CN103161452B - Two-dimensional microscopic visualization simulation experiment device and using method thereof - Google Patents
Two-dimensional microscopic visualization simulation experiment device and using method thereof Download PDFInfo
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Abstract
Description
技术领域technical field
本发明涉及油田开发实验技术领域,尤其涉及二维微观可视化模拟实验装置及其使用方法。The invention relates to the technical field of oilfield development experiments, in particular to a two-dimensional microscopic visualization simulation experiment device and a use method thereof.
背景技术Background technique
二维微观可视化模拟实验是精确表征不同开发方式下油层多孔介质中的流体微观渗流特征,揭示不同开发方式的微观驱油机理的重要技术手段。随着注入流体越来越复杂(如:蒸汽、化学剂、凝析气体、非凝析气体等),以及注入的油藏对象越来越复杂,对于二维可视化微观模拟实验提出了新的要求,包括:1)能够表征微观仿真透明孔隙模型内流体的垂向渗流特征及驱油机理;2)能够表征任意倾角微观仿真透明孔隙模型内流体的平面渗流特征及驱油机理。The two-dimensional microscopic visualization simulation experiment is an important technical means to accurately characterize the microscopic seepage characteristics of fluid in the porous media of reservoirs under different development modes, and to reveal the microscopic oil displacement mechanism of different development modes. As the injected fluid becomes more and more complex (such as: steam, chemical agents, condensate gas, non-condensate gas, etc.), and the injected reservoir objects become more and more complex, new requirements are put forward for 2D visual microscopic simulation experiments , including: 1) It can characterize the vertical seepage characteristics and oil displacement mechanism of the fluid in the microscopically simulated transparent pore model; 2) It can characterize the planar seepage characteristics and oil displacement mechanism of the fluid in the microscopically simulated transparent pore model with any inclination angle.
专利CN201273903提出了一种高温高压微观实验夹持器,专利CN200985788提出了一种高温高压玻璃微观模型夹持器,该两个专利的优点均在于可以在较长时间、较高压力和较高温度下利用微观仿真透明孔隙模型进行二维微观可视化实验,并利用显微镜、摄像头、显示器和刻录机对微观渗流过程进行图像视频采集和后期处理分析。但专利CN201273903的不足之处在于,由于高温高压微观实验夹持器固定在显微镜底座上,因此夹持器不具备按任意倾角的旋转功能,只能用于水平微观仿真透明孔隙模型内的平面渗流模拟实验;而专利CN200985788的不足之处在于,仅说明了夹持器的模型床体底座与夹持器其它部件之间的结构关系,未说明夹持器是否具备任意倾角旋转功能及实现该功能的部件组成。以上两个专利的技术方案中均未详细说明采用何种技术手段来实现油层内流体的垂向渗流及任意倾角油层内流体的平面渗流模拟实验。Patent CN201273903 proposes a high-temperature and high-pressure microscopic experiment holder, and patent CN200985788 proposes a high-temperature and high-pressure glass microscopic model holder. Next, use the microscopic simulation transparent pore model to conduct two-dimensional microscopic visualization experiments, and use microscopes, cameras, displays and recorders to collect images and videos of the microscopic seepage process and post-processing analysis. However, the disadvantage of patent CN201273903 is that since the high-temperature and high-pressure microscopic experiment holder is fixed on the base of the microscope, the holder does not have the function of rotating at any inclination angle, and can only be used for horizontal microscopic simulation of planar seepage in transparent pore models Simulation experiment; and the disadvantage of patent CN200985788 is that it only illustrates the structural relationship between the model bed base of the clamper and other parts of the clamper, and does not explain whether the clamper has the function of rotating at any inclination angle and realizes this function components. The technical solutions of the above two patents do not specify which technical means are used to realize the vertical seepage of the fluid in the oil layer and the simulation experiment of the plane seepage of the fluid in the oil layer at any inclination angle.
发明内容Contents of the invention
本发明实施例提供一种二维微观可视化模拟实验装置,用以表征微观仿真透明孔隙模型内流体的垂向渗流特征及驱油机理,以及任意倾角微观仿真透明孔隙模型内流体的平面渗流特征及驱油机理,该装置包括:The embodiment of the present invention provides a two-dimensional microscopic visualization simulation experiment device, which is used to characterize the vertical seepage characteristics and oil displacement mechanism of the fluid in the microscopically simulated transparent pore model, and the planar seepage characteristics and characteristics of the fluid in the microscopically simulated transparent pore model with any inclination angle Oil displacement mechanism, the device includes:
成像系统、驱替系统和模型倾角控制系统;其中:Imaging system, displacement system and model dip angle control system; where:
成像系统包括:显微镜1、发光二极管LED强光源3、第一螺栓7、显微镜横梁8、立柱9、第一凹槽10、移动平台11和计算机16;驱替系统包括:高温高压微观实验夹持器2、回压阀17、驱替泵18和手动泵19;模型倾角控制系统包括:模型半圆形支架4、半圆形刻度盘5、模型底座6、第二螺栓12、第三螺栓13、第二凹槽14、第三凹槽15、滚珠轴承20;The imaging system includes: microscope 1, light-emitting diode LED strong light source 3, first bolt 7, microscope beam 8, column 9, first groove 10, mobile platform 11 and computer 16; the displacement system includes: high temperature and high pressure microscopic experiment clamping Device 2, back pressure valve 17, displacement pump 18 and manual pump 19; model inclination angle control system includes: model semicircle bracket 4, semicircle dial 5, model base 6, second bolt 12, third bolt 13 , the second groove 14, the third groove 15, the ball bearing 20;
