodorizing products in household and industrial applications.

本实施例中,通过4-乙基-4-大豆基硫酸乙酯吗啉与四氢甲基嘧啶羧酸的复配,能够将4-乙基-4-大豆基硫酸乙酯吗啉应用于卫生巾的护理液领域,有效去除异味。In the present embodiment, through the compounding of 4-ethyl-4-soydyl ethyl sulfate morpholine and tetrahydromethyl pyrimidine carboxylic acid, 4-ethyl-4-soydyl ethyl sulfate morpholine can be used in The care solution field of sanitary napkins can effectively remove odors.

甘草酸二钾具有有抗炎、抗过敏、保湿等功效,甘草酸二钾的加入能够降低护理液对阴道黏膜的刺激性,提高卫生巾的安全和舒适度。Dipotassium glycyrrhizinate has anti-inflammatory, anti-allergic, moisturizing and other effects. The addition of dipotassium glycyrrhizinate can reduce the irritation of the nursing solution to the vaginal mucosa and improve the safety and comfort of sanitary napkins.

苯甲酸钠亲油性较大,易穿透细胞膜进入细胞体内,干扰细胞膜的通透性,抑制细胞膜对氨基酸的吸收;进入细胞体内电离酸化细胞内的碱储,并抑制细胞的呼吸酶系的活性,阻止乙酰辅酶A缩合反应,从而起到防腐的目的。同时还具有杀菌、抗微生物的作用。本实施例中通过复配甘草酸二钾和苯甲酸钠,能够有效降低苯甲酸钠的刺激剂,使得除异味护理液的安全系数更高,刺激性更小。Sodium benzoate is highly lipophilic, easily penetrates the cell membrane and enters the cell body, interferes with the permeability of the cell membrane, and inhibits the absorption of amino acids by the cell membrane; enters the cell body, ionizes and acidifies the alkali storage in the cell, and inhibits the activity of the respiratory enzyme system of the cell. Prevent the condensation reaction of acetyl Coenzyme A, so as to achieve the purpose of antiseptic. At the same time, it also has bactericidal and antimicrobial effects. In this embodiment, by compounding dipotassium glycyrrhizinate and sodium benzoate, the irritant of sodium benzoate can be effectively reduced, so that the deodorizing care solution has a higher safety factor and less irritation.

苯氧乙醇是一种无色的油状液体,具有抗菌功效,能够作为防腐剂。Phenoxyethanol is a colorless, oily liquid that has antimicrobial properties and acts as a preservative.

葡萄糖酸氯己定具有较广的抗微生物活性,能够抑菌和杀菌,为无色或淡黄色几乎透明略为黏稠的液体;无臭或几乎无臭。Chlorhexidine gluconate has broad antimicrobial activity and can inhibit and kill bacteria. It is a colorless or light yellow almost transparent and slightly viscous liquid; odorless or almost odorless.

葡萄柚提取物具有抗菌抗感染、滋养组织细胞的作用。Grapefruit extract has antibacterial, anti-infection, and nourishing tissue cells.

本实施例中,利用苯氧乙醇、葡萄糖酸氯己定以及葡萄柚提取物等多种具有抑菌抗菌功效的成分添加至除异味护理液中,苯氧乙醇、葡萄糖酸氯己定以及葡萄柚提取物通过对微生物和细菌的抑制作用,能够有效防止卫生巾表面繁殖细菌,造成人体生殖器感染,带来疾病。苯氧乙醇、葡萄糖酸氯己定以及葡萄柚提取物的复配能够实现对多种细菌具有抑制作用,同时抑制细菌能够有效降低经血异味,为用户提供更好的体验。苯氧乙醇、葡萄糖酸氯己定以及葡萄柚提取物按照特定的质量份数进行配伍,效果更好。In this example, phenoxyethanol, chlorhexidine gluconate, and grapefruit extract are used to add various ingredients with antibacterial and antibacterial effects to the deodorant care solution. Phenoxyethanol, chlorhexidine gluconate, and grapefruit By inhibiting microorganisms and bacteria, the extract can effectively prevent bacteria from multiplying on the surface of sanitary napkins, causing human genital infection and disease. The combination of phenoxyethanol, chlorhexidine gluconate, and grapefruit extract can inhibit a variety of bacteria, and inhibiting bacteria can effectively reduce the odor of menstrual blood and provide users with a better experience. Phenoxyethanol, chlorhexidine gluconate and grapefruit extract are compatible according to specific mass parts, and the effect is better.

乙醇易挥发,将乙醇作为组分添加到除异味护理液中,能使除异味护理液在喷涂在卫生巾表面时易于挥发,在生产完成后处于干燥状态,使卫生巾本身的吸收性能提高,使用感受更好。Ethanol is volatile. Adding ethanol as a component to the deodorizing care solution can make the deodorizing care solution easy to volatilize when sprayed on the surface of the sanitary napkin, and it will be in a dry state after production, improving the absorption performance of the sanitary napkin itself. It feels better to use.

经发明人研究发现,组成成分按质量份数计优选包括:四氢甲基嘧啶羧酸0.2-1份、4-乙基-4-大豆基硫酸乙酯吗啉0.5-3份、甘草酸二钾0.1-1份、苯甲酸钠0.1-1份、苯氧乙醇1-3份、葡萄柚果提取物0.1-0.8份、葡萄糖氯己定1-3份、乙醇20-35份以及水40-70份。按照上述质量份数配伍形成的除异味护理液的除异味效果更佳。The inventors have found through research that the composition preferably includes: 0.2-1 parts of tetrahydromethylpyrimidine carboxylic acid, 0.5-3 parts of 4-ethyl-4-soydyi ethylsulfate morpholine, and glycyrrhizic acid di Potassium 0.1-1 part, sodium benzoate 0.1-1 part, phenoxyethanol 1-3 part, grapefruit fruit extract 0.1-0.8 part, glucose chlorhexidine 1-3 part, ethanol 20-35 part and water 40-70 part share. The deodorizing care solution formed according to the above-mentioned compatibility in parts by mass has a better deodorizing effect.

