CN106365365A - Method of treating manganese ore waste water - Google Patents
Method of treating manganese ore waste water Download PDFInfo
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- CN106365365A CN106365365A CN201610729983.1A CN201610729983A CN106365365A CN 106365365 A CN106365365 A CN 106365365A CN 201610729983 A CN201610729983 A CN 201610729983A CN 106365365 A CN106365365 A CN 106365365A
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- waste water
- manganese ore
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/20—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/288—Treatment of water, waste water, or sewage by sorption using composite sorbents, e.g. coated, impregnated, multi-layered
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/30—Treatment of water, waste water, or sewage by irradiation
- C02F1/32—Treatment of water, waste water, or sewage by irradiation with ultraviolet light
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/72—Treatment of water, waste water, or sewage by oxidation
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/20—Heavy metals or heavy metal compounds
- C02F2101/206—Manganese or manganese compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/10—Nature of the water, waste water, sewage or sludge to be treated from quarries or from mining activities
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2301/00—General aspects of water treatment
- C02F2301/08—Multistage treatments, e.g. repetition of the same process step under different conditions
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2303/00—Specific treatment goals
- C02F2303/04—Disinfection
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Water Treatment By Sorption (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
The invention discloses a method of treating manganese ore waste water. The method includes the steps of: adsorption, irradiation, secondary adsorption, and coagulation and emission. In the method, a secondary adsorption method is employed, wherein a large amount of harmful substances in the manganese ore waste water are adsorbed; the waste water is further disinfected by means of ultraviolet treatment. A self-made carbonized material employed in the invention has very strong adsorption and purification effects. The method is simple and has significant effects. Finally, a high-effective coagulator is employed and has compensation effects with the carbonized material, thereby improving efficiency.
Description
Technical field
The present invention relates to technical field of waste water processing is and in particular to a kind of method of process manganese ore waste water.
Background technology
The exploitation of manganese ore can produce substantial amounts of manganese ore waste water, and manganese ore waste water can reduce drain pipe in long-term discharge process
Water passing capacity, substantial amounts of precipitation can be produced in pipeline, when serious, also can cause pipeline breaking, and if entered containing the waste water of manganese
Enter in our normal Drinking Waters, chronic poisoning also can be caused to be detrimental to health, but China's manganese resource is relatively scarce
Weary, rich ore is less, due to the restriction of each side such as equipment and treatment technology in the exploitation of a large amount of manganese ores and deep-processing process, makes
The waste material containing manganese of China and Mn-bearing waste water pollution are more serious, and manganese ore mine water pollution can be divided into mineral pollution, Organic substance dirty
Dye and germ contamination.Also there is radioactive material contamination and thermal pollution in some mines.Mineral pollution has sand, mud granule, ore deposit
Thing impurity, dust, solvency, bronsted lowry acids and bases bronsted lowry etc.；Organic Pollution has the oxygen of oils and fatss, biological metabolic product, timber and other materials
Change catabolite.The polluting of rock dust, breeze and the associated mineral that germ contamination is mainly exploited, be scattered in transportation.Manganese
One big feature of Ore mine water is that manganese ion content is high, and the manganese in mine water is by the oxide of manganese, sulfur in rock and mineral
Caused by compound, carbonate and silicate etc. are dissolved in water.In oxidizing process, manganese migrates generation mn2 in water, therefore in mine water
Manganese is mainly existed with mn2 form.During mining, discharge a large amount of waste water barren rocks from down-hole, pollute river, occupy
A large amount of farmland, mountain forest, grasslands, if destroy ecological balance it can be seen that manganese ore waste water deal with improperly will result in serious
Environmental pollution, passes through substantial amounts of experiment for this present inventor and studies, there is provided a kind of method processing manganese ore waste water.
Content of the invention
For solving above-mentioned technical problem, the invention provides a kind of method processing manganese ore waste water.
The present invention is achieved by the following technical programs:
A kind of method processing manganese ore waste water, the method comprises the following steps:
A, absorption: manganese ore waste water is imported in sedimentation tank, adds char-forming material, stewing process 3-7h in manganese ore waste water；
B, irradiation: after the completion of stewing process, the supernatant taking out waste water carries out ultraviolet treatment with irradiation, then add strong
Oxidant, according to the linear velocity stirring 16-20min of regulation；
C, second adsorption: continuously add char-forming material in the supernatant completing to treatment with irradiation, process 1-2h；
D, coagulation discharge: add flocculant in the supernatant completing to second adsorption, stand after stirring reaction 16-20min
1h separates and discharges.