显微镜1固定在显微镜横梁8上,显微镜横梁8通过第一凹槽10内能够滑动的第一螺栓7固定在立柱9上;显微镜1与计算机16通过数据线连接;立柱9垂直固定在移动平台11上;第一螺栓7通过在第一凹槽10内上下滑动并固定显微镜横梁8改变显微镜1的倾角;显微镜1位于高温高压微观实验夹持器2的第一侧,用于显示和摄录高温高压微观实验夹持器2内微观仿真透明孔隙模型内流体的流动过程;LED强光源3位于高温高压微观实验夹持器2的第二侧,用于向微观仿真透明孔隙模型提供光源;计算机16用于存储显微镜1拍摄到的图像、视频以及驱替泵18、手动泵19和回压阀17的压力和流量数据;The microscope 1 is fixed on the microscope beam 8, and the microscope beam 8 is fixed on the column 9 through the first bolt 7 that can slide in the first groove 10; the microscope 1 is connected with the computer 16 through a data line; the column 9 is vertically fixed on the mobile platform 11 Upper; the first bolt 7 changes the tilt angle of the microscope 1 by sliding up and down in the first groove 10 and fixing the microscope beam 8; The flow process of the fluid in the microscopically simulated transparent pore model in the high-pressure microscopic experiment holder 2; the LED strong light source 3 is located on the second side of the high-temperature and high-pressure microscopic experiment holder 2, and is used to provide light source for the microscopically simulated transparent pore model; the computer 16 It is used to store the images and videos taken by the microscope 1, as well as the pressure and flow data of the displacement pump 18, the manual pump 19 and the back pressure valve 17;
回压阀17、驱替泵18和手动泵19通过管线连接到高温高压微观实验夹持器2;高温高压微观实验夹持器2采用电加热保持恒温,腔体内水平方向密封固定微观仿真透明孔隙模型;微观仿真透明孔隙模型上下用高压钢化透明玻璃密封,沿对角线设置入口和出口,与高温高压微观实验夹持器2的入口和出口形成密封通道;驱替泵18用于向微观仿真透明孔隙模型中注入驱替剂;手动泵19用于为高温高压微观实验夹持器2提供围压;回压阀17用于控制微观仿真透明孔隙模型的回压;The back pressure valve 17, the displacement pump 18 and the manual pump 19 are connected to the high-temperature and high-pressure microscopic experiment holder 2 through pipelines; the high-temperature and high-pressure microscopic experiment holder 2 adopts electric heating to maintain a constant temperature, and the horizontal direction of the chamber is sealed and fixed to simulate transparent microscopic pores Model; the microscopic simulation transparent pore model is sealed with high-pressure toughened transparent glass up and down, and the inlet and outlet are arranged along the diagonal to form a sealed channel with the inlet and outlet of the high-temperature and high-pressure microscopic experiment holder 2; the displacement pump 18 is used for microscopic simulation. The displacing agent is injected into the transparent pore model; the manual pump 19 is used to provide confining pressure for the high temperature and high pressure microscopic experiment holder 2; the back pressure valve 17 is used to control the back pressure of the microscopically simulated transparent pore model;
高温高压微观实验夹持器2和LED强光源3固定于模型半圆形支架4内;模型半圆形支架4的第一侧设半圆形的第二凹槽14,半圆形刻度盘5的第一侧设半圆形的第三凹槽15,模型半圆形支架4的第一侧与半圆形刻度盘5的第一侧为同侧;第二凹槽14中左右两侧对称设有两个能够沿第二凹槽14滑动的第二螺栓12,第三凹槽15中左右两侧对称设有两个能够沿着第三凹槽15滑动的第三螺栓13;模型半圆形支架4通过第二螺栓12固定在模型底座6上,半圆形刻度盘5通过第三螺栓13固定在模型底座6上;模型半圆形支架4与半圆形刻度盘5为同轴的半圆形轴体,模型半圆形支架4与半圆形刻度盘5之间通过接触的缝隙中滚珠轴承20相连接。The high temperature and high pressure microscopic experiment holder 2 and the LED strong light source 3 are fixed in the model semicircle support 4; The first side of the semicircle is provided with the third semicircular groove 15, and the first side of the model semicircular support 4 and the first side of the semicircular dial 5 are the same side; the left and right sides are symmetrical in the second groove 14 There are two second bolts 12 that can slide along the second groove 14, and two third bolts 13 that can slide along the third groove 15 are symmetrically arranged on the left and right sides of the third groove 15; the model semicircle The shape support 4 is fixed on the model base 6 by the second bolt 12, and the semicircle dial 5 is fixed on the model base 6 by the third bolt 13; the model semicircle support 4 and the semicircle dial 5 are coaxial The semicircular shaft body, the model semicircular bracket 4 and the semicircular dial 5 are connected by ball bearings 20 in the contact gap.
一个实施例中,模型半圆形支架4旋转90°时,高温高压微观实验夹持器2内的微观仿真透明孔隙模型为垂直竖立。In one embodiment, when the model semicircular support 4 is rotated by 90°, the microscopic simulation transparent pore model in the high temperature and high pressure microscopic experiment holder 2 is vertically erected.
一个实施例中,模型半圆形支架4的第二侧设有零刻度线,以记录并校准模型半圆形支架4水平放置时的位置。In one embodiment, a zero scale line is provided on the second side of the model semicircle support 4 to record and calibrate the position of the model semicircle support 4 when it is placed horizontally.