进一步地,上述组成成分还包括:磷酸氢二钠为0.1-1份;优选地,磷酸氢二钠为0.1-0.8份。Further, the above composition also includes: 0.1-1 part of disodium hydrogen phosphate; preferably, 0.1-0.8 part of disodium hydrogen phosphate.

磷酸氢二钠用作中和剂,能够中和经血中的异味。由于磷酸氢二钠具有一定的刺激作用,会刺激皮肤,因此本实施例中,磷酸氢二钠的用量较少。并且,本实施例中通过复配甘草酸二钾能够有效中和并降低磷酸氢二钠的刺激作用,同时也可以防止磷酸氢二钠的过敏反应。甘草酸二钾能够与柠檬酸钠以及磷酸氢二钠配伍,可加速皮肤对柠檬酸钠的吸收而增加除异味的功效,同时能够降低磷酸氢二钠的刺激性。Disodium hydrogen phosphate is used as a neutralizing agent, which can neutralize the bad smell in menstrual blood. Because disodium hydrogen phosphate has a certain stimulating effect, it can irritate the skin, so in this embodiment, the consumption of disodium hydrogen phosphate is less. Moreover, in this example, compounding dipotassium glycyrrhizinate can effectively neutralize and reduce the stimulating effect of disodium hydrogen phosphate, and can also prevent the allergic reaction of disodium hydrogen phosphate. Dipotassium glycyrrhizinate can be compatible with sodium citrate and disodium hydrogen phosphate, which can accelerate the skin's absorption of sodium citrate and increase the effect of deodorization, while reducing the irritation of disodium hydrogen phosphate.

进一步地,本发明实施例中的除异味护理液的组成成分按照质量份数计还包括:植物活性硒0.1-2份、地龙提取物1-2份以及拳参醇提物1-2份。Further, the composition of the deodorizing care solution in the embodiment of the present invention also includes: 0.1-2 parts of plant active selenium, 1-2 parts of earthworm extract and 1-2 parts of ethanol extract .

植物活性硒具有抗氧化的功效。地龙提取物具有抗凝血作用,能够有效延长凝血时间。经发明人研究发现,将植物活性硒、地龙提取物以及拳参醇提物复配使用,植物活性硒能够有效防止经血氧化,而拳参醇提物与地龙提取物复配,能有效延长经血凝结时间,进而避免经血凝结。Phytoactive selenium has antioxidant properties. Earthworm extract has anticoagulant effect and can effectively prolong blood coagulation time. The inventors have found through research that the combination of plant active selenium, earthworm extract and box ginseng alcohol extract can effectively prevent menstrual blood oxidation, and the compounding of box ginseng alcohol extract and earthworm extract can effectively Prolong the clotting time of menstrual blood, thereby avoiding menstrual blood clotting.

经发明人研究发现,优选采用植物活性硒0.1-1份、地龙提取物1-1.5份以及拳参醇提物1-1.5份进行复配,防止血液凝结的作用更佳,经血不易凝结和氧化,产生的异味少。The inventors found that it is better to use 0.1-1 parts of plant active selenium, 1-1.5 parts of earthworm extract and 1-1.5 parts of ginseng alcohol extract for compounding, which can prevent blood coagulation better, menstrual blood is not easy to coagulate and Oxidation, less odor.

一种除异味护理液的制备方法,其包括:A preparation method for deodorizing care solution, comprising:

S1:形成第一混合液。S1: forming the first mixed solution.

将部分水、四氢甲基嘧啶羧酸、4-乙基-4-大豆基硫酸乙酯吗啉、甘草酸二钾、苯甲酸钠、苯氧乙醇以及葡萄柚果提取物混合均匀,搅拌直至无沉淀或结晶,形成第一混合液,调节pH至5-6;Mix part of water, tetrahydromethyl pyrimidine carboxylic acid, 4-ethyl-4-soylyl ethyl sulfate morpholine, dipotassium glycyrrhizinate, sodium benzoate, phenoxyethanol and grapefruit fruit extract, stir until no Precipitate or crystallize to form the first mixed solution, adjust the pH to 5-6;

值得注意的是,水、四氢甲基嘧啶羧酸、4-乙基-4-大豆基硫酸乙酯吗啉、甘草酸二钾、苯甲酸钠、苯氧乙醇以及葡萄柚果提取物是按照特定的步骤和顺序加入,搅拌均匀后再进入后续的组分,这样有利于各个组分混合均匀。调节pH至5-6有利于使得整个第一混合液呈弱酸性,有利于保持除异味护理液中组分的活性。Of note, water, tetrahydromethyl pyrimidine carboxylic acid, 4-ethyl-4-soylyl ethyl sulfate morpholine, dipotassium glycyrrhizinate, sodium benzoate, phenoxyethanol, and grapefruit fruit extract were Add in the steps and order, stir evenly before entering the subsequent components, which is conducive to the uniform mixing of each component. Adjusting the pH to 5-6 is beneficial to make the entire first mixed solution weakly acidic, and is beneficial to maintain the activity of the components in the deodorizing care solution.

S2:形成第二混合液。S2: forming a second mixed solution.

取部分水,并向水中加入磷酸氢二钠,混合均匀,形成第二混合液,将第二混合液加入第一混合液中,搅拌均匀。Take part of the water, add disodium hydrogen phosphate to the water, mix well to form the second mixed solution, add the second mixed solution into the first mixed solution, and stir evenly.