Char-forming material in described step a is made up of following raw material: rice husk 8-14 part, timber 8-14 part, swelling
Native 6-12 part, kieselguhr 4-12 part, calcite 4-8 part, quartz sand 4-8 part, zeolite 2-8 part, gelatin 4-10 part.
The preparation method of described char-forming material is: by calcite and zeolite be crushed to after 220-260 mesh with bentonite, diatom
Soil, quartz sand, mix homogeneously obtain compound, after the wood particle that timber is cut into a diameter of 0.8-1cm is mixed with rice husk
Pour the diesel oil improved quality as wood particle and rice husk 5-7%, after igniting is fired into black wood charcoal, is put out by water with water and obtain carbon material, according to than
After compound is mixed homogeneously with carbon material by example, put into and in pulverizer, be crushed to 220-260 mesh, obtain mixed powder, by mixed powder
After material is mixed with water according to mass ratio, add gelatin, obtain the carbonization material for wastewater treatment finally by dried
Material finished product.
The ratio mixing for 1:1 according to mass ratio of the mixed proportion of described compound and carbon material.
Described step mixed powder is 1:1 with the mass ratio of water.
The time of described step b middle-ultraviolet lamp treatment with irradiation is 8-16min, and irradiation distance is 12-18cm.
The temperature of described dried is 60-70 DEG C, and drying time is 20-30min.
Strong oxidizer in described step b is potassium permanganate.
Stirring wire velocity control in described step b is 8-12m/s.
Flocculant in described step d is iron sulfate.
The beneficial effects of the present invention is: present invention employs absorption method twice, effectively will be a large amount of in manganese ore waste water
Harmful substance suctions out, and the process of combined with ultraviolet radiation, further waste water is sterilized, the self-control carbon that the present invention adopts
Change material and there is extremely strong absorption, clean-up effect, and processing method simply, effect substantially, finally coordinates efficient flocculant again,
Serve with char-forming material and mutually make up, propose efficient effect.
Specific embodiment
Below in conjunction with specific embodiment, technical scheme is further described, but claimed scope is not
It is confined to described.
Embodiment one
A kind of method processing manganese ore waste water, the method comprises the following steps:
A, absorption: manganese ore waste water is imported in sedimentation tank, adds char-forming material, stewing process 3h in manganese ore waste water；
B, irradiation: after the completion of stewing process, the supernatant taking out waste water carries out ultraviolet treatment with irradiation, at ultraviolet irradiation
The time of reason is 8min, and irradiation distance is 12cm, then adds potassium permanganate, stirs for 8m/s according to stirring wire velocity control
16min；
C, second adsorption: continuously add char-forming material in the supernatant completing to treatment with irradiation, process 1h；
D, coagulation discharge: add iron sulfate in the supernatant completing to second adsorption, after stirring reaction 16min, standing 1h divides
From discharging.
Char-forming material formula: 8 parts of rice husk, 8 parts of timber, 6 parts of bentonite, 4 parts of kieselguhr, 4 parts of calcite, 4 parts of quartz sand,
2 parts of zeolite, 4 parts of gelatin.
Char-forming material preparation method: by calcite and zeolite be crushed to after 220 mesh with bentonite, kieselguhr, quartz sand, mixed
Close and uniformly obtain compound, the wood particle that timber is cut into a diameter of 0.8cm is poured after being mixed with rice husk and improves quality as timber
Granule and the diesel oil of rice husk 5%, after igniting is fired into black wood charcoal, is put out by water with water and obtain carbon material, will according to the ratio for 1:1 for the mass ratio
After compound is mixed homogeneously with carbon material, put into and in pulverizer, be crushed to 220 mesh, obtain mixed powder, mixed powder is pressed with water
After the ratio mixing for 1:1 for the mass ratio, add gelatin, obtain the carbonization for wastewater treatment finally by dried
Finished material, the temperature of dried is 60 DEG C, and drying time is 20min.
Embodiment two
A kind of method processing manganese ore waste water, the method comprises the following steps:
A, absorption: manganese ore waste water is imported in sedimentation tank, adds char-forming material, stewing process 7h in manganese ore waste water；
B, irradiation: after the completion of stewing process, the supernatant taking out waste water carries out ultraviolet treatment with irradiation, at ultraviolet irradiation
The time of reason is 16min, and irradiation distance is 18cm, then adds potassium permanganate, stirs for 12m/s according to stirring wire velocity control
Mix 20min；
C, second adsorption: continuously add char-forming material in the supernatant completing to treatment with irradiation, process 2h；
D, coagulation discharge: add iron sulfate in the supernatant completing to second adsorption, after stirring reaction 20min, standing 1h divides
From discharging.