一个实施例中,半圆形刻度盘5的第二侧左右两端均匀分布0°~90°之间的刻度线,用于指示在模型半圆形支架4旋转过程中,模型半圆形支架4的零刻度线指向的半圆形刻度盘5的刻度为高温高压微观实验夹持器2旋转的倾角。In one embodiment, the second side left and right ends of the semicircular dial 5 are evenly distributed with scale lines between 0° and 90°, which are used to indicate that during the rotation of the model semicircle support 4, the model semicircle support The scale of the semicircular dial 5 pointed to by the zero scale line of 4 is the inclination angle of the rotation of the high temperature and high pressure microscopic experiment holder 2 .
本发明实施例还提供一种上述二维微观可视化模拟实验装置的使用方法,用以表征微观仿真透明孔隙模型内流体的垂向渗流特征及驱油机理,以及任意倾角微观仿真透明孔隙模型内流体的平面渗流特征及驱油机理,该方法包括:The embodiment of the present invention also provides a method of using the above-mentioned two-dimensional microscopic visualization simulation experiment device, which is used to characterize the vertical seepage characteristics and oil displacement mechanism of the fluid in the microscopically simulated transparent pore model, and the fluid in the microscopically simulated transparent pore model with any inclination angle The plane seepage characteristics and oil displacement mechanism, the method includes:
松开第二螺栓12,逆时针旋转模型半圆形支架4直至模型半圆形支架4上的零刻度线指向油层实际倾角在半圆形刻度盘5的刻度线位置后,拧紧第二螺栓12将模型半圆形支架4固定在模型底座6上;Loosen the second bolt 12, rotate the model semicircle support 4 counterclockwise until the zero scale line on the model semicircle support 4 points to the position where the actual inclination of the oil layer is at the scale line of the semicircle dial 5, then tighten the second bolt 12 The model semicircular support 4 is fixed on the model base 6;
松开第一螺栓7、沿第一凹槽10向下滑动显微镜横梁8,直到显微镜1的物镜与高温高压微观实验夹持器2顶部的高压玻璃视窗平行时,拧紧第一螺栓7将显微镜横梁8固定在立柱9上;Loosen the first bolt 7, slide the microscope beam 8 down along the first groove 10, until the objective lens of the microscope 1 is parallel to the high-pressure glass window on the top of the high-temperature and high-pressure microscopic experiment holder 2, tighten the first bolt 7 to lock the microscope beam 8 is fixed on the column 9;
建立起微观仿真透明孔隙模型的围压并对微观仿真透明孔隙模型进行升温处理;Establish the confining pressure of the microscopic simulation transparent pore model and heat up the microscopic simulation transparent pore model;
利用驱替泵18将配制好的地层水从高温高压微观实验夹持器2的入口注入微观仿真透明孔隙模型;同时,打开LED强光源3并调节其亮度,直到在显微镜1的物镜中观测到微观仿真透明孔隙模型中的流体流动;Use the displacement pump 18 to inject the prepared formation water from the entrance of the high-temperature and high-pressure microscopic experiment holder 2 into the microscopic simulation transparent pore model; at the same time, turn on the LED strong light source 3 and adjust its brightness until it is observed in the objective lens of the microscope 1 Microscopic simulation of fluid flow in transparent pore models;
利用驱替泵18将配制好的地层油从高温高压微观实验夹持器2的入口注入微观仿真透明孔隙模型,直到出口含水为0%时,停止注入,建立起微观仿真透明孔隙模型的束缚水饱和度;Use the displacement pump 18 to inject the prepared formation oil from the inlet of the high-temperature and high-pressure micro-experiment holder 2 into the micro-simulation transparent pore model until the outlet water content is 0%, stop the injection, and establish the bound water of the micro-simulation transparent pore model saturation;
利用驱替泵18将氮气从高温高压微观实验夹持器2的入口注入微观仿真透明孔隙模型,利用显微镜1连续观测微观仿真透明孔隙模型内氮气气泡的流变特征及驱油特征,并用计算机16连续录像。Use the displacement pump 18 to inject nitrogen gas from the inlet of the high-temperature and high-pressure microscopic experiment holder 2 into the microscopic simulation transparent pore model, use the microscope 1 to continuously observe the rheological characteristics and oil displacement characteristics of the nitrogen gas bubbles in the microscopic simulation transparent pore model, and use the computer 16 Continuous recording.
一个实施例中,建立起微观仿真透明孔隙模型的围压,包括:In one embodiment, the confining pressure of the microscopically simulated transparent pore model is established, including:
利用手动泵19向密封有微观仿真透明孔隙模型的高温高压微观实验夹持器2中注入高透明度的乙二醇,注入速度3ml/min,直到压力达到8.5MPa,建立起模型围压。Use the manual pump 19 to inject high-transparency ethylene glycol into the high-temperature and high-pressure micro-experiment holder 2 sealed with a micro-simulated transparent pore model, at an injection rate of 3ml/min, until the pressure reaches 8.5 MPa, and the model confining pressure is established.
一个实施例中,对微观仿真透明孔隙模型进行升温处理,包括:In one embodiment, the microscopically simulated transparent pore model is subjected to heating treatment, including:
利用高温高压微观实验夹持器2的电加热套,将高温高压微观实验夹持器2加热到预定温度45℃。The electric heating jacket of the high temperature and high pressure microscopic experiment holder 2 is used to heat the high temperature and high pressure microscopic experiment holder 2 to a predetermined temperature of 45°C.
一个实施例中,利用驱替泵18将配制好的地层水和地层油从高温高压微观实验夹持器2的入口注入微观仿真透明孔隙模型时,注入压力8MPa,高温高压微观实验夹持器2的出口回压控制在7.7MPa。In one embodiment, when using the displacement pump 18 to inject the prepared formation water and formation oil from the entrance of the high-temperature and high-pressure microscopic experiment holder 2 into the microscopic simulation transparent pore model, the injection pressure is 8 MPa, and the high-temperature and high-pressure microscopic experiment holder 2 The outlet back pressure is controlled at 7.7MPa.