磷酸氢二钠极易溶于水,通过取部分水,并向水中加入磷酸氢二钠,磷酸氢二钠能够在水中分布均匀,然后再与第一混合液混合,均匀性更佳。Disodium hydrogen phosphate is very soluble in water. By taking part of the water and adding disodium hydrogen phosphate to the water, disodium hydrogen phosphate can be evenly distributed in the water, and then mixed with the first mixed solution to achieve better uniformity.

值得注意的是,步骤S2为可选步骤,当组分中不含磷酸氢二钠时,可省略该步骤。It should be noted that step S2 is an optional step, and this step can be omitted when disodium hydrogen phosphate is not contained in the components.

S3:形成第三混合液。S3: forming a third mixed solution.

向第二混合液中依次间隔加入地龙提取物1-2份、植物活性硒0.1-2份以及拳参醇提物1-2份,间隔时间为3-5min;搅拌均匀,形成第三混合液,将第三混合液加入第一混合液中,搅拌均匀。Add 1-2 parts of earthworm extract, 0.1-2 parts of plant active selenium and 1-2 parts of ginseng alcohol extract to the second mixed solution in sequence, with an interval of 3-5 minutes; stir evenly to form the third mixed solution liquid, add the third mixed liquid to the first mixed liquid, and stir evenly.

地龙提取物和拳参醇提物均具有抗凝血功效,本实施例中,通过以植物活性硒作为中间桥梁,利用其抗氧化活性将地龙提取物和拳参醇提物进行复配,从而能够有效避免经血凝结。Both the extract of Earthworm and the alcoholic extract of Panax ginseng have anticoagulant effects. In this example, the extract of Earthworm and the alcoholic extract of Panax ginseng were compounded by using plant active selenium as an intermediate bridge to make use of its antioxidant activity , so as to effectively prevent menstrual blood from clotting.

在将地龙提取物、植物活性硒以及拳参醇提物加入上述第二混合液时,需注意,应当先添加地龙提取物、再加入植物活性硒,最后加入拳参醇提物,植物活性硒的中间加入能够起到很好的桥梁和调节的作用。When adding the earthworm extract, plant active selenium, and ginseng ethanol extract to the above-mentioned second mixture, it should be noted that the earthworm extract should be added first, then the plant active selenium, and finally the ethanol extract of ginseng. The addition of active selenium in the middle can play a very good role in bridge and regulation.

值得注意的是,步骤S3为可选步骤,当组分中不含地龙提取物、植物活性硒以及拳参醇提物时,可省略该步骤。It is worth noting that step S3 is an optional step, and this step can be omitted when the components do not contain earthworm extract, plant active selenium and ginseng alcohol extract.

S4:加入葡萄糖氯己定和乙醇。S4: Add glucose chlorhexidine and ethanol.

向第一混合液和第三混合液的混合物中加入葡萄糖氯己定搅拌直至无沉淀析出,再加入乙醇搅拌直至无沉淀析出,补足剩余的水。当步骤S2和S3省略后,可直接向第一混合液中加入葡萄糖氯己定。Add chlorhexidine dextrose to the mixture of the first mixed solution and the third mixed solution and stir until no precipitation occurs, then add ethanol and stir until no precipitation occurs, and make up the remaining water. When steps S2 and S3 are omitted, glucose chlorhexidine can be directly added to the first mixed solution.

一种除异味卫生巾,将上述除异味护理液喷涂至卫生巾表面经挥发后制成。其中,除异味护理液的喷涂量为0.1-0.3g/片。挥发时间为3-5min,挥发时间快。A sanitary napkin for deodorizing, which is made by spraying the deodorizing care solution on the surface of the sanitary napkin and volatilizing it. Wherein, the spray amount of deodorizing care solution is 0.1-0.3g/piece. The volatilization time is 3-5min, and the volatilization time is fast.

通过适宜的喷涂量能够保证每片卫生巾的除异味效果达到最佳,同时除异味护理液中的水分和乙醇挥发,使除异味护理液中的有效成分保留至卫生巾表面,经后续的小袋包装,能够有效保持有效成分附着于卫生巾表面且不易挥发。The appropriate amount of spraying can ensure the best deodorizing effect of each piece of sanitary napkin. At the same time, the water and ethanol in the deodorizing care solution will volatilize, so that the active ingredients in the deodorizing care solution will be retained on the surface of the sanitary napkin, and then passed through the subsequent sachet The packaging can effectively keep the active ingredient attached to the surface of the sanitary napkin and is not easy to volatilize.

本发明实施例提供的除异味护理液利用其组成成分中的四氢甲基嘧啶羧酸与4-乙基-4-大豆基硫酸乙酯吗啉进行复配,有效去除异味,4-乙基-4-大豆基硫酸乙酯吗啉能够有效配位或中和有异味的有机分子,且减少它们在蒸气相中的浓度,从而达到驱除异味的效果。甘草酸二钾的复配,能够进一步减缓4-乙基-4-大豆基硫酸乙酯吗啉的刺激性,且有利于保护皮肤,苯氧乙醇、葡萄糖酸氯己定以及葡萄柚提取物具有抑菌抗菌功效,其通过对微生物和细菌的抑制作用,能够有效防止卫生巾表面繁殖细菌,进而减少了细菌滋生产生的异味。此外,利用易挥发的乙醇作为组分中的一种,能够将防异味护理液喷涂在卫生巾上后,保持卫生巾的干燥,舒适度更佳。The odor-removing care solution provided by the embodiment of the present invention utilizes tetrahydromethylpyrimidine carboxylic acid and 4-ethyl-4-soydyl ethylsulfate morpholine in its components to compound, effectively removes odor, and 4-ethyl -4-Soydyl ethyl sulfate morpholine can effectively coordinate or neutralize odorous organic molecules, and reduce their concentration in the vapor phase, thereby achieving the effect of repelling odors. The compound of dipotassium glycyrrhizinate can further slow down the irritation of 4-ethyl-4-soydyl ethyl sulfate morpholine, and is beneficial to protect the skin. Phenoxyethanol, chlorhexidine gluconate and grapefruit extract have Antibacterial and antibacterial effect, through the inhibition of microorganisms and bacteria, it can effectively prevent the breeding of bacteria on the surface of the sanitary napkin, thereby reducing the odor produced by bacterial breeding. In addition, by using volatile ethanol as one of the components, the anti-odor care solution can be sprayed on the sanitary napkin to keep the sanitary napkin dry and more comfortable.

