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Preparation of micro-calcite powder using fine-bubble assisted carbonation as toothpaste material Febrida, Renny; Nabillah Salma, Dinda Jihan; Azzahra, Fauziah; Karlina, Elin; Andiesta, Niekla Survia; Faza, Yanwar
Padjadjaran Journal of Dentistry Vol 35, No 1 (2023): March 2023
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjd.vol35no1.44519

Abstract

ABSTRACTIntroduction: Calcite (CaCO3) is typically used in commercial toothpaste with particle size ranges from 1-12 μm. In the latest study, calcite was synthesized by using Ca(OH)2 precursor from natural resources However, the resulting particle size does not match the size of the toothpaste filler. This study aims to prepare micro-calcite via fine-bubble assisted carbonation as toothpaste material. Methods: The calcite powder was prepared from Ca(OH)2 analytical grade powder utilizing the fine-bubble carbonation process with the Ca(OH)2 concentration and initial pH variation. The study was started by making a Ca(OH)2 suspension with a concentration of 0.25, 0.5, 0.75, 1 and 1.25 M using 2.000 ml methanol as a solvent. 0.5 M NaH2PO4 solutions were utilized to adjust the initial pH of 0.5 M Ca(OH)2 suspension into 8, 9, and 10. The suspensions were aerated using CO2 fine-bubble for two hours to produce CaCO3 samples. All precipitated CaCO3 particles were characterized by PSA, Zeta-Potential, and FTIR measurements. Results: The calcite phase was identified from the FTIR transmittance. Aragonite or vaterite phase was not observed in the samples. PSA result shows the size of CaCO3 particles from samples 0.25 M to 1.25 M are as follows 3.03, 3.23, 2.79, 3.70, 0.99 μm respectively. Meanwhile, the particle sizes of CaCO3 in samples with a pH of 8, 9 and 10 are 3.00, 2.03 and 2.50 μm respectively. The zeta potential shows the value ranges from -23.2 mV to -11.9 mV, indicating fair dispersion ability. Conclusion: The fine bubble assisted carbonation method in this study helps in producing calcite in micron size that could be used as alternative fillers for toothpaste.Keywords: calcite, fine-bubble, carbonation, particle size, toothpaste
The effect of ZrCl4, Al(NO3)3 and Na2SiO3 precursors concentration on particle size as dental composites filler through spray pyrolysis method Karlina, Elin; Idznihaq, Khairina; Febrida, Renny; Andiesta, Niekla Survia
Padjadjaran Journal of Dentistry Vol 35, No 1 (2023): March 2023
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjd.vol35no1.44518

Abstract

ABSTRACTIntroduction: one of the important components in dental composites is a filler which can be made through various methods, including spray pyrolysis. In the spray pyrolysis method, some factors determine the size and morphology of the resulting filler particles, one of which is the concentration of precursors. This study aimed to analyze the effect of precursor concentration on the particle size produced using the spray pyrolysis method. Methods: in this experimental laboratory study, zirconia-alumina-silica particles were synthesized using the spray pyrolysis method. The precursor solution consisted of ZrCl4, Al (NO3)3, and Na2SiO3 with a concentration variation of (0.1; 0.2; and 0.3) M. The furnace temperature was set at 750°C, and the electric precipitator temperature was 100°C with a feed rate of 3L/min. Then, the tests performed were using PSA (Particle Size Analyzer), and XRF (X-Ray Fluorescence). Results: The results showed that the best zirconia alumina silica filler particle with the smallest size is the result with a concentration of 0.1 M and its size was 618.6 nm. The particle size for 0.2 M was 911.9 nm and 1799.4 nm for 0.3 M.  According to XRF test results the zirconia alumina silica filler system contains all the precursor elements. Conclusions: The effect of precursor concentration on the particle size produced using the spray pyrolysis method showed that the smaller the precursor concentration used, the smaller the particle size produced. The best results from synthesizing a filler system with a concentration of 0.1 M precursor solution. All the results are in submicron and micron size, and could be used as the component of dental composites.Keywords: precursors concentration, particle size, spray pyrolysis, dental composites filler
The association of oral health knowledge with the behavior of pregnant women visiting the dentist based on the theory of planned behavior: Cross-sectional studies Rizqi, Dikkara; Suryanti, Netty; Suwargiani, Anne Agustina; Andiesta, Niekla Survia
Padjadjaran Journal of Dentistry Vol 36, No 2 (2024): July 2024
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjd.vol36no2.56007