一个实施例中,利用驱替泵18将氮气从高温高压微观实验夹持器2的入口注入微观仿真透明孔隙模型时,注入压力8MPa,高温高压微观实验夹持器2的出口回压控制在7.7MPa,注入速度0.05ml/min。In one embodiment, when using the displacement pump 18 to inject nitrogen gas from the inlet of the high-temperature and high-pressure microscopic experiment holder 2 into the microscopic simulation transparent pore model, the injection pressure is 8 MPa, and the outlet back pressure of the high-temperature and high-pressure microscopic experiment holder 2 is controlled at 7.7 MPa, injection speed 0.05ml/min.
一个实施例中,模型半圆形支架4旋转90°时,通过从微观仿真透明孔隙模型的顶部入口注入、底部出口采出,模拟微观仿真透明孔隙模型内流体的垂向渗流特征。In one embodiment, when the model semicircular support 4 is rotated by 90°, the vertical seepage characteristics of the fluid in the microscopically simulated transparent pore model are simulated by injecting from the top inlet of the microscopically simulated transparent pore model and extracting from the bottom outlet.
本发明实施例的二维微观可视化模拟实验装置能够完成模仿地层高温高压条件下的微观仿真透明孔隙模型内流体的垂向渗流实验,以及任意倾角微观仿真透明孔隙模型内流体的平面渗流实验;可用于表征微观仿真透明孔隙模型内流体的垂向渗流特征及驱油机理,以及任意倾角微观仿真透明孔隙模型内流体的平面渗流特征及驱油机理。The two-dimensional microscopic visualization simulation experiment device of the embodiment of the present invention can complete the vertical seepage experiment of the fluid in the microscopic simulation transparent pore model imitating the high temperature and high pressure of the formation, and the plane seepage experiment of the fluid in the microscopic simulation transparent pore model of any inclination angle; available It is used to characterize the vertical seepage characteristics and oil displacement mechanism of the fluid in the microscopically simulated transparent pore model, and the planar seepage characteristics and oil displacement mechanism of the fluid in the microscopically simulated transparent pore model at any inclination angle.
附图说明Description of drawings
为了更清楚地说明本发明实施例中的技术方案,下面将对实施例描述中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本发明的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其他的附图。在附图中:In order to more clearly illustrate the technical solutions in the embodiments of the present invention, the drawings that need to be used in the description of the embodiments will be briefly introduced below. Obviously, the drawings in the following description are only some embodiments of the present invention. For those skilled in the art, other drawings can also be obtained based on these drawings without creative effort. In the attached picture:
图1为本发明实施例中二维微观可视化模拟实验装置的结构示意图;Fig. 1 is the structural representation of the two-dimensional microscopic visualization simulation experiment device in the embodiment of the present invention;
图2为本发明实施例中二维微观可视化模拟实验装置的具体实例的结构示意图;Fig. 2 is the structural schematic diagram of the specific example of two-dimensional microscopic visualization simulation experiment device in the embodiment of the present invention;
图3为本发明实施例中二维微观可视化模拟实验装置模拟油层倾角为7°条件下的结构示意图。Fig. 3 is a schematic diagram of the structure of the two-dimensional microscopic visualization simulation experiment device in the embodiment of the present invention under the condition that the simulated oil layer dip angle is 7°.
具体实施方式Detailed ways
为使本发明实施例的目的、技术方案和优点更加清楚明白,下面结合附图对本发明实施例做进一步详细说明。在此,本发明的示意性实施例及其说明用于解释本发明,但并不作为对本发明的限定。In order to make the purpose, technical solutions and advantages of the embodiments of the present invention more clear, the embodiments of the present invention will be further described in detail below in conjunction with the accompanying drawings. Here, the exemplary embodiments and descriptions of the present invention are used to explain the present invention, but not to limit the present invention.
为了解决现有装置无法完成微观仿真透明孔隙模型内流体的垂向渗流及任意倾角微观仿真透明孔隙模型内流体的平面渗流模拟实验的技术问题,本发明实施例提供一种二维微观可视化模拟实验装置及其使用方法。In order to solve the technical problem that the existing device cannot complete the vertical seepage simulation experiment of the fluid in the microscopic simulation transparent pore model and the plane seepage simulation experiment of the fluid in the microscopic simulation transparent pore model at any inclination angle, the embodiment of the present invention provides a two-dimensional microscopic visualization simulation experiment Device and method of use thereof.