本发明实施例提供的除异味护理液的制备方法,该制备方法简单,操作条件容易实现,制得的除异味护理液能有效去除异味,防止异味散发。The preparation method of the odor-removing care solution provided by the embodiment of the present invention is simple, and the operating conditions are easy to realize. The prepared deodorization care solution can effectively remove the odor and prevent the emission of the odor.

本发明实施例提供的除异味卫生巾,将除异味护理液应用于卫生巾上,能有效去除异味,防止异味散发。The odor-removing sanitary napkin provided by the embodiment of the present invention applies the deodorizing care solution to the sanitary napkin, which can effectively remove the odor and prevent the emission of the odor.

以下结合实施例对本发明的除异味护理液、其制备方法以及除异味卫生巾进一步进行阐述。The deodorizing care solution of the present invention, its preparation method and deodorizing sanitary napkin are further described below in conjunction with the examples.

实施例1Example 1

本实施例提供了一种除异味护理液,其组成成分包括:四氢甲基嘧啶羧酸1g、4-乙基-4-大豆基硫酸乙酯吗啉2.5g、甘草酸二钾1g、苯甲酸钠1g、苯氧乙醇3g、葡萄柚果提取物0.5g、葡萄糖氯己定2g、乙醇30g以及水59g。The present embodiment provides a deodorizing nursing solution, the composition of which includes: 1 g of tetrahydromethylpyrimidine carboxylic acid, 2.5 g of 4-ethyl-4-soydyl ethyl sulfate morpholine, 1 g of dipotassium glycyrrhizinate, benzene Sodium formate 1g, phenoxyethanol 3g, grapefruit fruit extract 0.5g, dextrose chlorhexidine 2g, ethanol 30g and water 59g.

其制备方法如下:部分水、四氢甲基嘧啶羧酸、4-乙基-4-大豆基硫酸乙酯吗啉、甘草酸二钾、苯甲酸钠、苯氧乙醇以及葡萄柚果提取物混合均匀,搅拌直至无沉淀或结晶,形成第一混合液,调节pH至5-6;再向第一混合液中加入葡萄糖氯己定搅拌直至无沉淀析出,再加入乙醇搅拌直至无沉淀析出,补足剩余的水。Its preparation method is as follows: part of water, tetrahydromethyl pyrimidine carboxylic acid, 4-ethyl-4-soydyl ethyl sulfate morpholine, dipotassium glycyrrhizinate, sodium benzoate, phenoxyethanol and grapefruit fruit extract are mixed evenly , stir until there is no precipitation or crystallization to form the first mixed solution, adjust the pH to 5-6; then add glucose chlorhexidine to the first mixed solution and stir until no precipitation, then add ethanol and stir until no precipitation, make up the remaining of water.

本实施例还提供了一种除异味卫生巾,将上述制备的除异味护理液按照每片0.3g的喷涂量喷涂至卫生巾表面,经挥发后制得。This embodiment also provides a deodorizing sanitary napkin, which is prepared by spraying the deodorizing care solution prepared above on the surface of the sanitary napkin at a spraying amount of 0.3 g per piece, and volatilizing.

实施例2Example 2

本实施例提供了一种除异味护理液,其组成成分包括:四氢甲基嘧啶羧酸0.2g、4-乙基-4-大豆基硫酸乙酯吗啉5g、甘草酸二钾0.1g、苯甲酸钠0.1g、苯氧乙醇1g、葡萄柚果提取物0.1g、葡萄糖氯己定1g、乙醇25g、磷酸氢二钠0.1g以及水67.4g。The present embodiment provides a deodorizing care solution, the composition of which includes: 0.2 g of tetrahydromethylpyrimidine carboxylic acid, 5 g of 4-ethyl-4-soydine ethyl sulfate morpholine, 0.1 g of dipotassium glycyrrhizinate, 0.1 g of sodium benzoate, 1 g of phenoxyethanol, 0.1 g of grapefruit fruit extract, 1 g of chlorhexidine dextrose, 25 g of ethanol, 0.1 g of disodium hydrogen phosphate, and 67.4 g of water.

其制备方法如下:部分水、四氢甲基嘧啶羧酸、4-乙基-4-大豆基硫酸乙酯吗啉、甘草酸二钾、苯甲酸钠、苯氧乙醇以及葡萄柚果提取物混合均匀,搅拌直至无沉淀或结晶,形成第一混合液,调节pH至5-6;取部分水,并向水中加入磷酸氢二钠,混合均匀,形成第二混合液,将第二混合液加入第一混合液中,搅拌均匀。再加入葡萄糖氯己定搅拌直至无沉淀析出,再加入乙醇搅拌直至无沉淀析出,补足剩余的水。Its preparation method is as follows: part of water, tetrahydromethyl pyrimidine carboxylic acid, 4-ethyl-4-soydyl ethyl sulfate morpholine, dipotassium glycyrrhizinate, sodium benzoate, phenoxyethanol and grapefruit fruit extract are mixed evenly , stir until there is no precipitation or crystallization to form the first mixed solution, adjust the pH to 5-6; take part of the water, and add disodium hydrogen phosphate to the water, mix well to form the second mixed solution, add the second mixed solution to the second mixed solution In a mixture, stir well. Then add glucose chlorhexidine and stir until no precipitation occurs, then add ethanol and stir until no precipitation occurs, and make up the remaining water.