Char-forming material formula: 14 parts of rice husk, 14 parts of timber, 12 parts of bentonite, 12 parts of kieselguhr, 8 parts of calcite, quartz sand
8 parts, 8 parts of zeolite, 10 parts of gelatin.
Char-forming material preparation method: by calcite and zeolite be crushed to after 260 mesh with bentonite, kieselguhr, quartz sand, mixed
Close and uniformly obtain compound, the wood particle that timber is cut into a diameter of 1cm is poured after being mixed with rice husk and improves quality as timber
Grain and the diesel oil of rice husk 7%, after igniting is fired into black wood charcoal, is put out by water with water and obtain carbon material, will mix according to the ratio for 1:1 for the mass ratio
Close after material mixs homogeneously with carbon material, put into and in pulverizer, be crushed to 260 mesh, obtain mixed powder, by mixed powder and water according to
After mass ratio is the ratio mixing of 1:1, adds gelatin, obtain the carbonization material for wastewater treatment finally by dried
Material finished product, the temperature of dried is 70 DEG C, and drying time is 30min.
Embodiment three
A kind of method processing manganese ore waste water, the method comprises the following steps:
A, absorption: manganese ore waste water is imported in sedimentation tank, adds char-forming material, stewing process 5h in manganese ore waste water；
B, irradiation: after the completion of stewing process, the supernatant taking out waste water carries out ultraviolet treatment with irradiation, at ultraviolet irradiation
The time of reason is 12min, and irradiation distance is 15cm, then adds potassium permanganate, stirs for 15m/s according to stirring wire velocity control
Mix 18min；
C, second adsorption: continuously add char-forming material in the supernatant completing to treatment with irradiation, process 1.5h；
D, coagulation discharge: add iron sulfate in the supernatant completing to second adsorption, after stirring reaction 18min, standing 1h divides
From discharging.
Char-forming material formula: 11 parts of rice husk, 11 parts of timber, 9 parts of bentonite, 8 parts of kieselguhr, 6 parts of calcite, quartz sand 6
Part, 5 parts of zeolite, 7 parts of gelatin.
Char-forming material preparation method: by calcite and zeolite be crushed to after 240 mesh with bentonite, kieselguhr, quartz sand, mixed
Close and uniformly obtain compound, the wood particle that timber is cut into a diameter of 0.9cm is poured after being mixed with rice husk and improves quality as timber
Granule and the diesel oil of rice husk 6%, after igniting is fired into black wood charcoal, is put out by water with water and obtain carbon material, will according to the ratio for 1:1 for the mass ratio
After compound is mixed homogeneously with carbon material, put into and in pulverizer, be crushed to 240 mesh, obtain mixed powder, mixed powder is pressed with water
After the ratio mixing for 1:1 for the mass ratio, add gelatin, obtain the carbonization for wastewater treatment finally by dried
Finished material, the temperature of dried is 65 DEG C, and drying time is 25min.
Claims (10)
1. a kind of process manganese ore waste water method it is characterised in that: the method comprises the following steps:
A, absorption: manganese ore waste water is imported in sedimentation tank, adds char-forming material, stewing process 3-7h in manganese ore waste water；
B, irradiation: after the completion of stewing process, the supernatant taking out waste water carries out ultraviolet treatment with irradiation, then adds Strong oxdiative
Agent, according to the linear velocity stirring 16-20min of regulation；
C, second adsorption: continuously add char-forming material in the supernatant completing to treatment with irradiation, process 1-2h；
D, coagulation discharge: add flocculant in the supernatant completing to second adsorption, after stirring reaction 16-20min, standing 1h divides
From discharging.
2. according to claim 1 process manganese ore waste water method it is characterised in that: the char-forming material in described step a
It is made up of following raw material: rice husk 8-14 part, timber 8-14 part, bentonite 6-12 part, kieselguhr 4-12 part, calcite 4-
8 parts, quartz sand 4-8 part, zeolite 2-8 part, gelatin 4-10 part.