图1为本发明实施例中二维微观可视化模拟实验装置的结构示意图。如图1所示,本发明实施例中二维微观可视化模拟实验装置可以包括:FIG. 1 is a schematic structural diagram of a two-dimensional microscopic visualization simulation experiment device in an embodiment of the present invention. As shown in Figure 1, the two-dimensional microscopic visualization simulation experiment device in the embodiment of the present invention may include:
成像系统、驱替系统和模型倾角控制系统;其中:Imaging system, displacement system and model dip angle control system; where:
成像系统包括:显微镜1、LED(LightEmittingDiode,发光二极管)强光源3、第一螺栓7、显微镜横梁8、立柱9、第一凹槽10、移动平台11和计算机16;驱替系统包括:高温高压微观实验夹持器2、回压阀17、驱替泵18和手动泵19;模型倾角控制系统包括:模型半圆形支架4、半圆形刻度盘5、模型底座6、第二螺栓12、第三螺栓13、第二凹槽14、第三凹槽15、滚珠轴承20;The imaging system includes: microscope 1, LED (Light Emitting Diode, light emitting diode) strong light source 3, first bolt 7, microscope beam 8, column 9, first groove 10, mobile platform 11 and computer 16; the displacement system includes: high temperature and high pressure Microscopic experiment holder 2, back pressure valve 17, displacement pump 18 and manual pump 19; model inclination angle control system includes: model semicircle support 4, semicircle dial 5, model base 6, second bolt 12, The third bolt 13, the second groove 14, the third groove 15, the ball bearing 20;
显微镜1固定在显微镜横梁8上,显微镜横梁8通过第一凹槽10内可滑动的第一螺栓7固定在立柱9上;显微镜1与计算机16通过数据线连接;立柱9垂直固定在移动平台11上;第一螺栓7通过在第一凹槽10内上下滑动并固定显微镜横梁8,可沿任意角度改变显微镜1的倾斜角;显微镜1位于高温高压微观实验夹持器2的第一侧,用于显示和摄录高温高压微观实验夹持器2内微观仿真透明孔隙模型内流体的流动过程;LED强光源3设于高温高压微观实验夹持器2的第二侧,用于向微观仿真透明孔隙模型提供光源;计算机16用于存储显微镜1拍摄到的图像、视频以及驱替泵18、手动泵19和回压阀17的压力、流量数据;The microscope 1 is fixed on the microscope beam 8, and the microscope beam 8 is fixed on the column 9 through the slidable first bolt 7 in the first groove 10; the microscope 1 is connected with the computer 16 through a data line; the column 9 is vertically fixed on the mobile platform 11 Above; the first bolt 7 slides up and down in the first groove 10 and fixes the microscope beam 8, so that the inclination angle of the microscope 1 can be changed along any angle; the microscope 1 is located on the first side of the high temperature and high pressure microscopic experiment holder 2, and is It is used to display and record the flow process of the fluid in the microscopic simulation transparent pore model in the high-temperature and high-pressure microscopic experiment holder 2; the LED strong light source 3 is arranged on the second side of the high-temperature and high-pressure microscopic experiment holder 2, and is used to be transparent to the microscopic simulation. The pore model provides a light source; the computer 16 is used to store the images and videos taken by the microscope 1, and the pressure and flow data of the displacement pump 18, the manual pump 19 and the back pressure valve 17;
回压阀17、驱替泵18和手动泵19通过管线连接到高温高压微观实验夹持器2,高温高压微观实验夹持器2采用电加热保持恒温,高温高压微观实验夹持器2腔体内水平方向密封固定有微观仿真透明孔隙模型,微观仿真透明孔隙模型上下用高压钢化透明玻璃密封,微观仿真透明孔隙模型沿对角线设置入口和出口,并与高温高压微观实验夹持器2的入口和出口形成密封通道;驱替泵18用于向微观仿真透明孔隙模型中注入驱替剂;手动泵19用于为高温高压微观实验夹持器提供围压;回压阀17用于控制微观仿真透明孔隙模型的回压;The back pressure valve 17, the displacement pump 18 and the manual pump 19 are connected to the high temperature and high pressure microscopic experiment holder 2 through pipelines. The horizontal direction is sealed and fixed with a microscopic simulation transparent pore model. The upper and lower parts of the microscopic simulation transparent pore model are sealed with high-pressure tempered transparent glass. and the outlet to form a sealed channel; the displacement pump 18 is used to inject the displacing agent into the transparent pore model of the microscopic simulation; the manual pump 19 is used to provide confining pressure for the high temperature and high pressure microscopic experiment holder; the back pressure valve 17 is used to control the microscopic simulation Backpressure for transparent pore models;
高温高压微观实验夹持器2和LED强光源3固定于模型半圆形支架4内;模型半圆形支架4的第一侧设半圆形的第二凹槽14,半圆形刻度盘5的第一侧设半圆形的第三凹槽15,模型半圆形支架4的第一侧与半圆形刻度盘5的第一侧为同侧;模型半圆形支架4的第二凹槽14中左右两侧对称分布两个能够沿着第二凹槽14滑动的第二螺栓12,半圆形刻度盘5的第三凹槽15中左右两侧对称分布两个能够沿着第三凹槽15滑动的第三螺栓13;模型半圆形支架4通过第二凹槽14中的第二螺栓12固定在模型底座6上,半圆形刻度盘5通过第三凹槽15中的第三螺栓13固定在模型底座6上;模型半圆形支架4与半圆形刻度盘5为同轴的半圆形轴体,模型半圆形支架4与半圆形刻度盘5之间通过接触的缝隙中滚珠轴承20相连接。The high temperature and high pressure microscopic experiment holder 2 and the LED strong light source 3 are fixed in the model semicircle support 4; The first side of the semicircle is provided with the third groove 15 of the semicircle, and the first side of the model semicircle support 4 is the same side as the first side of the semicircle dial 5; the second recess of the model semicircle support 4 In the groove 14, two left and right sides are symmetrically distributed and two second bolts 12 that can slide along the second groove 14 are distributed, and in the third groove 15 of the semicircular dial 5, two left and right sides are symmetrically distributed and can be moved along the third bolt 12. The third bolt 13 of the groove 15 sliding; the model semicircle support 4 is fixed on the model base 6 by the second bolt 12 in the second groove 14, and the semicircle dial 5 passes through the first bolt 12 in the third groove 15 Three bolts 13 are fixed on the model base 6; the model semicircle support 4 and the semicircle dial 5 are coaxial semicircle shafts, and the model semicircle support 4 and the semicircle dial 5 are contacted The ball bearing 20 is connected in the gap.
具体实施时,模型半圆形支架4的第二侧可设有零刻度线,以记录并校准模型半圆形支架4水平放置时的位置。During specific implementation, a zero scale line can be provided on the second side of the model semicircle support 4 to record and calibrate the position of the model semicircle support 4 when it is placed horizontally.