本实施例还提供了一种除异味卫生巾,将上述制备的除异味护理液按照每片0.1g的喷涂量喷涂至卫生巾表面,经挥发后制得。This embodiment also provides a deodorizing sanitary napkin, which is prepared by spraying the deodorizing care solution prepared above on the surface of the sanitary napkin at a spraying amount of 0.1 g per piece, and volatilizing.

实施例3Example 3

本实施例提供了一种除异味护理液,其组成成分包括:四氢甲基嘧啶羧酸2g、4-乙基-4-大豆基硫酸乙酯吗啉0.5g、甘草酸二钾2g、苯甲酸钠2g、苯氧乙醇5g、葡萄柚果提取物1g、葡萄糖氯己定4g、乙醇20g、植物活性硒2份、地龙提取物2份、拳参醇提物2份以及水57.5g。The present embodiment provides a deodorizing care solution, the composition of which comprises: 2 g of tetrahydromethylpyrimidine carboxylic acid, 0.5 g of 4-ethyl-4-soydyl ethyl sulfate morpholine, 2 g of dipotassium glycyrrhizinate, benzene Sodium formate 2g, phenoxyethanol 5g, grapefruit fruit extract 1g, glucose chlorhexidine 4g, ethanol 20g, plant active selenium 2 parts, earthworm extract 2 parts, ginseng ethanol extract 2 parts and water 57.5g.

其制备方法如下:部分水、四氢甲基嘧啶羧酸、4-乙基-4-大豆基硫酸乙酯吗啉、甘草酸二钾、苯甲酸钠、苯氧乙醇以及葡萄柚果提取物混合均匀,搅拌直至无沉淀或结晶,形成第一混合液,调节pH至5-6;向第一混合液中依次间隔加入地龙提取物、植物活性硒以及拳参醇提物,间隔时间为3-5min;搅拌均匀,再加入葡萄糖氯己定搅拌直至无沉淀析出,再加入乙醇搅拌直至无沉淀析出,补足剩余的水。Its preparation method is as follows: part of water, tetrahydromethyl pyrimidine carboxylic acid, 4-ethyl-4-soydyl ethyl sulfate morpholine, dipotassium glycyrrhizinate, sodium benzoate, phenoxyethanol and grapefruit fruit extract are mixed evenly , stir until there is no precipitation or crystallization to form the first mixed solution, adjust the pH to 5-6; add earthworm extract, plant active selenium and ginseng alcohol extract to the first mixed solution at intervals, and the interval is 3- 5min; Stir evenly, then add glucose chlorhexidine and stir until no precipitation occurs, then add ethanol and stir until no precipitation occurs, and make up the remaining water.

本实施例还提供了一种除异味卫生巾,将上述制备的除异味护理液按照每片0.2g的喷涂量喷涂至卫生巾表面,经挥发后制得。This embodiment also provides a deodorizing sanitary napkin, which is prepared by spraying the deodorizing care solution prepared above on the surface of the sanitary napkin at a spraying amount of 0.2 g per piece, and volatilizing.

实施例4Example 4

本实施例提供了一种除异味护理液,其组成成分包括:四氢甲基嘧啶羧酸1.5g、4-乙基-4-大豆基硫酸乙酯吗啉4g、甘草酸二钾1.5g、苯甲酸钠1.5g、苯氧乙醇3.5g、葡萄柚果提取物0.8g、葡萄糖氯己定3g、乙醇50g、磷酸氢二钠为0.8g、植物活性硒0.5份、地龙提取物1.2份、拳参醇提物1.2份以及水30.5g。The present embodiment provides a deodorizing care solution, the composition of which comprises: 1.5 g of tetrahydromethylpyrimidine carboxylic acid, 4 g of 4-ethyl-4-soydine ethyl sulfate morpholine, 1.5 g of dipotassium glycyrrhizinate, Sodium benzoate 1.5g, phenoxyethanol 3.5g, grapefruit fruit extract 0.8g, glucose chlorhexidine 3g, ethanol 50g, disodium hydrogen phosphate 0.8g, plant active selenium 0.5 parts, earthworm extract 1.2 parts, punch 1.2 parts of ginseng alcohol extract and 30.5 g of water.

其制备方法如下:部分水、四氢甲基嘧啶羧酸、4-乙基-4-大豆基硫酸乙酯吗啉、甘草酸二钾、苯甲酸钠、苯氧乙醇以及葡萄柚果提取物混合均匀,搅拌直至无沉淀或结晶,形成第一混合液,调节pH至5-6;取部分水,并向水中加入磷酸氢二钠,混合均匀,形成第二混合液,向第二混合液中依次间隔加入地龙提取物1-2份、植物活性硒0.1-2份以及拳参醇提物1-2份,间隔时间为3-5min;搅拌均匀,形成第三混合液,将第三混合液加入第一混合液中,搅拌均匀。再加入葡萄糖氯己定搅拌直至无沉淀析出,再加入乙醇搅拌直至无沉淀析出,补足剩余的水。Its preparation method is as follows: part of water, tetrahydromethyl pyrimidine carboxylic acid, 4-ethyl-4-soydyl ethyl sulfate morpholine, dipotassium glycyrrhizinate, sodium benzoate, phenoxyethanol and grapefruit fruit extract are mixed evenly , stir until there is no precipitation or crystallization to form the first mixed solution, adjust the pH to 5-6; take part of the water, and add disodium hydrogen phosphate to the water, mix well to form the second mixed solution, and add to the second mixed solution in turn Add 1-2 parts of earthworm extract, 0.1-2 parts of plant active selenium and 1-2 parts of ginseng alcohol extract at intervals, the interval time is 3-5min; stir evenly to form the third mixed solution, and the third mixed solution Add to the first mixture and stir well. Then add glucose chlorhexidine and stir until no precipitation occurs, then add ethanol and stir until no precipitation occurs, and make up the remaining water.