Abstract

ABSTRACTIntroduction: A lack of knowledge of oral health maintenance among pregnant women affects the behavior of maintaining poor oral health.  It is important for pregnant women to visit the dentist due to their increased susceptibility to oral diseases, which can adversely impact pregnancy outcomes, including premature birth and low birth weight. According to the theory of planned behavior, a mother's knowledge can influence her health-related behavior. To determine the level of oral health knowledge among pregnant women and to examine the relationship between this knowledge and the factors that influence their behavior regarding dental visits. Methods: This study uses a correlational analytical design with a cross-sectional approach, focusing on pregnant women at the Cijerah Community Health Centerin Bandung City, Indonesia. A purposive sampling method resulted 67 participants. A new questionnaire assessed oral health knowledge (20 items) and factors influencinh visiting behavior based on the theory of planned behavior (26 items). Data analysis used the Spearman correlation test. Results:Most pregnant women (76.2%) had insufficient oral health knowledge, but showed a positive attitude towards dental visits in the first trimester and every six months (11.91 ± 2.66 and 11.65 ± 2.87). They also reported good subjective norm (28.73 ± 5.42 and 28.31 ± 5.19), good behavioral control (8.23 ± 1.67 and 8.32 ± 1.61) and good intention (3.94 ± 0.96 and 3.83 ± 1.06). Conclusion: The level of oral health knowledge is  low, and althoughfactors influencing the dental visit behavior are positive, there is no correlation between this knowledge and factors that influence the behavior of visiting the dentist.
Effect of mixed water and methanol solvents ratio on the CaCO3 characteristics via fine bubble diffuser as a dental biomaterial Febrida, Renny; Ramadhan, Muhammad Farhan; Karlina, Elin; Andiesta, Niekla Survia
Padjadjaran Journal of Dental Researchers and Students Vol 7, No 1 (2023): Februari 2023
Publisher : Fakultas Kedokteran Gigi Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjdrs.v7i1.40418