3. according to claim 2 process manganese ore waste water method it is characterised in that: the preparation method of described char-forming material
For: by calcite and zeolite be crushed to after 220-260 mesh with bentonite, kieselguhr, quartz sand, mix homogeneously and obtain compound,
The wood particle that timber is cut into a diameter of 0.8-1cm is poured after being mixed with rice husk improves quality as wood particle and rice husk 5-7%
Diesel oil, igniting be fired into black wood charcoal after, put out by water with water and obtain carbon material, after proportionally compound being mixed homogeneously with carbon material, put
Enter to be crushed to 220-260 mesh in pulverizer, obtain mixed powder, after mixed powder is mixed with water according to mass ratio, add
Gelatin, obtains the char-forming material finished product for wastewater treatment finally by dried.
4. the method processing manganese ore waste water according to claim 3 it is characterised in that: the mixing of described compound and carbon material
Ratio ratio mixing for 1:1 according to mass ratio.
5. the method processing manganese ore waste water according to claim 3 it is characterised in that: described step mixed powder and water
Mass ratio is 1:1.
6. the method processing manganese ore waste water according to claim 1 it is characterised in that: described step b middle-ultraviolet lamp irradiates
The time processing is 8-16min, and irradiation distance is 12-18cm.
7. according to claim 3 process manganese ore waste water method it is characterised in that: the temperature of described dried is
60-70 DEG C, drying time is 20-30min.
8. according to claim 1 process manganese ore waste water method it is characterised in that: the strong oxidizer in described step b
For potassium permanganate.
9. according to claim 1 process manganese ore waste water method it is characterised in that: the stirring linear speed in described step b
Degree is controlled to 8-12m/s.
10. according to claim 1 process manganese ore waste water method it is characterised in that: the flocculant in described step d is
Iron sulfate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610729983.1A CN106365365B (en) | 2016-08-25 | 2016-08-25 | Method for treating manganese ore wastewater |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610729983.1A CN106365365B (en) | 2016-08-25 | 2016-08-25 | Method for treating manganese ore wastewater |
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| CN106365365A true CN106365365A (en) | 2017-02-01 |
| CN106365365B CN106365365B (en) | 2020-02-14 |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040188352A1 (en) * | 2003-03-28 | 2004-09-30 | Avijit Dey | Apparatus and method for continuous electrodeionization |
| CN104229957A (en) * | 2013-06-24 | 2014-12-24 | 张家领 | Compound flocculant taking natural minerals as main components |
| CN105236637A (en) * | 2015-10-10 | 2016-01-13 | 贵州万山兴隆锰业有限公司 | Manganese ore wastewater comprehensive treatment method |
| CN105706704A (en) * | 2016-03-02 | 2016-06-29 | 贵州闲草堂医药科技有限公司 | Method for cultivating rhizoma gastrodiae by taking carbonization material as rhizoma gastrodiae cultivating filler |
-
2016
- 2016-08-25 CN CN201610729983.1A patent/CN106365365B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040188352A1 (en) * | 2003-03-28 | 2004-09-30 | Avijit Dey | Apparatus and method for continuous electrodeionization |
| CN104229957A (en) * | 2013-06-24 | 2014-12-24 | 张家领 | Compound flocculant taking natural minerals as main components |
| CN105236637A (en) * | 2015-10-10 | 2016-01-13 | 贵州万山兴隆锰业有限公司 | Manganese ore wastewater comprehensive treatment method |
| CN105706704A (en) * | 2016-03-02 | 2016-06-29 | 贵州闲草堂医药科技有限公司 | Method for cultivating rhizoma gastrodiae by taking carbonization material as rhizoma gastrodiae cultivating filler |
Non-Patent Citations (1)
| Title |
|---|
| 张克荣等: ""活性炭对锰吸附作用的研究"", 《中国卫生检验杂志》 * |
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Effective date of registration: 20200713 Address after: 3 / F, building 2, economic development zone, Wanshan District, Tongren City, Guizhou Province Patentee after: Tongren Guizhou Hecheng Manganese Industry Co.,Ltd. Address before: Xi Xiang prosperous village Wanshan District 554200 in Guizhou province Tongren City Patentee before: GUIZHOU WANSHAN XINGLONG MANGANESE INDUSTRY Co.,Ltd. |
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Address after: 554299 floor 3, building 2, economic development zone, Wanshan District, Tongren City, Guizhou Province Patentee after: Guizhou Tongren Hecheng Manganese Alloy Co.,Ltd. Address before: 554299 floor 3, building 2, economic development zone, Wanshan District, Tongren City, Guizhou Province Patentee before: Tongren Guizhou Hecheng Manganese Industry Co.,Ltd. |
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