本实施例还提供了一种除异味卫生巾,将上述制备的除异味护理液按照每片0.25g的喷涂量喷涂至卫生巾表面,经挥发后制得。This embodiment also provides a deodorizing sanitary napkin, which is prepared by spraying the deodorizing care solution prepared above on the surface of the sanitary napkin at a spraying amount of 0.25 g per piece, and volatilizing.

实施例5Example 5

本实施例提供了一种除异味护理液,其组成成分包括:四氢甲基嘧啶羧酸1g、4-乙基-4-大豆基硫酸乙酯吗啉3g、甘草酸二钾1g、苯甲酸钠1g、苯氧乙醇3g、葡萄柚果提取物0.7g、葡萄糖氯己定2.1g、乙醇33g、磷酸氢二钠为0.7g、植物活性硒0.9份、地龙提取物1.3份、拳参醇提物1.3份以及水49g。The present embodiment provides a deodorizing nursing solution, the composition of which includes: 1 g of tetrahydromethylpyrimidine carboxylic acid, 3 g of 4-ethyl-4-soydyl ethylsulfate morpholine, 1 g of dipotassium glycyrrhizinate, and sodium benzoate 1g, 3g of phenoxyethanol, 0.7g of grapefruit fruit extract, 2.1g of glucose chlorhexidine, 33g of ethanol, 0.7g of disodium hydrogen phosphate, 0.9 parts of plant active selenium, 1.3 parts of earthworm extract, ethanol extract of ginseng 1.3 parts of food and 49g of water.

本实施例还提供了一种除异味卫生巾,将上述制备的除异味护理液按照每片0.15g的喷涂量喷涂至卫生巾表面,经挥发后制得。This embodiment also provides a deodorizing sanitary napkin, which is prepared by spraying the deodorizing care solution prepared above on the surface of the sanitary napkin at a spraying amount of 0.15 g per piece, and volatilizing.

对比实验Comparative Experiment

一、除异味试验1. Odor removal test

将纯净水等量喷涂在相同材质的卫生巾表面作为空白例;Spray an equal amount of purified water on the surface of a sanitary napkin of the same material as a blank example;

将实施例1-5制备的除异味卫生巾作为试验例1-5;The deodorizing sanitary napkin prepared by embodiment 1-5 is used as test example 1-5;

将实施例1提供的除异味护理液稀释5、10、15以及20倍后,喷涂等量的除异味护理液于卫生巾表面作为对比例1-4;After diluting the deodorizing care solution provided by Example 1 by 5, 10, 15 and 20 times, spray an equal amount of deodorizing care solution on the surface of the sanitary napkin as comparative examples 1-4;

将市售的卫生巾作为对比例5。A commercially available sanitary napkin was used as Comparative Example 5.

测试上述空白例、试验例1-5以及对比例1-5的除异味功效。Test the deodorizing effect of the above blank example, test examples 1-5 and comparative examples 1-5.

接着向空白例、试验例1-5以及对比例1-5卫生巾上分别加入等量的兔血,放入37℃条件下,将卫生巾按原样包好,放置10min,用嗅觉评定除异味效果,评定结果参见表1。Then add the same amount of rabbit blood to the sanitary napkins of the blank example, test examples 1-5 and comparative examples 1-5 respectively, place them at 37°C, wrap the sanitary napkins as they are, and leave them for 10 minutes, and use the sense of smell to evaluate the deodorization For results, see Table 1.

表1.嗅觉评定除血腥味结果Table 1. Olfactory evaluation results for removing bloody smell

接着再向相同的空白例、试验例1-5以及对比例1-5卫生巾上分别加入等量的异味源物质,放入37℃条件下,将卫生巾按原样包好,放置10min,用嗅觉评定除异味效果,评定结果参见表2。Then add the same amount of odor source substances to the same blank example, test example 1-5 and comparative example 1-5 sanitary napkin respectively, put it under the condition of 37 ℃, wrap the sanitary napkin as it is, leave it for 10min, use Olfactory evaluation of deodorizing effect, the evaluation results are shown in Table 2.