Abstract

ABSTRACTIntroduction: The application of calcium carbonate in dental biomaterial depends on the charcateristics after the synthesis process. This study aims to determine the effect of the ratio of methanol and water on the characteristics of the CaCo3 produced through the fine bubble diffuser method. Methods: Synthesis of calcium carbonate by CO2 carbonation method using fine bubble diffuser to produce fine CO2 bubbles (bubble size range 100-500 nm). The Ca(OH)2 precursor was dissolved in various ratios of water and methanol mixtures, namely: 25% water 75% methanol, 20% water 80% methanol, 15% water 85% methanol, 10% water 90% methanol, 5% water 95% methanol, and 100% methanol. The suspension was carbonated using CO2 fine bubbles for 2 hours to produce CaCO3 powder. The resulting calcium carbonate powder was tested with FTIR (Fourier Transform Infra Red), PSA (Particle Size Analyzer), and Zeta-Potential. Results: The FTIR test obtained the wave numbers of calcite (712 cm-1), vaterite (744, 873, 874, and 875 cm-1) and aragonite (848, 849, and 854 cm-1) phases in the six variations of the solvent used. The PSA test showed that the particle size produced was submicron with the smallest size being 191.1 nm and the largest being 576.2 nm. The ZetaPotential test showed that the particles were relatively stable in solution with a Zeta-Potential value range of -15.1 mV to -20.8 mV and particles with moderate stability -21.2 mV to -25.1 mV. Conclusion: The addition of the organic solvent methanol to water increases the solubility of CaOH and increases the formation of the vaterite phase. Increasing the amount of water decreases the amount of vaterite phase, increasing the particle size and zeta potential value. but the addition of 15% water decreases the particle size of CaCO3 KEY WORDSCaCO3, fine bubble diffuser, FTIR, PSA, zeta potential Pengaruh perbandingan campuran pelarut air dan metanol terhadap karakteristik CaCO3 melalui metode fine bubble diffuser sebagai biomaterial kedokteran gigiABSTRAKPendahuluan: Kalsium karbonat (CaCO3) merupakan salah satu sumber kalsium yang umum digunakan di bidang biomaterial kedokteran gigi. Aplikasi kalsium karbonat tergantung dari fasa dan ukuran partikelnya. Penelitian ini bertujuan untuk mengetahui pengaruh perbandingan metanol dan air terhadap karakteristik CaCO3 yang dihasilkan melalui metode fine bubble diffuser. Metode: Prekursor Ca(OH)2 dilarutkan dengan berbagai variasi campuran pelarut air dan metanol, yaitu: 25% air 75% metanol, 20% air 80% metanol, 15% air 85% metanol, 10% air 90% metanol, 5% air 95% metanol, dan 100% metanol. Suspensi Ca(OH)2 dikarbonasi menggunakan gelembung halus CO2 selama 2 jam untuk menghasilkan bubuk CaCO3. Bubuk CaCO3 yang dihasilkan diuji dengan FTIR (Fourier Transform Infra Red), PSA (Particle Size Analyzer), dan ZetaPotential. Hasil: Uji FTIR didapatkan bilangan gelombang fasa kalsit (712 cm-1 ), vaterit (744, 873, 874, dan 875 cm-1 ) dan aragonit (848, 849, dan 854 cm-1 ) pada keenam variasi pelarut yang digunakan. Uji PSA didapatkan ukuran partikel terkecil 191,1 nm dan terbesar 576,2 nm. Partikel relatif stabil dalam larutan berdasarkan Uji Zeta-Potential (-15,1 mV sampai -17,8 mV) dan stabilitas moderat (-20,8 mV sampai -25,1 mV). Simpulan: Penambahan pelarut organik methanol pada pelarut air meningkatkan kelarutan CaOH dan meningkatkan pembentukan fasa vaterite. peningkatan jumlah air menurunkan jumlah fasa vaterite, meningkatkan ukuran partikel dan nilai zeta potensial. namun pada penambahan 15% air dan seterusnya menurunkan ukuran partikel CaCO3. KATA KUNCI CaCO3, fine bubble diffuser, FTIR, PSA, zeta potential
The effectiveness of brushing the teeth using two shapes of toothbrush Riyanti, Eriska; Andisetyanto, Prima; Pratidina, Naninda Berliana; Primarti, Risti Saptarini; Andiesta, Niekla Survia
Padjadjaran Journal of Dentistry Vol 33, No 2 (2021): July 2021
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjd.vol33no2.34790

Abstract

Introduction: Dental and oral health or cleanliness is one indicator to measure the effectiveness of brushing teeth, particularly concerning the type and shape of toothbrush and the way of brushing teeth. The aim of the study was to find out the effectiveness of plaque index decrease before and after brushing teeth using two different types of the toothbrush.  Methods: The investigation was carried out using single-blind and parallel quasi-experimental methods.  The sample comprises 30 people from Bandung City aged between 6 – 7 years old, selected through purposive sampling.  The subjects were directly categorized into two groups of treatment.  Patient Hygiene Performance Modification (PHP-M) used to measure the amount of plaque. Results: The data were analyzed using paired t-test and independent t-test.  The straight-handled toothbrush yielded a score of 11.967 in the paired t-test.  This score is higher than the t-table (t = 2.160; p < 0.05), which meant that the H0 is rejected.  The angled-handled toothbrush had a score of 7.385 in the paired t-test.  The score is higher than the t-table (t = 2.131; p < 0.05), which meant that the H0 is rejected.  The statistical analysis using independent t-test yielded a score of 1.814, which was lower than the t-table (t = 2.048; p > 0.05). Thus, meaning that the H0 is accepted. Conclusion: It was concluded that there is no difference in the plaque index before and after brushing teeth using the two types of the toothbrush.
Prevalence of maxillary and mandibular physiological space in the primary dentition Megan, Felisia Flaviana; Andiesta, Niekla Survia; Indriyanti, Ratna; Setiawan, Arlette Suzy Puspa Pertiwi
Padjadjaran Journal of Dentistry Vol 32, No 1 (2020): March 2020
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjd.vol32no1.19317