具体实施时,半圆形刻度盘5的第二侧左右两端可均匀分布0°~90°之间的刻度线,用于指示在模型半圆形支架4旋转过程中,模型半圆形支架4的零刻度线指向的半圆形刻度盘5的刻度为高温高压微观实验夹持器2旋转的倾角。During specific implementation, the second side left and right ends of the semicircle dial 5 can evenly distribute the scale lines between 0 ° ~ 90 °, which is used to indicate that the model semicircle support 4 rotates during the rotation process of the model semicircle support. The scale of the semicircular dial 5 pointed to by the zero scale line of 4 is the inclination angle of the rotation of the high temperature and high pressure microscopic experiment holder 2 .
图2为本发明实施例中二维微观可视化模拟实验装置的具体实例的结构示意图。在图2中示出了模型半圆形支架4第二侧的零刻度线,以及半圆形刻度盘5第二侧左右两端均匀分布的0°~90°之间的刻度线。FIG. 2 is a schematic structural diagram of a specific example of a two-dimensional microscopic visualization simulation experiment device in an embodiment of the present invention. 2 shows the zero scale line on the second side of the semicircular support 4 of the model, and the scale lines between 0° and 90° evenly distributed at the left and right ends of the second side of the semicircular dial 5 .
具体实施时,模型半圆形支架4旋转90°时,高温高压微观实验夹持器2内的微观仿真透明孔隙模型为垂直竖立,通过从微观仿真透明孔隙模型的顶部入口注入、底部出口采出,可模拟微观仿真透明孔隙模型内流体的垂向渗流特征。During specific implementation, when the model semicircular support 4 rotates 90°, the microscopic simulation transparent pore model in the high-temperature and high-pressure microscopic experiment holder 2 is vertically erected, and is injected from the top inlet of the microscopic simulation transparent pore model and extracted from the bottom outlet. , which can simulate the vertical seepage characteristics of the fluid in the microscopic simulation transparent pore model.
本发明实施例中二维微观可视化模拟实验装置的使用方法可以包括:The method for using the two-dimensional microscopic visualization simulation experiment device in the embodiment of the present invention may include:
1、设置模型倾角:1. Set the model inclination:
松开第二螺栓12,逆时针旋转模型半圆形支架4直至模型半圆形支架4上的零刻度线指向油层实际倾角在半圆形刻度盘5的刻度线位置后,拧紧第二螺栓12将模型半圆形支架4固定在模型底座6上;Loosen the second bolt 12, rotate the model semicircle support 4 counterclockwise until the zero scale line on the model semicircle support 4 points to the position where the actual inclination of the oil layer is at the scale line of the semicircle dial 5, then tighten the second bolt 12 The model semicircular support 4 is fixed on the model base 6;
2、设置显微镜倾角:2. Set the tilt angle of the microscope:
松开第一螺栓7、沿第一凹槽10向下滑动显微镜横梁8,直到显微镜1的物镜与高温高压微观实验夹持器2顶部的高压玻璃视窗平行时,拧紧第一螺栓7将显微镜横梁8固定在立柱9上;Loosen the first bolt 7, slide the microscope beam 8 down along the first groove 10, until the objective lens of the microscope 1 is parallel to the high-pressure glass window on the top of the high-temperature and high-pressure microscopic experiment holder 2, tighten the first bolt 7 to lock the microscope beam 8 is fixed on the column 9;
3、建立模型围压及控制模型升温:3. Establish model confining pressure and control model temperature rise:
建立起微观仿真透明孔隙模型的围压并对微观仿真透明孔隙模型进行升温处理;其中,建立起微观仿真透明孔隙模型的围压,例如可以包括:利用手动泵19向密封有微观仿真透明孔隙模型的高温高压微观实验夹持器2中注入高透明度的乙二醇,注入速度3ml/min,直到压力达到8.5MPa,从而建立起模型围压;对微观仿真透明孔隙模型进行升温处理,例如可以包括:利用高温高压微观实验夹持器2的电加热套,将高温高压微观实验夹持器2加热到预定温度45℃;前例中涉及的注入物质、注入速度、压力、预定温度可以根据实际需求进行调整;Establish the confining pressure of the microscopically simulated transparent pore model and heat up the microscopically simulated transparent pore model; wherein, establishing the confining pressure of the microscopically simulated transparent pore model may include, for example: using a manual pump 19 to seal the microscopically simulated transparent pore model Inject high-transparency ethylene glycol into the high-temperature and high-pressure micro-experiment holder 2 at an injection rate of 3ml/min until the pressure reaches 8.5MPa, thereby establishing the model confining pressure; heat-up the micro-simulation transparent pore model, for example, it may include : Use the electric heating jacket of the high-temperature and high-pressure microscopic experiment holder 2 to heat the high-temperature and high-pressure microscopic experiment holder 2 to a predetermined temperature of 45°C; the injection material, injection speed, pressure, and predetermined temperature involved in the previous example can be carried out according to actual needs Adjustment;
4、饱和水处理:4. Saturated water treatment:
利用驱替泵18将配制好的地层水从高温高压微观实验夹持器2的入口注入微观仿真透明孔隙模型;同时,打开LED强光源3并调节其亮度,直到在显微镜1的物镜中观测到微观仿真透明孔隙模型中的流体流动;其中,地层水注入压力可以是8MPa,高温高压微观实验夹持器2的出口回压可以控制在7.7MPa;该注入压力、出口回压可以根据实际需求进行调整;Use the displacement pump 18 to inject the prepared formation water from the entrance of the high-temperature and high-pressure microscopic experiment holder 2 into the microscopic simulation transparent pore model; at the same time, turn on the LED strong light source 3 and adjust its brightness until it is observed in the objective lens of the microscope 1 Microscopically simulate the fluid flow in the transparent pore model; among them, the formation water injection pressure can be 8MPa, and the outlet backpressure of the high-temperature and high-pressure microscopic experiment holder 2 can be controlled at 7.7MPa; the injection pressure and outlet backpressure can be adjusted according to actual needs Adjustment;