表2.嗅觉评定除异味源结果Table 2. Odor source removal results of olfactory evaluation

示例example 0min0min 2min2min 5min5min 10min10min 空白例blank example 刺鼻的氨味pungent ammonia smell 刺鼻的氨味pungent ammonia smell 较浓的氨味strong ammonia smell 氨味变淡Ammonia smell fades 试验例1Test example 1 刺鼻的氨味pungent ammonia smell 少有氨味little ammonia smell 几乎无味almost tasteless 无味tasteless 试验例2Test example 2 刺鼻的氨味pungent ammonia smell 少有氨味little ammonia smell 几乎无味almost tasteless 无味tasteless 试验例3Test example 3 刺鼻的氨味pungent ammonia smell 少有氨味little ammonia smell 几乎无味almost tasteless 无味tasteless 试验例4Test example 4 刺鼻的氨味pungent ammonia smell 少有氨味little ammonia smell 几乎无味almost tasteless 无味tasteless 试验例5Test example 5 刺鼻的氨味pungent ammonia smell 少有氨味little ammonia smell 几乎无味almost tasteless 无味tasteless 对比例1Comparative example 1 刺鼻的氨味pungent ammonia smell 氨味变淡Ammonia smell fades 少有氨味little ammonia smell 几乎无味almost tasteless 对比例2Comparative example 2 刺鼻的氨味pungent ammonia smell 较浓的氨味strong ammonia smell 氨味变淡Ammonia smell fades 少有氨味little ammonia smell 对比例3Comparative example 3 刺鼻的氨味pungent ammonia smell 较浓的氨味strong ammonia smell 少有氨味little ammonia smell 少有氨味little ammonia smell 对比例4Comparative example 4 刺鼻的氨味pungent ammonia smell 较浓的氨味strong ammonia smell 氨味变淡Ammonia smell fades 少有氨味little ammonia smell 对比例5Comparative example 5 刺鼻的氨味pungent ammonia smell 较浓的氨味strong ammonia smell 氨味变淡Ammonia smell fades 少有氨味little ammonia smell

通过表1和表2可以看出,本实施例提供的除异味护理液不管是对于逐渐产生的异味或者原始的异味源均有较好的去除异味的作用。It can be seen from Table 1 and Table 2 that the deodorizing care solution provided in this embodiment has a good deodorizing effect on both the gradually generated odor or the original odor source.

二、产品性能检测2. Product performance testing

本发明提供的除异味护理液喷涂于卫生巾产品后,经试验检测:抑菌性能;抑菌稳定性能达到国家标、法规要求,符合产品性能宣称;经除异味护理液喷涂的卫生巾进行皮肤变态反应试验;阴道黏膜刺激性试验均符合国家标准、法规要求,符合产品性能宣称。After the odor-removing care solution provided by the present invention is sprayed on the sanitary napkin product, it is detected through tests: antibacterial performance; the antibacterial stability performance reaches the requirements of national standards and regulations, and conforms to the product performance claim; Allergic reaction test; vaginal mucosa irritation test are in compliance with national standards and regulations, and in line with product performance claims.

表3:抑菌性能检测内容和结果;Table 3: Antibacterial performance test content and results;

表4:抑菌稳定性能检测内容和结果;Table 4: Test content and results of antibacterial stability performance;

表5:皮肤变态反应试验检测内容和结果;Table 5: Skin allergy test detection content and results;

表6:阴道黏膜刺激性试验检测内容和结果。Table 6: Test contents and results of vaginal mucosa irritation test.

具体检测内容和信息如下:The specific inspection content and information are as follows:

本发明提供的除异味护理液喷涂于卫生巾产品后,经检测,抑菌性能达到GB15979-2002一次性使用卫生用品卫生标准和《消毒技术规范》(第三版)的要求,明确具有抑菌功效,符合法规要求。检测内容参见表3:After the odor-removing care solution provided by the invention is sprayed on sanitary napkin products, the bacteriostatic performance reaches the requirements of GB15979-2002 Hygienic Standard for Disposable Sanitary Articles and "Disinfection Technical Specifications" (Third Edition), and it clearly has bacteriostatic properties. Efficacy, in line with regulatory requirements. See Table 3 for the test content:

表3:抑菌性能检测内容和结果Table 3: Contents and results of antibacterial performance test

本发明提供的除异味护理液喷涂于卫生巾产品后,经过恒温恒湿加速,加速周期为37℃下90天,即换算为贮存时间为两年,经检测,抑菌稳定性能达到GB15979-2002一次性使用卫生用品卫生标准和《消毒技术规范》(第三版)的要求,符合法规要求。检测内容参见表4:After the odor-removing care solution provided by the invention is sprayed on sanitary napkins, it is accelerated by constant temperature and humidity. The acceleration period is 90 days at 37°C, which means that the storage time is two years. After testing, the antibacterial stability reaches GB15979-2002 The hygienic standards for disposable sanitary products and the requirements of "Technical Specifications for Disinfection" (Third Edition) meet the requirements of laws and regulations. See Table 4 for the test content:

表4:抑菌稳定性能检测内容和结果Table 4: Test content and results of antibacterial stability performance

本发明提供的除异味护理液喷涂于卫生巾产品后,进行皮肤变态反应试验,达到《消毒技术规范》(第三版)的要求,明确该产品为极轻度致敏作用,符合法规要求,检测内容参见表5:After the odor-removing nursing solution provided by the invention is sprayed on the sanitary napkin product, a skin allergy test is carried out to meet the requirements of the "Technical Specification for Disinfection" (third edition), and it is clear that the product is extremely mildly sensitized and meets the requirements of regulations. See Table 5 for the test content:

表5:皮肤变态反应试验检测内容和结果Table 5: Test content and results of skin allergy test

本发明提供的除异味护理液喷涂于卫生巾产品后,进行阴道黏膜刺激性试验,达到《消毒技术规范》(第三版)的要求,明确该产品无阴道黏膜刺激性,符合法规要求,检测内容参见表6:After the odor-removing care solution provided by the invention is sprayed on sanitary napkin products, the vaginal mucosa irritation test is carried out to meet the requirements of the "Technical Specification for Disinfection" (third edition), and it is clear that the product has no vaginal mucosa irritation and meets the requirements of regulations. See Table 6 for content:

表6:阴道黏膜刺激性试验检测内容和结果Table 6: Test content and results of vaginal mucosa irritation test

以上仅为本发明的优选实施例而已,并不用于限制本发明,对于本领域的技术人员来说,本发明可以有各种更改和变化。凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。The above are only preferred embodiments of the present invention, and are not intended to limit the present invention. For those skilled in the art, the present invention may have various modifications and changes. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principles of the present invention shall be included within the protection scope of the present invention.