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Introduction: Physiological space is the space between maxillary and mandibular primary central incisors as well as maxillary and mandibular primary lateral incisors that occur during primary dentition period. The absence of physiological space will lead the crowded of permanent dentition due to discrepancy of the size of tooth and jaw. The objective of this study was to evaluate and analyse the prevalence of physiological space of maxillary and mandibular during primary dentition period. Methods: The type of research was a descriptive survey technique. The study was conducted at the Early Childhood Education (PAUD) in Bandung City throughout January-March 2017. The study population was children aged 3-5 years. Multistage cluster sampling used to choose subjects based on the division of the area from the city area to obtain the desired population. The data used were primary data obtained by examining the existence of a gap with a gap width indicator that is used as a benchmark of at least 0.5 mm with the help of WHO probe tool. Data were collected, processed and analysed using the SPSS (Statistical Package for Social Sciences) version 20. Results: A total of 65 out of 97 subjects had physiological space in their first dentition period. From 97 study subjects (100%) examined, 44 children (45.36%) had maxillary physiological space, and 53 children (54.64%) did not have maxillary physiological space. In 97 research subjects (100%) there were also 48 children (49.48%) having physiological space in the lower jaw, and 49 children (50.52%) did not have physiological space in the lower jaw. Conclusion: Prevalence of the maxillary and mandibular physiological space in the primary dentition period of children in the city of Bandung are 67.01%.
Correlation between mandibular bone density with CD4-T cells and duration of HAART in HIV-infected children Maulani, Intan; Primarti, Risti Saptarini; Sufiawati, Irna; Indriyanti, Ratna; Andiesta, Niekla Survia; Riyanti, Eriska
Padjadjaran Journal of Dentistry Vol 33, No 1 (2021): March 2021
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjd.vol33no1.15894

Abstract

Introduction: Perinatal HIV infection has decreased adverse bone health effects and mineral accrual. HIV-infected patients have a multifactorial origin, including HIV bone cell infections, inflammatory cytokine effects on osteoblast and osteoclast activity, and HAART. The research objective was to analyze the correlation between the mandibular bone density with CD4 T-cells and duration of HAART in HIV-infected children. Methods: The mandibular bone density in the HIV-infected pediatric population was evaluated using a panoramic radiograph. The research design was a cross-sectional and univariate regression analysis for the sampling method. Mandibular density analysis using Spearman and Pearson correlation and HAART duration using Kendall correlation. Thirty-five HIV-infected children and seventeen non-HIV-infected children were recruited. Results: This study showed the significant correlation between Mandibular cortical shape index of HIV-infected and non-HIV children and there is a significant correlation between fractal dimension of HIV-infected and non-HIV children (p<0.05). There is no significant correlation between mandibular bone density and the CD4 level(p<0.05). Mandibular bone density and duration HAART and have a significant correlation (p<0.001). This research showed correlations between mandibular bone density CD4 T-cells and duration of HAART in HIV-infected children. Conclusion: There is no correlation between the mandibular bone density and CD4 T-cells count, however, there is a correlation between the mandibular bone density and duration of HAART in HIV-infected children.
Relationship between protein deficiency accompanied by low body mass index with the head shape and face type of 6-7 years old children Gunawan, Idelia; Andiesta, Niekla Survia; Gartika, Meirina; Primarti, Risti Saptarini
Padjadjaran Journal of Dentistry Vol 32, No 1 (2020): March 2020
Publisher : Faculty of Dentistry Universitas Padjadjaran

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.24198/pjd.vol32no1.21165

Abstract

Introduction: Environmental factors such as socio-economic and nutrients factor can affect the dimensions and proportions of the body. Nutritional intake has a long-term effect on physical growth and can be assessed through body mass index up to age. Children with a nutritional disorder are characterised with low body mass index. This study was aimed to analyse the relationship of protein deficiency and low body mass index on the head shape and facial type of 6-7 years old children. Methods: The research type was descriptive correlative, and the research was conducted towards 16 subjects with low body mass index. Protein deficiency was assessed from food intake for 3 x 24 hours through food recall method and interview. The measurement of the cephalic and facial index was carried out to find out the head shape and face type, and then to correlate with protein deficiency and body mass index. Data was analysed using the chi-square test with the significance (p-value)<0.05. Results: There was a significant correlation between protein deficiency and low body mass index with the head shape (p-value=0.007), and the facial type of 6-7 years old children (p-value=0.027). There was a significant correlation between head shape with facial type in protein-deficient children with low body mass index (p-value=0). Conclusion: Protein deficiency accompanied by low body mass index influences the head shape and facial type of children.