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All Journal Jurnal Bahan Alam Terbarukan Jurnal Agro Fabrica
Wahyu Rinaldi
Jurusan Teknik Kimia, Fakultas Teknik, Universitas Syiah Kuala, Banda Aceh
Chemical Engineering, Chemistry & Bioengineering Materials Science & Nanotechnology Mechanical Engineering

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Synthesis of Triacetin Catalyzed by Activated Natural Zeolite Under Microwave Irradiation Hamzah, Dzikri; Rinaldi, Taufik; Marwan, Marwan; Rinaldi, Wahyu
Jurnal Bahan Alam Terbarukan Vol 8, No 1 (2019): June 2019 [Nationally Accredited - Sinta 2]
Publisher : Universitas Negeri Semarang

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.15294/jbat.v8i1.14028

Abstract

Esterification of glycerol with acetic acid under microwave irradiation in the presence of activated natural zeolite was investigated. Natural zeolite was collected from Ujung Pancu (Aceh Besar) and chemically activated with hydrochloric acid. The reaction was carried out in a stirred glass flask reactor placed inside microwave oven. Experimental variables include microwave transmission time, molar ratio of glycerol to acetic acid, and catalyst loading. XRD profile of activated zeolite showed an increase of Si/Al ratio to 6.042 and the crystallinity decreased slightly by 12.23%, mainly due to dealumination during chemical treatment. Qualitative analysis by FTIR shows that the reaction product obtained by microwave heating contains ester group (triacetin) at wavelength 1706.669 cm-1, while the quantitative analysis by acidi-alkalimetry titration indicates the highest glycerol conversion of 93.033% at the reaction condition of the molar ratio of 1:9, catalyst loading of 3%, and microwave transmission of 10 minutes. The present work suggests that microwave can be utilized as efficient heating technique in esterification of glycerol to triacetin.
OPTIMASI NIRA SAWIT DALAM PEMBUATAN MINUMAN SINBIOTIK DENGAN TAMBAHAN INULIN DAN KULTUR BAKTERI LACTOBACILLUS CASEI Rinaldi, Wahyu; Raja, Pada Mulia; Syukri, Muhammad; Maharani, Rhyna; Rangkuti, Ika Ucha Pradifta
Jurnal Agro Fabrica Vol. 4 No. 1 (2022): Juni 2022
Publisher : Institut Teknologi Sawit Indonesia (ITSI)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.47199/jaf.v4i1.178

Abstract

Oil palm trunks can produce quite a lot of sap water, which is approximately 10 per day for 1 month for 1 oil palm tree that is uprooted, currently, there is not much optimal processing of palm oil with an economical selling price, for this reason, it is necessary to develop functional foods. This study aims to determine whether palm sap can be used in the manufacture of symbiotic beverage products with optimum chemical, microbiological and organoleptic qualities. The study was arranged using a non-factorial Completely Randomized Design (CRD) method with 3 treatments of incubation time, namely 12 hours, 24 hours, and 36 hours with each treatment using 6 replications so that 18 experiments were carried out. The best treatment by SNI 2981:2009 was obtained at an incubation time of 24 hours, namely with a pH of 5.2, water content is 82.50%, total dissolved solids is 17.33%, the lactic acid content is 0.81%, a total lactic acid bacteria of 2.8 x 108 and produces a minimum dense texture with sufficient acidity. The organoleptic aspect of taste and aroma at 24 hours of incubation time was favored or acceptable to consumers with a taste score of 3.3b and aroma of 3.3ab (scale 1-5) in the hedonic rating test. Meanwhile, at 36 hours of incubation, consumers did not like it with a taste score of 2.2a and aroma of 2.1a. This is because the longer the fermentation time can increase the acidity of the product which causes the distinctive taste and aroma of palm sap to increase.
OPTIMASI NIRA SAWIT DALAM PEMBUATAN MINUMAN SINBIOTIK DENGAN TAMBAHAN INULIN DAN KULTUR BAKTERI LACTOBACILLUS CASEI Rinaldi, Wahyu; Raja, Pada Mulia; Syukri, Muhammad; Maharani, Rhyna; Rangkuti, Ika Ucha Pradifta
Jurnal Agro Fabrica Vol. 4 No. 1 (2022): Juni 2022
Publisher : Institut Teknologi Sawit Indonesia (ITSI)

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.47199/jaf.v4i1.178

Abstract

Oil palm trunks can produce quite a lot of sap water, which is approximately 10 per day for 1 month for 1 oil palm tree that is uprooted, currently, there is not much optimal processing of palm oil with an economical selling price, for this reason, it is necessary to develop functional foods. This study aims to determine whether palm sap can be used in the manufacture of symbiotic beverage products with optimum chemical, microbiological and organoleptic qualities. The study was arranged using a non-factorial Completely Randomized Design (CRD) method with 3 treatments of incubation time, namely 12 hours, 24 hours, and 36 hours with each treatment using 6 replications so that 18 experiments were carried out. The best treatment by SNI 2981:2009 was obtained at an incubation time of 24 hours, namely with a pH of 5.2, water content is 82.50%, total dissolved solids is 17.33%, the lactic acid content is 0.81%, a total lactic acid bacteria of 2.8 x 108 and produces a minimum dense texture with sufficient acidity. The organoleptic aspect of taste and aroma at 24 hours of incubation time was favored or acceptable to consumers with a taste score of 3.3b and aroma of 3.3ab (scale 1-5) in the hedonic rating test. Meanwhile, at 36 hours of incubation, consumers did not like it with a taste score of 2.2a and aroma of 2.1a. This is because the longer the fermentation time can increase the acidity of the product which causes the distinctive taste and aroma of palm sap to increase.
Co-Authors Hamzah, Dzikri Heni Pujiastuti Ika Ucha Pradifta Rangkuti Maharani, Rhyna Marwan Marwan Muhammad Syukri Pada Mulia Raja Rinaldi, Taufik