Claims (10)

  1. The conditioning liquid 1. one kind eliminates the unusual smell, it is characterised in that its constituent includes according to the mass fraction:Tetrahydrochysene methylpyrimidine carboxylic acid 0.2-2 parts, 0.5-5 parts of 4- ethyl -4- soybean-baseds ethyl-sulfate morpholine, 0.1-2 parts of dipotassium glycyrrhizinate, 0.1-2 parts of sodium benzoate, 1-5 parts of Phenoxyethanol, 0.1-1 parts of grape Fructus Citri grandis extract, 1-4 parts of glucose Chlorhexidine, 20-50 parts of ethanol and water 20-70 Part.
  2. 2. the conditioning liquid according to claim 1 that eliminates the unusual smell, it is characterised in that the constituent is wrapped according to the mass fraction Include:0.2-1 parts of tetrahydrochysene methylpyrimidine carboxylic acid, 0.5-3 parts of 4- ethyl -4- soybean-baseds ethyl-sulfate morpholine, dipotassium glycyrrhizinate 0.1-1 Part, 0.1-1 parts of sodium benzoate, 1-3 parts of Phenoxyethanol, 0.1-0.8 parts of grape Fructus Citri grandis extract, 1-3 parts of glucose Chlorhexidine, second 40-70 parts of 20-35 parts of alcohol and water.
  3. 3. the conditioning liquid according to claim 1 that eliminates the unusual smell, it is characterised in that the constituent further includes:Phosphoric acid hydrogen two Sodium is 0.1-1 parts;Preferably, the disodium hydrogen phosphate is 0.1-0.8 parts.
  4. 4. eliminated the unusual smell conditioning liquid according to claim 1-3 any one of them, it is characterised in that the constituent is according to quality Number meter further includes:1-2 parts of 0.1-2 parts of vegetable active selenium, 1-2 parts of Pheretima extract and adder-wort alcohol extract;
    Preferably, 0.1-1 parts of the vegetable active selenium, Pheretima extract 1-1.5 parts and the adder-wort alcohol extract 1-1.5 described Part.
  5. 5. a kind of preparation method of the conditioning liquid as claimed in claim 1 that eliminates the unusual smell, it is characterised in that it includes:
    By the part water, the tetrahydrochysene methylpyrimidine carboxylic acid, the 4- ethyls -4- soybean-based ethyl-sulfates morpholine, described sweet Oxalic acid dipotassium, the sodium benzoate, the Phenoxyethanol and the grape Fructus Citri grandis extract are uniformly mixed, and stirring is until without heavy Form sediment or crystallize, form the first mixed liquor, adjust pH to 5-6;
    The glucose Chlorhexidine stirring is added into first mixed liquor again up to no Precipitation, adds the ethanol Stirring supplies the remaining water up to no Precipitation.
  6. 6. the preparation method of the conditioning liquid according to claim 5 that eliminates the unusual smell, it is characterised in that to first mixed liquor It is middle to add before the glucose Chlorhexidine, the part water is taken, and disodium hydrogen phosphate is added into the water, it is uniformly mixed, The second mixed liquor is formed, second mixed liquor is added in first mixed liquor, is stirred evenly.
  7. 7. the preparation method of the conditioning liquid according to claim 6 that eliminates the unusual smell, it is characterised in that by second mixed liquor Before adding in first mixed liquor, further include into second mixed liquor interval successively add 1-2 parts of Pheretima extract, 1-2 parts of 0.1-2 parts of vegetable active selenium and adder-wort alcohol extract, interval time 3-5min;Stir evenly, form the 3rd mixing Liquid, the 3rd mixed liquor is added in first mixed liquor, is stirred evenly.
  8. The sanitary napkin 8. one kind eliminates the unusual smell, it is characterised in that the conditioning liquid that eliminates the unusual smell described in claim 1 is sprayed into sanitary napkin table Face is made after volatilization.
  9. 9. the sanitary napkin according to claim 8 that eliminates the unusual smell, it is characterised in that the quantity for spray of the conditioning liquid that eliminates the unusual smell is 0.1-0.3g/ pieces.
  10. 10. the sanitary napkin according to claim 8 that eliminates the unusual smell, it is characterised in that the time of the volatilization is 3-5min.
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CN108324590A (en) * 2018-05-17 2018-07-27 云南白药清逸堂实业有限公司 A kind of whitening conditioning liquid and preparation method thereof
CN108524304A (en) * 2018-05-17 2018-09-14 云南白药清逸堂实业有限公司 A kind of whitening protection pad and sanitary napkin, and preparation method thereof
CN109173677A (en) * 2018-11-03 2019-01-11 上海宸海科技集团有限公司 A kind of antibacterial type odor scavenging agent and preparation method thereof
CN109876059A (en) * 2019-04-30 2019-06-14 李风青 Women's antibacterial liquid
CN111329862A (en) * 2020-02-21 2020-06-26 华熙生物科技股份有限公司 Disinfectant, preparation method and application thereof
CN111329862B (en) * 2020-02-21 2021-06-01 华熙生物科技股份有限公司 Tetrahydropyrimidine and ethanol compound disinfectant and preparation method and application thereof
CN111282432A (en) * 2020-03-03 2020-06-16 安氧新材料科技(金华)有限公司 Preparation method of long-acting antibacterial aldehyde-removing odor-removing treatment liquid and product thereof
CN111282432B (en) * 2020-03-03 2022-06-14 安氧新材料科技(金华)有限公司 Preparation method of long-acting antibacterial aldehyde-removing odor-removing treatment liquid and product thereof
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