5、饱和油处理:5. Saturated oil treatment:
利用驱替泵18将配制好的地层油从高温高压微观实验夹持器2的入口注入微观仿真透明孔隙模型,直到出口含水为0%时,停止注入,建立起微观仿真透明孔隙模型的束缚水饱和度;其中,地层油注入压力可以是8MPa,高温高压微观实验夹持器2的出口回压可以控制在7.7MPa;该注入压力、出口回压可以根据实际需求进行调整;Use the displacement pump 18 to inject the prepared formation oil from the inlet of the high-temperature and high-pressure micro-experiment holder 2 into the micro-simulation transparent pore model until the outlet water content is 0%, stop the injection, and establish the bound water of the micro-simulation transparent pore model Saturation; among them, the formation oil injection pressure can be 8MPa, and the outlet back pressure of the high temperature and high pressure microscopic experiment holder 2 can be controlled at 7.7MPa; the injection pressure and outlet back pressure can be adjusted according to actual needs;
6、氮气驱油:6. Nitrogen flooding:
利用驱替泵18将氮气从高温高压微观实验夹持器2的入口注入微观仿真透明孔隙模型,利用显微镜1连续观测微观仿真透明孔隙模型内氮气气泡的流变特征及驱油特征,并用计算机16连续录像;其中,氮气注入压力可以是8MPa,高温高压微观实验夹持器2的出口回压可以控制在7.7MPa,注入速度可以是0.05ml/min;该注入压力、出口回压、注入速度可以根据实际需求进行调整。Use the displacement pump 18 to inject nitrogen gas from the inlet of the high-temperature and high-pressure microscopic experiment holder 2 into the microscopic simulation transparent pore model, use the microscope 1 to continuously observe the rheological characteristics and oil displacement characteristics of the nitrogen gas bubbles in the microscopic simulation transparent pore model, and use the computer 16 Continuous video recording; wherein, the nitrogen injection pressure can be 8MPa, the outlet back pressure of the high temperature and high pressure microscopic experiment holder 2 can be controlled at 7.7MPa, and the injection speed can be 0.05ml/min; the injection pressure, outlet back pressure, and injection speed can be Adjust according to actual needs.
具体实施时,本发明实施例中二维微观可视化模拟实验装置的使用方法还可以包括:模型半圆形支架4旋转90°时,通过从微观仿真透明孔隙模型的顶部入口注入、底部出口采出,可以模拟微观仿真透明孔隙模型内流体的垂向渗流特征。During specific implementation, the use method of the two-dimensional microscopic visualization simulation experiment device in the embodiment of the present invention may also include: when the model semicircular support 4 is rotated 90°, injecting from the top inlet of the transparent pore model of the microscopic simulation, and extracting from the bottom outlet , which can simulate the vertical seepage characteristics of the fluid in the micro-simulation transparent pore model.
下面举一例说明使用本发明实施例的二维微观可视化模拟实验装置的具体实验过程。本例中二维微观可视化模拟实验装置模拟油层倾角为7°,具体实施时也可以为其它倾角度数,实验过程与此类似。An example is given below to illustrate the specific experimental process of using the two-dimensional microscopic visualization simulation experimental device of the embodiment of the present invention. In this example, the two-dimensional microscopic visualization simulation experiment device simulates the dip angle of the oil layer as 7°, and other dip angles can also be used in actual implementation, and the experimental process is similar to this.
图3为本例中二维微观可视化模拟实验装置模拟油层倾角为7°条件下的结构示意图。如图3所示,具体实验过程可以包括:Fig. 3 is a schematic diagram of the structure of the two-dimensional microscopic visualization simulation experiment device in this example under the condition that the simulated oil layer dip angle is 7°. As shown in Figure 3, the specific experimental process may include:
1、设置模型倾角:1. Set the model inclination:
根据油层实际倾角为7°,松开第二螺栓12,逆时针旋转模型半圆形支架4直到模型半圆形支架4上的零刻度线指向半圆形刻度盘5的7°刻度线位置后,拧紧第二螺栓12将模型半圆形支架4固定在模型底座6上;According to the actual inclination angle of the oil layer is 7°, loosen the second bolt 12, and rotate the model semicircle support 4 counterclockwise until the zero scale line on the model semicircle support 4 points to the 7° scale line position of the semicircle dial 5 , tighten the second bolt 12 to fix the model semicircular bracket 4 on the model base 6;
2、设置显微镜倾角:2. Set the tilt angle of the microscope:
松开第一螺栓7、沿第一凹槽10向下滑动显微镜横梁8,直到显微镜1的物镜与高温高压微观实验夹持器2顶部的高压玻璃视窗平行时,拧紧第一螺栓7将显微镜横梁8固定在立柱9上;Loosen the first bolt 7, slide the microscope beam 8 down along the first groove 10, until the objective lens of the microscope 1 is parallel to the high-pressure glass window on the top of the high-temperature and high-pressure microscopic experiment holder 2, tighten the first bolt 7 to lock the microscope beam 8 is fixed on the column 9;
3、建立模型围压及控制模型升温:3. Establish model confining pressure and control model temperature rise:
利用手动泵19向密封有微观仿真透明孔隙模型的高温高压微观实验夹持器2中注入高透明度的乙二醇,注入速度3ml/min,直到压力达到8.5MPa,建立起模型围压;利用高温高压微观实验夹持器2的电加热套,将高温高压微观实验夹持器2加热到预定温度45℃;Utilize the hand pump 19 to inject high-transparency ethylene glycol into the high-temperature and high-pressure micro-experiment holder 2 sealed with a micro-simulation transparent pore model, at an injection rate of 3ml/min, until the pressure reaches 8.5MPa, and the model confining pressure is established; The electric heating jacket of the high-pressure micro-experiment holder 2 heats the high-temperature and high-pressure micro-experiment holder 2 to a predetermined temperature of 45°C;
4、饱和水处理:4. Saturated water treatment:
利用驱替泵18将配制好的地层水从高温高压微观实验夹持器2的入口注入微观仿真透明孔隙模型,注入压力8MPa,高温高压微观实验夹持器2的出口回压控制在7.7MPa;同时,打开LED强光源3并调节其亮度,直到在显微镜1的物镜中能清晰观测到微观仿真透明孔隙模型中的流体流动;Use the displacement pump 18 to inject the prepared formation water from the inlet of the high-temperature and high-pressure micro-experiment holder 2 into the microscopic simulation transparent pore model, the injection pressure is 8 MPa, and the outlet back pressure of the high-temperature and high-pressure micro-experiment holder 2 is controlled at 7.7 MPa; At the same time, turn on the LED strong light source 3 and adjust its brightness until the fluid flow in the microscopically simulated transparent pore model can be clearly observed in the objective lens of the microscope 1;
5、饱和油处理:5. Saturated oil treatment:
利用驱替泵18将配制好的地层油从高温高压微观实验夹持器2的入口注入微观仿真透明孔隙模型,注入压力8MPa,高温高压微观实验夹持器2的出口回压控制在7.7MPa,直到出口含水为0%时,停止注入,建立起微观仿真透明孔隙模型的束缚水饱和度;Use the displacement pump 18 to inject the prepared formation oil from the inlet of the high-temperature and high-pressure micro-experiment holder 2 into the microscopic simulation transparent pore model, the injection pressure is 8 MPa, and the outlet back pressure of the high-temperature and high-pressure micro-experiment holder 2 is controlled at 7.7 MPa, When the outlet water content is 0%, the injection is stopped, and the irreducible water saturation of the microscopically simulated transparent pore model is established;
6、氮气驱油:6. Nitrogen flooding:
利用驱替泵18将氮气从高温高压微观实验夹持器2的入口注入微观仿真透明孔隙模型,注入压力8MPa,高温高压微观实验夹持器2的出口回压控制在7.7MPa,注入速度0.05ml/min,利用显微镜1连续观测微观仿真透明孔隙模型内氮气气泡的流变特征及驱油特征,并用计算机16连续录像。Use the displacement pump 18 to inject nitrogen gas from the inlet of the high-temperature and high-pressure microscopic experiment holder 2 into the microscopic simulation transparent pore model, the injection pressure is 8MPa, the outlet back pressure of the high-temperature and high-pressure microscopic experiment holder 2 is controlled at 7.7MPa, and the injection speed is 0.05ml /min, use the microscope 1 to continuously observe the rheological characteristics and oil displacement characteristics of the nitrogen bubbles in the microscopically simulated transparent pore model, and use the computer 16 to record continuously.
实施时在氮气驱油过程中通过显微镜1拍摄到二维微观模拟实验图像,通过分析不同时刻拍摄到的图像或视频,可得到不同孔隙尺寸条件下氮气的微观驱油特征,以及剩余油的分布规律。During the implementation, the two-dimensional microscopic simulation experiment images were taken by microscope 1 during the nitrogen flooding process. By analyzing the images or videos taken at different times, the microcosmic oil flooding characteristics of nitrogen under different pore sizes and the distribution of remaining oil can be obtained. law.
综上所述,本发明实施例的二维微观可视化模拟实验装置能够完成模仿地层高温高压条件下的微观仿真透明孔隙模型内流体的垂向渗流实验,以及任意倾角微观仿真透明孔隙模型内流体的平面渗流实验;可用于表征微观仿真透明孔隙模型内流体的垂向渗流特征及驱油机理,以及任意倾角微观仿真透明孔隙模型内流体的平面渗流特征及驱油机理。同时,可以对比顶部注入和底部注入的渗流特征差异,分析不同油层倾角对孔隙介质中流体渗流特征的影响规律。In summary, the two-dimensional microscopic visualization simulation experiment device of the embodiment of the present invention can complete the vertical seepage experiment of the fluid in the microscopic simulation transparent pore model imitating the high temperature and high pressure of the formation, and the microscopic simulation of the fluid in the transparent pore model at any inclination angle. Plane seepage experiment: it can be used to characterize the vertical seepage characteristics and oil displacement mechanism of the fluid in the microscopically simulated transparent pore model, and the planar seepage characteristics and oil displacement mechanism of the fluid in the microscopically simulated transparent pore model at any inclination angle. At the same time, the difference in seepage characteristics between top injection and bottom injection can be compared, and the influence of different oil layer dip angles on fluid seepage characteristics in porous media can be analyzed.
以上所述的具体实施例,对本发明的目的、技术方案和有益效果进行了进一步详细说明,所应理解的是,以上所述仅为本发明的具体实施例而已,并不用于限定本发明的保护范围,凡在本发明的精神和原则之内,所做的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。The specific embodiments described above have further described the purpose, technical solutions and beneficial effects of the present invention in detail. It should be understood that the above descriptions are only specific embodiments of the present invention and are not intended to limit the scope of the present invention. Protection scope, within the spirit and principles of the present invention, any modification, equivalent replacement, improvement, etc., shall be included in the protection scope of the present invention.
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